Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method

Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formul...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Jian, Yu [verfasserIn] He, Yong [verfasserIn] Jiang, Tongzhou [verfasserIn] Li, Chunguang [verfasserIn] Yang, Wantai [verfasserIn] Nie, Jun [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2012

Schlagwörter:	Real-time UV-curing Volume shrinkage

Übergeordnetes Werk:	Enthalten in: Journal of coatings technology and research - Blue Bell, Pa., 2004, 10(2012), 2 vom: 04. Okt., Seite 231-237
Übergeordnetes Werk:	volume:10 ; year:2012 ; number:2 ; day:04 ; month:10 ; pages:231-237

Links:	Volltext

DOI / URN:	10.1007/s11998-012-9446-2

Katalog-ID:	SPR023533463

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520			\|a Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion.
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912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_120
912			\|a GBV_ILN_138
912			\|a GBV_ILN_150
912			\|a GBV_ILN_151
912			\|a GBV_ILN_161
912			\|a GBV_ILN_170
912			\|a GBV_ILN_171
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_250
912			\|a GBV_ILN_266
912			\|a GBV_ILN_281
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_702
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2008
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2070
912			\|a GBV_ILN_2086
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2113
912			\|a GBV_ILN_2116
912			\|a GBV_ILN_2118
912			\|a GBV_ILN_2119
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2144
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912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2188
912			\|a GBV_ILN_2190
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2446
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2472
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_2548
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4046
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
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912			\|a GBV_ILN_4324
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912			\|a GBV_ILN_4333
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912			\|a GBV_ILN_4336
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matchkey_str	article:19353804:2012----::ouehikgoucrbeotnfruainnetgtdyel
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allfields	10.1007/s11998-012-9446-2 doi (DE-627)SPR023533463 (SPR)s11998-012-9446-2-e DE-627 ger DE-627 rakwb eng 600 ASE Jian, Yu verfasserin aut Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion. Real-time (dpeaa)DE-He213 UV-curing (dpeaa)DE-He213 Volume shrinkage (dpeaa)DE-He213 He, Yong verfasserin aut Jiang, Tongzhou verfasserin aut Li, Chunguang verfasserin aut Yang, Wantai verfasserin aut Nie, Jun verfasserin aut Enthalten in Journal of coatings technology and research Blue Bell, Pa., 2004 10(2012), 2 vom: 04. Okt., Seite 231-237 (DE-627)51834584X (DE-600)2252471-X 1935-3804 nnns volume:10 year:2012 number:2 day:04 month:10 pages:231-237 https://dx.doi.org/10.1007/s11998-012-9446-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2012 2 04 10 231-237
spelling	10.1007/s11998-012-9446-2 doi (DE-627)SPR023533463 (SPR)s11998-012-9446-2-e DE-627 ger DE-627 rakwb eng 600 ASE Jian, Yu verfasserin aut Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion. Real-time (dpeaa)DE-He213 UV-curing (dpeaa)DE-He213 Volume shrinkage (dpeaa)DE-He213 He, Yong verfasserin aut Jiang, Tongzhou verfasserin aut Li, Chunguang verfasserin aut Yang, Wantai verfasserin aut Nie, Jun verfasserin aut Enthalten in Journal of coatings technology and research Blue Bell, Pa., 2004 10(2012), 2 vom: 04. Okt., Seite 231-237 (DE-627)51834584X (DE-600)2252471-X 1935-3804 nnns volume:10 year:2012 number:2 day:04 month:10 pages:231-237 https://dx.doi.org/10.1007/s11998-012-9446-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2012 2 04 10 231-237
allfields_unstemmed	10.1007/s11998-012-9446-2 doi (DE-627)SPR023533463 (SPR)s11998-012-9446-2-e DE-627 ger DE-627 rakwb eng 600 ASE Jian, Yu verfasserin aut Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion. Real-time (dpeaa)DE-He213 UV-curing (dpeaa)DE-He213 Volume shrinkage (dpeaa)DE-He213 He, Yong verfasserin aut Jiang, Tongzhou verfasserin aut Li, Chunguang verfasserin aut Yang, Wantai verfasserin aut Nie, Jun verfasserin aut Enthalten in Journal of coatings technology and research Blue Bell, Pa., 2004 10(2012), 2 vom: 04. Okt., Seite 231-237 (DE-627)51834584X (DE-600)2252471-X 1935-3804 nnns volume:10 year:2012 number:2 day:04 month:10 pages:231-237 https://dx.doi.org/10.1007/s11998-012-9446-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2012 2 04 10 231-237
allfieldsGer	10.1007/s11998-012-9446-2 doi (DE-627)SPR023533463 (SPR)s11998-012-9446-2-e DE-627 ger DE-627 rakwb eng 600 ASE Jian, Yu verfasserin aut Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion. Real-time (dpeaa)DE-He213 UV-curing (dpeaa)DE-He213 Volume shrinkage (dpeaa)DE-He213 He, Yong verfasserin aut Jiang, Tongzhou verfasserin aut Li, Chunguang verfasserin aut Yang, Wantai verfasserin aut Nie, Jun verfasserin aut Enthalten in Journal of coatings technology and research Blue Bell, Pa., 2004 10(2012), 2 vom: 04. Okt., Seite 231-237 (DE-627)51834584X (DE-600)2252471-X 1935-3804 nnns volume:10 year:2012 number:2 day:04 month:10 pages:231-237 https://dx.doi.org/10.1007/s11998-012-9446-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2012 2 04 10 231-237
allfieldsSound	10.1007/s11998-012-9446-2 doi (DE-627)SPR023533463 (SPR)s11998-012-9446-2-e DE-627 ger DE-627 rakwb eng 600 ASE Jian, Yu verfasserin aut Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion. Real-time (dpeaa)DE-He213 UV-curing (dpeaa)DE-He213 Volume shrinkage (dpeaa)DE-He213 He, Yong verfasserin aut Jiang, Tongzhou verfasserin aut Li, Chunguang verfasserin aut Yang, Wantai verfasserin aut Nie, Jun verfasserin aut Enthalten in Journal of coatings technology and research Blue Bell, Pa., 2004 10(2012), 2 vom: 04. Okt., Seite 231-237 (DE-627)51834584X (DE-600)2252471-X 1935-3804 nnns volume:10 year:2012 number:2 day:04 month:10 pages:231-237 https://dx.doi.org/10.1007/s11998-012-9446-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_266 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2012 2 04 10 231-237
language	English
source	Enthalten in Journal of coatings technology and research 10(2012), 2 vom: 04. Okt., Seite 231-237 volume:10 year:2012 number:2 day:04 month:10 pages:231-237
sourceStr	Enthalten in Journal of coatings technology and research 10(2012), 2 vom: 04. Okt., Seite 231-237 volume:10 year:2012 number:2 day:04 month:10 pages:231-237
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Real-time UV-curing Volume shrinkage
dewey-raw	600
isfreeaccess_bool	false
container_title	Journal of coatings technology and research
authorswithroles_txt_mv	Jian, Yu @@aut@@ He, Yong @@aut@@ Jiang, Tongzhou @@aut@@ Li, Chunguang @@aut@@ Yang, Wantai @@aut@@ Nie, Jun @@aut@@
publishDateDaySort_date	2012-10-04T00:00:00Z
hierarchy_top_id	51834584X
dewey-sort	3600
id	SPR023533463
language_de	englisch
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author	Jian, Yu
spellingShingle	Jian, Yu ddc 600 misc Real-time misc UV-curing misc Volume shrinkage Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method
authorStr	Jian, Yu
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topic_title	600 ASE Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method Real-time (dpeaa)DE-He213 UV-curing (dpeaa)DE-He213 Volume shrinkage (dpeaa)DE-He213
topic	ddc 600 misc Real-time misc UV-curing misc Volume shrinkage
topic_unstemmed	ddc 600 misc Real-time misc UV-curing misc Volume shrinkage
topic_browse	ddc 600 misc Real-time misc UV-curing misc Volume shrinkage
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title	Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method
ctrlnum	(DE-627)SPR023533463 (SPR)s11998-012-9446-2-e
title_full	Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method
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journal	Journal of coatings technology and research
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author_browse	Jian, Yu He, Yong Jiang, Tongzhou Li, Chunguang Yang, Wantai Nie, Jun
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class	600 ASE
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doi_str_mv	10.1007/s11998-012-9446-2
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author2-role	verfasserin
title_sort	volume shrinkage of uv-curable coating formulation investigated by real-time laser reflection method
title_auth	Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method
abstract	Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion.
abstractGer	Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion.
abstract_unstemmed	Abstract Volume shrinkage is one of the main drawbacks of UV-cured coatings and can lead to premature coating failures. Due to the rapid polymerization during UV-curing, real-time volume shrinkage has been challenging to measure accurately. In this article, the shrinkage process of UV-curable formulations was systematically investigated by a recently developed laser reflection method. The influence of oligomers, monomers, and photoinitiators on shrinkage process has been evaluated. Compared with the oligomers, the monomer was the main contributor to shrinkage due to the high concentration of double bonds. Polymerization shrinkage could be reduced by increasing the oligomer/monomer ratio. Because monomers were the main contributors of shrinkage, the chemical structure of monomers was important for decreasing shrinkage. Methacrylate monomers decreased the final shrinkage but unfortunately reduced the conversion. Monomers with a high degree of ethoxylation lowered the shrinkage and simultaneously increased the conversion. The concentration of photoinitiators had no obvious effect on the normalized shrinkage. Thus, the low shrinkage caused by the low concentration of photoinitiators was only attributed to the significant drop of the conversion.
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container_issue	2
title_short	Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method
url	https://dx.doi.org/10.1007/s11998-012-9446-2
remote_bool	true
author2	He, Yong Jiang, Tongzhou Li, Chunguang Yang, Wantai Nie, Jun
author2Str	He, Yong Jiang, Tongzhou Li, Chunguang Yang, Wantai Nie, Jun
ppnlink	51834584X
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isOA_txt	false
hochschulschrift_bool	false
doi_str	10.1007/s11998-012-9446-2
up_date	2024-07-03T19:31:50.713Z
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Volume shrinkage of UV-curable coating formulation investigated by real-time laser reflection method

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