Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations

Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of...
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Gespeichert in:

Autor*in:	Iyer, Rajesh [verfasserIn] Desai, Rucha [verfasserIn] Upadhyay, R. V. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2009

Schlagwörter:	Nanosized mixed ferrites superparamagnetism spinel phase

Übergeordnetes Werk:	Enthalten in: Bulletin of materials science - Bangalore, 1979, 32(2009), 2 vom: Apr., Seite 141-147
Übergeordnetes Werk:	volume:32 ; year:2009 ; number:2 ; month:04 ; pages:141-147

Links:	Volltext

DOI / URN:	10.1007/s12034-009-0021-0

Katalog-ID:	SPR023922729

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245	1	0	\|a Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations
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520			\|a Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found.
650		4	\|a Nanosized mixed ferrites \|7 (dpeaa)DE-He213
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matchkey_str	article:09737669:2009----::otmeaueyteionnszdn1z_f_o4ertsn
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allfields	10.1007/s12034-009-0021-0 doi (DE-627)SPR023922729 (SPR)s12034-009-0021-0-e DE-627 ger DE-627 rakwb eng 600 ASE 51.00 bkl Iyer, Rajesh verfasserin aut Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found. Nanosized mixed ferrites (dpeaa)DE-He213 superparamagnetism (dpeaa)DE-He213 spinel phase (dpeaa)DE-He213 Desai, Rucha verfasserin aut Upadhyay, R. V. verfasserin aut Enthalten in Bulletin of materials science Bangalore, 1979 32(2009), 2 vom: Apr., Seite 141-147 (DE-627)358454425 (DE-600)2096424-9 0973-7669 nnns volume:32 year:2009 number:2 month:04 pages:141-147 https://dx.doi.org/10.1007/s12034-009-0021-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 32 2009 2 04 141-147
spelling	10.1007/s12034-009-0021-0 doi (DE-627)SPR023922729 (SPR)s12034-009-0021-0-e DE-627 ger DE-627 rakwb eng 600 ASE 51.00 bkl Iyer, Rajesh verfasserin aut Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found. Nanosized mixed ferrites (dpeaa)DE-He213 superparamagnetism (dpeaa)DE-He213 spinel phase (dpeaa)DE-He213 Desai, Rucha verfasserin aut Upadhyay, R. V. verfasserin aut Enthalten in Bulletin of materials science Bangalore, 1979 32(2009), 2 vom: Apr., Seite 141-147 (DE-627)358454425 (DE-600)2096424-9 0973-7669 nnns volume:32 year:2009 number:2 month:04 pages:141-147 https://dx.doi.org/10.1007/s12034-009-0021-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 32 2009 2 04 141-147
allfields_unstemmed	10.1007/s12034-009-0021-0 doi (DE-627)SPR023922729 (SPR)s12034-009-0021-0-e DE-627 ger DE-627 rakwb eng 600 ASE 51.00 bkl Iyer, Rajesh verfasserin aut Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found. Nanosized mixed ferrites (dpeaa)DE-He213 superparamagnetism (dpeaa)DE-He213 spinel phase (dpeaa)DE-He213 Desai, Rucha verfasserin aut Upadhyay, R. V. verfasserin aut Enthalten in Bulletin of materials science Bangalore, 1979 32(2009), 2 vom: Apr., Seite 141-147 (DE-627)358454425 (DE-600)2096424-9 0973-7669 nnns volume:32 year:2009 number:2 month:04 pages:141-147 https://dx.doi.org/10.1007/s12034-009-0021-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 32 2009 2 04 141-147
allfieldsGer	10.1007/s12034-009-0021-0 doi (DE-627)SPR023922729 (SPR)s12034-009-0021-0-e DE-627 ger DE-627 rakwb eng 600 ASE 51.00 bkl Iyer, Rajesh verfasserin aut Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found. Nanosized mixed ferrites (dpeaa)DE-He213 superparamagnetism (dpeaa)DE-He213 spinel phase (dpeaa)DE-He213 Desai, Rucha verfasserin aut Upadhyay, R. V. verfasserin aut Enthalten in Bulletin of materials science Bangalore, 1979 32(2009), 2 vom: Apr., Seite 141-147 (DE-627)358454425 (DE-600)2096424-9 0973-7669 nnns volume:32 year:2009 number:2 month:04 pages:141-147 https://dx.doi.org/10.1007/s12034-009-0021-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 32 2009 2 04 141-147
allfieldsSound	10.1007/s12034-009-0021-0 doi (DE-627)SPR023922729 (SPR)s12034-009-0021-0-e DE-627 ger DE-627 rakwb eng 600 ASE 51.00 bkl Iyer, Rajesh verfasserin aut Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations 2009 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found. Nanosized mixed ferrites (dpeaa)DE-He213 superparamagnetism (dpeaa)DE-He213 spinel phase (dpeaa)DE-He213 Desai, Rucha verfasserin aut Upadhyay, R. V. verfasserin aut Enthalten in Bulletin of materials science Bangalore, 1979 32(2009), 2 vom: Apr., Seite 141-147 (DE-627)358454425 (DE-600)2096424-9 0973-7669 nnns volume:32 year:2009 number:2 month:04 pages:141-147 https://dx.doi.org/10.1007/s12034-009-0021-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 51.00 ASE AR 32 2009 2 04 141-147
language	English
source	Enthalten in Bulletin of materials science 32(2009), 2 vom: Apr., Seite 141-147 volume:32 year:2009 number:2 month:04 pages:141-147
sourceStr	Enthalten in Bulletin of materials science 32(2009), 2 vom: Apr., Seite 141-147 volume:32 year:2009 number:2 month:04 pages:141-147
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Nanosized mixed ferrites superparamagnetism spinel phase
dewey-raw	600
isfreeaccess_bool	false
container_title	Bulletin of materials science
authorswithroles_txt_mv	Iyer, Rajesh @@aut@@ Desai, Rucha @@aut@@ Upadhyay, R. V. @@aut@@
publishDateDaySort_date	2009-04-01T00:00:00Z
hierarchy_top_id	358454425
dewey-sort	3600
id	SPR023922729
language_de	englisch
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author	Iyer, Rajesh
spellingShingle	Iyer, Rajesh ddc 600 bkl 51.00 misc Nanosized mixed ferrites misc superparamagnetism misc spinel phase Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations
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topic_title	600 ASE 51.00 bkl Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations Nanosized mixed ferrites (dpeaa)DE-He213 superparamagnetism (dpeaa)DE-He213 spinel phase (dpeaa)DE-He213
topic	ddc 600 bkl 51.00 misc Nanosized mixed ferrites misc superparamagnetism misc spinel phase
topic_unstemmed	ddc 600 bkl 51.00 misc Nanosized mixed ferrites misc superparamagnetism misc spinel phase
topic_browse	ddc 600 bkl 51.00 misc Nanosized mixed ferrites misc superparamagnetism misc spinel phase
format_facet	Elektronische Aufsätze Aufsätze Elektronische Ressource
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title	Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations
ctrlnum	(DE-627)SPR023922729 (SPR)s12034-009-0021-0-e
title_full	Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations
author_sort	Iyer, Rajesh
journal	Bulletin of materials science
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author_browse	Iyer, Rajesh Desai, Rucha Upadhyay, R. V.
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class	600 ASE 51.00 bkl
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author-letter	Iyer, Rajesh
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title_sort	low temperature synthesis of nanosized $ mn_{1−x} %$ zn_{x} %$ fe_{2} %$ o_{4} $ ferrites and their characterizations
title_auth	Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations
abstract	Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found.
abstractGer	Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found.
abstract_unstemmed	Abstract Nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ (x = 0, 0·1, 0·3, 0·5, 0·6, 0·7, 0·9) mixed ferrite samples of particle size < 12 nm were prepared using the co-precipitation technique by doping the $ Zn^{2+} $ ion impurities. Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. The lattice constant is found to be constantly decreasing till x = 0·6 and beyond this an unusual slight increase in the lattice constant is found.
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title_short	Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations
url	https://dx.doi.org/10.1007/s12034-009-0021-0
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up_date	2024-07-03T22:20:51.130Z
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Autoclave was employed to maintain constant temperature of 80°C and a constant pressure. The X-ray analysis and the IR spectrum analysis were carried out to confirm the spinel phase formation as well as to ascertain the cation distribution in the ferrite samples. This clearly points to the fact that the $ Zn^{2+} $ ion’s presence is not restricted to A-site alone for some of the Mn-Zn ferrite series. The real part of a.c. susceptibility measurements clearly indicated the superparamagnetic behaviour of the ferrite samples. There is a systematic decrease in the particle size, Curie temperature and magnetization with the increase in the $ Zn^{2+} $ ion doping, measured using magneto thermal gravimetric analysis (MTGA) and vibrating sample magnetometer (VSM), respectively. 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Low temperature synthesis of nanosized $ Mn_{1−x} %$ Zn_{x} %$ Fe_{2} %$ O_{4} $ ferrites and their characterizations

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