Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry
Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The prelimin...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
de Andrade, Rodolpho M. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media New York 2016 |
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| Übergeordnetes Werk: |
Enthalten in: Food analytical methods - New York, NY : Springer, 2008, 10(2016), 5 vom: 12. Okt., Seite 1209-1215 |
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| Übergeordnetes Werk: |
volume:10 ; year:2016 ; number:5 ; day:12 ; month:10 ; pages:1209-1215 |
| Links: |
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| DOI / URN: |
10.1007/s12161-016-0659-3 |
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| Katalog-ID: |
SPR025188135 |
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| 520 | |a Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. | ||
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| 700 | 1 | |a de Gois, Jefferson S. |4 aut | |
| 700 | 1 | |a Toaldo, Isabela Maia |4 aut | |
| 700 | 1 | |a Batista, Diego Barros |4 aut | |
| 700 | 1 | |a Luna, Aderval S. |4 aut | |
| 700 | 1 | |a Borges, Daniel L. G. |4 aut | |
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10.1007/s12161-016-0659-3 doi (DE-627)SPR025188135 (SPR)s12161-016-0659-3-e DE-627 ger DE-627 rakwb eng de Andrade, Rodolpho M. verfasserin aut Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media New York 2016 Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. HR-CS GF AAS (dpeaa)DE-He213 Direct solid sample analysis (dpeaa)DE-He213 Food samples (dpeaa)DE-He213 de Gois, Jefferson S. aut Toaldo, Isabela Maia aut Batista, Diego Barros aut Luna, Aderval S. aut Borges, Daniel L. G. aut Enthalten in Food analytical methods New York, NY : Springer, 2008 10(2016), 5 vom: 12. Okt., Seite 1209-1215 (DE-627)566007320 (DE-600)2424728-5 1936-976X nnns volume:10 year:2016 number:5 day:12 month:10 pages:1209-1215 https://dx.doi.org/10.1007/s12161-016-0659-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2016 5 12 10 1209-1215 |
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10.1007/s12161-016-0659-3 doi (DE-627)SPR025188135 (SPR)s12161-016-0659-3-e DE-627 ger DE-627 rakwb eng de Andrade, Rodolpho M. verfasserin aut Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media New York 2016 Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. HR-CS GF AAS (dpeaa)DE-He213 Direct solid sample analysis (dpeaa)DE-He213 Food samples (dpeaa)DE-He213 de Gois, Jefferson S. aut Toaldo, Isabela Maia aut Batista, Diego Barros aut Luna, Aderval S. aut Borges, Daniel L. G. aut Enthalten in Food analytical methods New York, NY : Springer, 2008 10(2016), 5 vom: 12. Okt., Seite 1209-1215 (DE-627)566007320 (DE-600)2424728-5 1936-976X nnns volume:10 year:2016 number:5 day:12 month:10 pages:1209-1215 https://dx.doi.org/10.1007/s12161-016-0659-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2016 5 12 10 1209-1215 |
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10.1007/s12161-016-0659-3 doi (DE-627)SPR025188135 (SPR)s12161-016-0659-3-e DE-627 ger DE-627 rakwb eng de Andrade, Rodolpho M. verfasserin aut Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media New York 2016 Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. HR-CS GF AAS (dpeaa)DE-He213 Direct solid sample analysis (dpeaa)DE-He213 Food samples (dpeaa)DE-He213 de Gois, Jefferson S. aut Toaldo, Isabela Maia aut Batista, Diego Barros aut Luna, Aderval S. aut Borges, Daniel L. G. aut Enthalten in Food analytical methods New York, NY : Springer, 2008 10(2016), 5 vom: 12. Okt., Seite 1209-1215 (DE-627)566007320 (DE-600)2424728-5 1936-976X nnns volume:10 year:2016 number:5 day:12 month:10 pages:1209-1215 https://dx.doi.org/10.1007/s12161-016-0659-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2016 5 12 10 1209-1215 |
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10.1007/s12161-016-0659-3 doi (DE-627)SPR025188135 (SPR)s12161-016-0659-3-e DE-627 ger DE-627 rakwb eng de Andrade, Rodolpho M. verfasserin aut Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media New York 2016 Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. HR-CS GF AAS (dpeaa)DE-He213 Direct solid sample analysis (dpeaa)DE-He213 Food samples (dpeaa)DE-He213 de Gois, Jefferson S. aut Toaldo, Isabela Maia aut Batista, Diego Barros aut Luna, Aderval S. aut Borges, Daniel L. G. aut Enthalten in Food analytical methods New York, NY : Springer, 2008 10(2016), 5 vom: 12. Okt., Seite 1209-1215 (DE-627)566007320 (DE-600)2424728-5 1936-976X nnns volume:10 year:2016 number:5 day:12 month:10 pages:1209-1215 https://dx.doi.org/10.1007/s12161-016-0659-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2016 5 12 10 1209-1215 |
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10.1007/s12161-016-0659-3 doi (DE-627)SPR025188135 (SPR)s12161-016-0659-3-e DE-627 ger DE-627 rakwb eng de Andrade, Rodolpho M. verfasserin aut Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media New York 2016 Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. HR-CS GF AAS (dpeaa)DE-He213 Direct solid sample analysis (dpeaa)DE-He213 Food samples (dpeaa)DE-He213 de Gois, Jefferson S. aut Toaldo, Isabela Maia aut Batista, Diego Barros aut Luna, Aderval S. aut Borges, Daniel L. G. aut Enthalten in Food analytical methods New York, NY : Springer, 2008 10(2016), 5 vom: 12. Okt., Seite 1209-1215 (DE-627)566007320 (DE-600)2424728-5 1936-976X nnns volume:10 year:2016 number:5 day:12 month:10 pages:1209-1215 https://dx.doi.org/10.1007/s12161-016-0659-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2016 5 12 10 1209-1215 |
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de Andrade, Rodolpho M. @@aut@@ de Gois, Jefferson S. @@aut@@ Toaldo, Isabela Maia @@aut@@ Batista, Diego Barros @@aut@@ Luna, Aderval S. @@aut@@ Borges, Daniel L. G. @@aut@@ |
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The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). 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de Andrade, Rodolpho M. |
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Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry HR-CS GF AAS (dpeaa)DE-He213 Direct solid sample analysis (dpeaa)DE-He213 Food samples (dpeaa)DE-He213 |
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direct determination of trace elements in meat samples via high-resolution graphite furnace atomic absorption spectrometry |
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Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry |
| abstract |
Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. © Springer Science+Business Media New York 2016 |
| abstractGer |
Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. © Springer Science+Business Media New York 2016 |
| abstract_unstemmed |
Abstract This work presents a direct and straightforward approach for the determination of trace elements in fish muscle, oyster, and bovine liver via direct solid sample analysis (SS) using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR-CS GF AAS). The preliminary studies revealed the presence of spectral interferences at the analytical line of Ni at 231.096 nm, which could be corrected subtracting the spectrum of SiO and PO from the sample spectra using least-squares background correction. Moreover, all meat samples were proven homogeneous according to the homogeneity factor (He) (all values were <10 $ mg^{½} $). Pyrolysis (Tp) and atomization (Ta) temperatures were studied and optimized as 800 °C (Tp) and 2500 °C (Ta) for Mn, 700 °C (Tp) and 2600 °C (Ta) for Ni, and 600 °C (Tp) and 2500 °C (Ta) for Rb. Calibration against aqueous standards was proven feasible for Mn determination, whereas Ni and Rb required calibration against solid standards for their quantification. The detection limits achieved were demonstrated adequate for application to food analysis (0.005 μg $ g^{−1} $ for Mn, 0.002 μg $ g^{−1} $ for Ni, and 0.1 μg $ g^{−1} $ for Rb). The developed method was successfully applied for the elemental analysis of fish muscle, oyster, and bovine liver and three certified reference materials, demonstrating good agreement with the certified values and with the reference technique at a 95 % statistical confidence level. © Springer Science+Business Media New York 2016 |
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Direct Determination of Trace Elements in Meat Samples via High-Resolution Graphite Furnace Atomic Absorption Spectrometry |
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de Gois, Jefferson S. Toaldo, Isabela Maia Batista, Diego Barros Luna, Aderval S. Borges, Daniel L. G. |
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de Gois, Jefferson S. Toaldo, Isabela Maia Batista, Diego Barros Luna, Aderval S. Borges, Daniel L. G. |
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10.1007/s12161-016-0659-3 |
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| score |
7.4019966 |