Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode

Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2}...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Lakshmanan, R. [verfasserIn] Bhuvaneswari, D. [verfasserIn] Kalaiselvi, N. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2012

Übergeordnetes Werk:	Enthalten in: Metals and materials international - Sŏul : Inst., 1995, 18(2012), 2 vom: Apr., Seite 249-255
Übergeordnetes Werk:	volume:18 ; year:2012 ; number:2 ; month:04 ; pages:249-255

Links:	Volltext

DOI / URN:	10.1007/s12540-012-2008-4

Katalog-ID:	SPR026068699

Internformat


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520			\|a Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method.
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912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
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912			\|a GBV_ILN_2025
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912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
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Indexfelder

author_variant	r l rl d b db n k nk
matchkey_str	article:20054149:2012----::eprtrdpnetufcmrhlgadihudfuinie
hierarchy_sort_str	2012
publishDate	2012
allfields	10.1007/s12540-012-2008-4 doi (DE-627)SPR026068699 (SPR)s12540-012-2008-4-e DE-627 ger DE-627 rakwb eng 620 660 670 ASE Lakshmanan, R. verfasserin aut Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method. Bhuvaneswari, D. verfasserin aut Kalaiselvi, N. verfasserin aut Enthalten in Metals and materials international Sŏul : Inst., 1995 18(2012), 2 vom: Apr., Seite 249-255 (DE-627)60059405X (DE-600)2496162-0 2005-4149 nnns volume:18 year:2012 number:2 month:04 pages:249-255 https://dx.doi.org/10.1007/s12540-012-2008-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 18 2012 2 04 249-255
spelling	10.1007/s12540-012-2008-4 doi (DE-627)SPR026068699 (SPR)s12540-012-2008-4-e DE-627 ger DE-627 rakwb eng 620 660 670 ASE Lakshmanan, R. verfasserin aut Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method. Bhuvaneswari, D. verfasserin aut Kalaiselvi, N. verfasserin aut Enthalten in Metals and materials international Sŏul : Inst., 1995 18(2012), 2 vom: Apr., Seite 249-255 (DE-627)60059405X (DE-600)2496162-0 2005-4149 nnns volume:18 year:2012 number:2 month:04 pages:249-255 https://dx.doi.org/10.1007/s12540-012-2008-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 18 2012 2 04 249-255
allfields_unstemmed	10.1007/s12540-012-2008-4 doi (DE-627)SPR026068699 (SPR)s12540-012-2008-4-e DE-627 ger DE-627 rakwb eng 620 660 670 ASE Lakshmanan, R. verfasserin aut Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method. Bhuvaneswari, D. verfasserin aut Kalaiselvi, N. verfasserin aut Enthalten in Metals and materials international Sŏul : Inst., 1995 18(2012), 2 vom: Apr., Seite 249-255 (DE-627)60059405X (DE-600)2496162-0 2005-4149 nnns volume:18 year:2012 number:2 month:04 pages:249-255 https://dx.doi.org/10.1007/s12540-012-2008-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 18 2012 2 04 249-255
allfieldsGer	10.1007/s12540-012-2008-4 doi (DE-627)SPR026068699 (SPR)s12540-012-2008-4-e DE-627 ger DE-627 rakwb eng 620 660 670 ASE Lakshmanan, R. verfasserin aut Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method. Bhuvaneswari, D. verfasserin aut Kalaiselvi, N. verfasserin aut Enthalten in Metals and materials international Sŏul : Inst., 1995 18(2012), 2 vom: Apr., Seite 249-255 (DE-627)60059405X (DE-600)2496162-0 2005-4149 nnns volume:18 year:2012 number:2 month:04 pages:249-255 https://dx.doi.org/10.1007/s12540-012-2008-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 18 2012 2 04 249-255
allfieldsSound	10.1007/s12540-012-2008-4 doi (DE-627)SPR026068699 (SPR)s12540-012-2008-4-e DE-627 ger DE-627 rakwb eng 620 660 670 ASE Lakshmanan, R. verfasserin aut Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode 2012 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method. Bhuvaneswari, D. verfasserin aut Kalaiselvi, N. verfasserin aut Enthalten in Metals and materials international Sŏul : Inst., 1995 18(2012), 2 vom: Apr., Seite 249-255 (DE-627)60059405X (DE-600)2496162-0 2005-4149 nnns volume:18 year:2012 number:2 month:04 pages:249-255 https://dx.doi.org/10.1007/s12540-012-2008-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 18 2012 2 04 249-255
language	English
source	Enthalten in Metals and materials international 18(2012), 2 vom: Apr., Seite 249-255 volume:18 year:2012 number:2 month:04 pages:249-255
sourceStr	Enthalten in Metals and materials international 18(2012), 2 vom: Apr., Seite 249-255 volume:18 year:2012 number:2 month:04 pages:249-255
format_phy_str_mv	Article
institution	findex.gbv.de
dewey-raw	620
isfreeaccess_bool	false
container_title	Metals and materials international
authorswithroles_txt_mv	Lakshmanan, R. @@aut@@ Bhuvaneswari, D. @@aut@@ Kalaiselvi, N. @@aut@@
publishDateDaySort_date	2012-04-01T00:00:00Z
hierarchy_top_id	60059405X
dewey-sort	3620
id	SPR026068699
language_de	englisch
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author	Lakshmanan, R.
spellingShingle	Lakshmanan, R. ddc 620 Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode
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title	Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode
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title_full	Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode
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author_browse	Lakshmanan, R. Bhuvaneswari, D. Kalaiselvi, N.
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title_sort	temperature dependent surface morphology and lithium diffusion kinetics of $ licoo_{2} $ cathode
title_auth	Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode
abstract	Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method.
abstractGer	Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method.
abstract_unstemmed	Abstract In an attempt to understand the effect of synthesis temperature upon surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $, the compound was synthesized at four different temperatures, viz., 600, 700, 800 and 900 °C using a novel gelatin-assisted combustion method. $ LiCoO_{2} $ synthesized at 800 °C is found to be a mixture of rhombohedral and cubic $ LiCoO_{2} $ and a temperature of 900 °C leads to the formation of cubic $ LiCo_{2} %$ O_{4} $ compound, thus favoring lower temperatures such as 600 and 700 °C to prepare phase pure rhombohedral $ LiCoO_{2} $. Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. The study demonstrates the possibility and superiority of synthesizing electrochemically active $ LiCoO_{2} $ with preferred surface morphology and better lithium diffusion kinetics at a relatively lower temperature of 600 °C, using a gelatin-assisted combustion method.
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title_short	Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode
url	https://dx.doi.org/10.1007/s12540-012-2008-4
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up_date	2024-07-03T18:41:51.970Z
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Cyclic voltametry and impedance spectral studies evidence that $ LiCoO_{2} $ synthesized at 600 °C exhibits better electrochemical cycling behavior and considerably reduced internal resistance upon cycling, which are substantiated further from the higher lithium diffusion coefficient value. 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Temperature dependent surface morphology and lithium diffusion kinetics of $ LiCoO_{2} $ cathode

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