Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System

Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing...
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Autor*in:	Wei, W. Q. [verfasserIn] Wu, S. B.

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2016

Schlagwörter:	Eucalyptus cellulose InCl 5-Hydroxymethylfurfural Biphasic systems

Anmerkung:	© Springer Science+Business Media Dordrecht 2016

Übergeordnetes Werk:	Enthalten in: Waste and biomass valorization - [Dordrecht] : Springer Netherlands, 2010, 8(2016), 4 vom: 30. Aug., Seite 1303-1311
Übergeordnetes Werk:	volume:8 ; year:2016 ; number:4 ; day:30 ; month:08 ; pages:1303-1311

Links:	Volltext

DOI / URN:	10.1007/s12649-016-9676-0

Katalog-ID:	SPR026569078

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520			\|a Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process.
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matchkey_str	article:1877265X:2016----::ovrinfuaytsellsit5yrxmtyfruauigeiaict
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allfields	10.1007/s12649-016-9676-0 doi (DE-627)SPR026569078 (SPR)s12649-016-9676-0-e DE-627 ger DE-627 rakwb eng Wei, W. Q. verfasserin aut Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media Dordrecht 2016 Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. Eucalyptus cellulose (dpeaa)DE-He213 InCl (dpeaa)DE-He213 5-Hydroxymethylfurfural (dpeaa)DE-He213 Biphasic systems (dpeaa)DE-He213 Wu, S. B. aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 8(2016), 4 vom: 30. Aug., Seite 1303-1311 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311 https://dx.doi.org/10.1007/s12649-016-9676-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 8 2016 4 30 08 1303-1311
spelling	10.1007/s12649-016-9676-0 doi (DE-627)SPR026569078 (SPR)s12649-016-9676-0-e DE-627 ger DE-627 rakwb eng Wei, W. Q. verfasserin aut Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media Dordrecht 2016 Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. Eucalyptus cellulose (dpeaa)DE-He213 InCl (dpeaa)DE-He213 5-Hydroxymethylfurfural (dpeaa)DE-He213 Biphasic systems (dpeaa)DE-He213 Wu, S. B. aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 8(2016), 4 vom: 30. Aug., Seite 1303-1311 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311 https://dx.doi.org/10.1007/s12649-016-9676-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 8 2016 4 30 08 1303-1311
allfields_unstemmed	10.1007/s12649-016-9676-0 doi (DE-627)SPR026569078 (SPR)s12649-016-9676-0-e DE-627 ger DE-627 rakwb eng Wei, W. Q. verfasserin aut Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media Dordrecht 2016 Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. Eucalyptus cellulose (dpeaa)DE-He213 InCl (dpeaa)DE-He213 5-Hydroxymethylfurfural (dpeaa)DE-He213 Biphasic systems (dpeaa)DE-He213 Wu, S. B. aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 8(2016), 4 vom: 30. Aug., Seite 1303-1311 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311 https://dx.doi.org/10.1007/s12649-016-9676-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 8 2016 4 30 08 1303-1311
allfieldsGer	10.1007/s12649-016-9676-0 doi (DE-627)SPR026569078 (SPR)s12649-016-9676-0-e DE-627 ger DE-627 rakwb eng Wei, W. Q. verfasserin aut Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media Dordrecht 2016 Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. Eucalyptus cellulose (dpeaa)DE-He213 InCl (dpeaa)DE-He213 5-Hydroxymethylfurfural (dpeaa)DE-He213 Biphasic systems (dpeaa)DE-He213 Wu, S. B. aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 8(2016), 4 vom: 30. Aug., Seite 1303-1311 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311 https://dx.doi.org/10.1007/s12649-016-9676-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 8 2016 4 30 08 1303-1311
allfieldsSound	10.1007/s12649-016-9676-0 doi (DE-627)SPR026569078 (SPR)s12649-016-9676-0-e DE-627 ger DE-627 rakwb eng Wei, W. Q. verfasserin aut Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System 2016 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media Dordrecht 2016 Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. Eucalyptus cellulose (dpeaa)DE-He213 InCl (dpeaa)DE-He213 5-Hydroxymethylfurfural (dpeaa)DE-He213 Biphasic systems (dpeaa)DE-He213 Wu, S. B. aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 8(2016), 4 vom: 30. Aug., Seite 1303-1311 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311 https://dx.doi.org/10.1007/s12649-016-9676-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 8 2016 4 30 08 1303-1311
language	English
source	Enthalten in Waste and biomass valorization 8(2016), 4 vom: 30. Aug., Seite 1303-1311 volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311
sourceStr	Enthalten in Waste and biomass valorization 8(2016), 4 vom: 30. Aug., Seite 1303-1311 volume:8 year:2016 number:4 day:30 month:08 pages:1303-1311
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institution	findex.gbv.de
topic_facet	Eucalyptus cellulose InCl 5-Hydroxymethylfurfural Biphasic systems
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container_title	Waste and biomass valorization
authorswithroles_txt_mv	Wei, W. Q. @@aut@@ Wu, S. B. @@aut@@
publishDateDaySort_date	2016-08-30T00:00:00Z
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author	Wei, W. Q.
spellingShingle	Wei, W. Q. misc Eucalyptus cellulose misc InCl misc 5-Hydroxymethylfurfural misc Biphasic systems Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System
authorStr	Wei, W. Q.
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topic_title	Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System Eucalyptus cellulose (dpeaa)DE-He213 InCl (dpeaa)DE-He213 5-Hydroxymethylfurfural (dpeaa)DE-He213 Biphasic systems (dpeaa)DE-He213
topic	misc Eucalyptus cellulose misc InCl misc 5-Hydroxymethylfurfural misc Biphasic systems
topic_unstemmed	misc Eucalyptus cellulose misc InCl misc 5-Hydroxymethylfurfural misc Biphasic systems
topic_browse	misc Eucalyptus cellulose misc InCl misc 5-Hydroxymethylfurfural misc Biphasic systems
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title	Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System
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title_full	Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System
author_sort	Wei, W. Q.
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doi_str_mv	10.1007/s12649-016-9676-0
title_sort	conversion of eucalyptus cellulose into 5-hydroxymethylfurfural using lewis acid catalyst in biphasic solvent system
title_auth	Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System
abstract	Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. © Springer Science+Business Media Dordrecht 2016
abstractGer	Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. © Springer Science+Business Media Dordrecht 2016
abstract_unstemmed	Abstract Conversion of eucalyptus cellulose into 5-hydroxymethylfurfural (5-HMF) by using Lewis acid catalyst in biphasic system was investigated in this study. The results show that the tetrahydrofuran/water biphasic system was more conducive to convert the eucalyptus cellulose into 5-HMF comparing to the single aqueous system. $ InCl_{3} $, a water-compatible Lewis acid, has the best catalytic effect. The highest yield of 5-HMF from eucalyptus cellulose is up to 45.05 mol%, which is a slight higher than that from microcrystalline cellulose. It can be ascribed to the lower crystallinity of isolated eucalyptus cellulose. The optimum conditions for catalytic conversion of eucalyptus cellulose into 5-HMF are at 200 °C for 2 h with 10 % $ InCl_{3} $ dosage. Additionally, the effect of recycling the whole biphasic system which contains $ InCl_{3} $, NaCl, $ H_{2} $O and THF indicated that the 5-HMF yield was gradually decreased as the cycle times increased, the possible reason could be due to the loss of partial $ InCl_{3} $ catalyst during the separation and distillation process. © Springer Science+Business Media Dordrecht 2016
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container_issue	4
title_short	Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System
url	https://dx.doi.org/10.1007/s12649-016-9676-0
remote_bool	true
author2	Wu, S. B.
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doi_str	10.1007/s12649-016-9676-0
up_date	2024-07-03T21:34:52.641Z
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Conversion of Eucalyptus Cellulose into 5-Hydroxymethylfurfural Using Lewis Acid Catalyst in Biphasic Solvent System

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