Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations
Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Solikhin, Achmad [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2017 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media B.V. 2017 |
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| Übergeordnetes Werk: |
Enthalten in: Waste and biomass valorization - [Dordrecht] : Springer Netherlands, 2010, 10(2017), 2 vom: 31. Aug., Seite 275-286 |
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| Übergeordnetes Werk: |
volume:10 ; year:2017 ; number:2 ; day:31 ; month:08 ; pages:275-286 |
| Links: |
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| DOI / URN: |
10.1007/s12649-017-0066-z |
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| Katalog-ID: |
SPR026574837 |
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| 520 | |a Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. | ||
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| 650 | 4 | |a Steam explosion |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Chemo-mechanical stages |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Characterizations |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Oil palm empty fruit bunch |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Hadi, Yusuf Sudo |4 aut | |
| 700 | 1 | |a Massijaya, Muh Yusram |4 aut | |
| 700 | 1 | |a Nikmatin, Siti |4 aut | |
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10.1007/s12649-017-0066-z doi (DE-627)SPR026574837 (SPR)s12649-017-0066-z-e DE-627 ger DE-627 rakwb eng Solikhin, Achmad verfasserin aut Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media B.V. 2017 Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. Microfibrillated cellulose (MFC) (dpeaa)DE-He213 Steam explosion (dpeaa)DE-He213 Chemo-mechanical stages (dpeaa)DE-He213 Characterizations (dpeaa)DE-He213 Oil palm empty fruit bunch (dpeaa)DE-He213 Hadi, Yusuf Sudo aut Massijaya, Muh Yusram aut Nikmatin, Siti aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 10(2017), 2 vom: 31. Aug., Seite 275-286 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:10 year:2017 number:2 day:31 month:08 pages:275-286 https://dx.doi.org/10.1007/s12649-017-0066-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2017 2 31 08 275-286 |
| spelling |
10.1007/s12649-017-0066-z doi (DE-627)SPR026574837 (SPR)s12649-017-0066-z-e DE-627 ger DE-627 rakwb eng Solikhin, Achmad verfasserin aut Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media B.V. 2017 Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. Microfibrillated cellulose (MFC) (dpeaa)DE-He213 Steam explosion (dpeaa)DE-He213 Chemo-mechanical stages (dpeaa)DE-He213 Characterizations (dpeaa)DE-He213 Oil palm empty fruit bunch (dpeaa)DE-He213 Hadi, Yusuf Sudo aut Massijaya, Muh Yusram aut Nikmatin, Siti aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 10(2017), 2 vom: 31. Aug., Seite 275-286 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:10 year:2017 number:2 day:31 month:08 pages:275-286 https://dx.doi.org/10.1007/s12649-017-0066-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2017 2 31 08 275-286 |
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10.1007/s12649-017-0066-z doi (DE-627)SPR026574837 (SPR)s12649-017-0066-z-e DE-627 ger DE-627 rakwb eng Solikhin, Achmad verfasserin aut Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media B.V. 2017 Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. Microfibrillated cellulose (MFC) (dpeaa)DE-He213 Steam explosion (dpeaa)DE-He213 Chemo-mechanical stages (dpeaa)DE-He213 Characterizations (dpeaa)DE-He213 Oil palm empty fruit bunch (dpeaa)DE-He213 Hadi, Yusuf Sudo aut Massijaya, Muh Yusram aut Nikmatin, Siti aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 10(2017), 2 vom: 31. Aug., Seite 275-286 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:10 year:2017 number:2 day:31 month:08 pages:275-286 https://dx.doi.org/10.1007/s12649-017-0066-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2017 2 31 08 275-286 |
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10.1007/s12649-017-0066-z doi (DE-627)SPR026574837 (SPR)s12649-017-0066-z-e DE-627 ger DE-627 rakwb eng Solikhin, Achmad verfasserin aut Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media B.V. 2017 Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. Microfibrillated cellulose (MFC) (dpeaa)DE-He213 Steam explosion (dpeaa)DE-He213 Chemo-mechanical stages (dpeaa)DE-He213 Characterizations (dpeaa)DE-He213 Oil palm empty fruit bunch (dpeaa)DE-He213 Hadi, Yusuf Sudo aut Massijaya, Muh Yusram aut Nikmatin, Siti aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 10(2017), 2 vom: 31. Aug., Seite 275-286 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:10 year:2017 number:2 day:31 month:08 pages:275-286 https://dx.doi.org/10.1007/s12649-017-0066-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2017 2 31 08 275-286 |
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10.1007/s12649-017-0066-z doi (DE-627)SPR026574837 (SPR)s12649-017-0066-z-e DE-627 ger DE-627 rakwb eng Solikhin, Achmad verfasserin aut Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Springer Science+Business Media B.V. 2017 Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. Microfibrillated cellulose (MFC) (dpeaa)DE-He213 Steam explosion (dpeaa)DE-He213 Chemo-mechanical stages (dpeaa)DE-He213 Characterizations (dpeaa)DE-He213 Oil palm empty fruit bunch (dpeaa)DE-He213 Hadi, Yusuf Sudo aut Massijaya, Muh Yusram aut Nikmatin, Siti aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 10(2017), 2 vom: 31. Aug., Seite 275-286 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:10 year:2017 number:2 day:31 month:08 pages:275-286 https://dx.doi.org/10.1007/s12649-017-0066-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 10 2017 2 31 08 275-286 |
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Enthalten in Waste and biomass valorization 10(2017), 2 vom: 31. Aug., Seite 275-286 volume:10 year:2017 number:2 day:31 month:08 pages:275-286 |
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Solikhin, Achmad @@aut@@ Hadi, Yusuf Sudo @@aut@@ Massijaya, Muh Yusram @@aut@@ Nikmatin, Siti @@aut@@ |
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The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. 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Solikhin, Achmad |
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Solikhin, Achmad misc Microfibrillated cellulose (MFC) misc Steam explosion misc Chemo-mechanical stages misc Characterizations misc Oil palm empty fruit bunch Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations |
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Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations Microfibrillated cellulose (MFC) (dpeaa)DE-He213 Steam explosion (dpeaa)DE-He213 Chemo-mechanical stages (dpeaa)DE-He213 Characterizations (dpeaa)DE-He213 Oil palm empty fruit bunch (dpeaa)DE-He213 |
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Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations |
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Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations |
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production of microfibrillated cellulose by novel continuous steam explosion assisted chemo-mechanical methods and its characterizations |
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Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations |
| abstract |
Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. © Springer Science+Business Media B.V. 2017 |
| abstractGer |
Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. © Springer Science+Business Media B.V. 2017 |
| abstract_unstemmed |
Abstract In this study, microfibrillated cellulose (MFC) was successfully isolated with different time treatments of steam explosion, which were combined with chemo-mechanical stages. The objectives of this study were to isolate and characterize MFC obtained from steam explosion—assisted novel chemo-mechanical methods, and to investigate the effects of different steam explosion times on obtained MFC. Characterizations used were SEM, TEM, PSA, GC–MS, EDS, XRD, FTIR, and STA. The result of this study showed an optimal diameter range of MFC samples was between 23.45 and 77.65 nm at 1 h steam explosion time. However, MFC fibers were aggregated until its particle size distribution by number was about 645.83 nm. That lignocellulose MFC comprised C, N, and O with a dramatic decrease of Si. Most of the samples had many transmittance peaks, indicating the presence of cellulose with –OH, –$ CH_{2} $, C–H, and C–O functional groups whereas IR peaks designated to hemicellulose and lignin were almost absent. The presence of n-heptadecanol-1; n-nonadecanol-1; n-nonadecanol; hexadecanoic acid, ethyl ester; ethyl oleate; and octadecanoic acid, ethyl ester was linked with existance of cellulose and cementing agents (hemicellulose and lignin). There was an increase of cellulose crystallinity along with the increase in steam explosion time. Native cellulose or cellulose I was the initial nature of obtained MFC. The decrease of thermal stability of hemicellulose was correlated with acid treatment and acetyl groups, while the increase of cellulose thermal stability was in accordance with the increase of cellulose crystallinity index. © Springer Science+Business Media B.V. 2017 |
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| title_short |
Production of Microfibrillated Cellulose by Novel Continuous Steam Explosion Assisted Chemo-Mechanical Methods and Its Characterizations |
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https://dx.doi.org/10.1007/s12649-017-0066-z |
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Hadi, Yusuf Sudo Massijaya, Muh Yusram Nikmatin, Siti |
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Hadi, Yusuf Sudo Massijaya, Muh Yusram Nikmatin, Siti |
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| doi_str |
10.1007/s12649-017-0066-z |
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2024-07-03T21:37:19.483Z |
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| score |
7.3987513 |