Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application
Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragona...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ashok Kumar, K. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
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| Anmerkung: |
© The Indian Institute of Metals - IIM 2015 |
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| Übergeordnetes Werk: |
Enthalten in: Transactions of the Indian Institute of Metals - [New Delhi] : Springer India, 2008, 68(2015), Suppl 2 vom: 02. Juni, Seite 221-225 |
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| Übergeordnetes Werk: |
volume:68 ; year:2015 ; number:Suppl 2 ; day:02 ; month:06 ; pages:221-225 |
| Links: |
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| DOI / URN: |
10.1007/s12666-015-0563-3 |
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| Katalog-ID: |
SPR026930854 |
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| 245 | 1 | 0 | |a Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application |
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| 520 | |a Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. | ||
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| 650 | 4 | |a Impedance spectroscopy |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a DSSC |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Ramesh, D. |4 aut | |
| 700 | 1 | |a Gunaseelan, M. |4 aut | |
| 700 | 1 | |a Subalakshmi, K. |4 aut | |
| 700 | 1 | |a Senthilselvan, J. |4 aut | |
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10.1007/s12666-015-0563-3 doi (DE-627)SPR026930854 (SPR)s12666-015-0563-3-e DE-627 ger DE-627 rakwb eng Ashok Kumar, K. verfasserin aut Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Indian Institute of Metals - IIM 2015 Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. SnO (dpeaa)DE-He213 nanoparticles (dpeaa)DE-He213 Hydrothermal (dpeaa)DE-He213 Solvothermal (dpeaa)DE-He213 Impedance spectroscopy (dpeaa)DE-He213 DSSC (dpeaa)DE-He213 Ramesh, D. aut Gunaseelan, M. aut Subalakshmi, K. aut Senthilselvan, J. aut Enthalten in Transactions of the Indian Institute of Metals [New Delhi] : Springer India, 2008 68(2015), Suppl 2 vom: 02. Juni, Seite 221-225 (DE-627)617807884 (DE-600)2535335-4 0975-1645 nnns volume:68 year:2015 number:Suppl 2 day:02 month:06 pages:221-225 https://dx.doi.org/10.1007/s12666-015-0563-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 68 2015 Suppl 2 02 06 221-225 |
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10.1007/s12666-015-0563-3 doi (DE-627)SPR026930854 (SPR)s12666-015-0563-3-e DE-627 ger DE-627 rakwb eng Ashok Kumar, K. verfasserin aut Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Indian Institute of Metals - IIM 2015 Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. SnO (dpeaa)DE-He213 nanoparticles (dpeaa)DE-He213 Hydrothermal (dpeaa)DE-He213 Solvothermal (dpeaa)DE-He213 Impedance spectroscopy (dpeaa)DE-He213 DSSC (dpeaa)DE-He213 Ramesh, D. aut Gunaseelan, M. aut Subalakshmi, K. aut Senthilselvan, J. aut Enthalten in Transactions of the Indian Institute of Metals [New Delhi] : Springer India, 2008 68(2015), Suppl 2 vom: 02. Juni, Seite 221-225 (DE-627)617807884 (DE-600)2535335-4 0975-1645 nnns volume:68 year:2015 number:Suppl 2 day:02 month:06 pages:221-225 https://dx.doi.org/10.1007/s12666-015-0563-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 68 2015 Suppl 2 02 06 221-225 |
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10.1007/s12666-015-0563-3 doi (DE-627)SPR026930854 (SPR)s12666-015-0563-3-e DE-627 ger DE-627 rakwb eng Ashok Kumar, K. verfasserin aut Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Indian Institute of Metals - IIM 2015 Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. SnO (dpeaa)DE-He213 nanoparticles (dpeaa)DE-He213 Hydrothermal (dpeaa)DE-He213 Solvothermal (dpeaa)DE-He213 Impedance spectroscopy (dpeaa)DE-He213 DSSC (dpeaa)DE-He213 Ramesh, D. aut Gunaseelan, M. aut Subalakshmi, K. aut Senthilselvan, J. aut Enthalten in Transactions of the Indian Institute of Metals [New Delhi] : Springer India, 2008 68(2015), Suppl 2 vom: 02. Juni, Seite 221-225 (DE-627)617807884 (DE-600)2535335-4 0975-1645 nnns volume:68 year:2015 number:Suppl 2 day:02 month:06 pages:221-225 https://dx.doi.org/10.1007/s12666-015-0563-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 68 2015 Suppl 2 02 06 221-225 |
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10.1007/s12666-015-0563-3 doi (DE-627)SPR026930854 (SPR)s12666-015-0563-3-e DE-627 ger DE-627 rakwb eng Ashok Kumar, K. verfasserin aut Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Indian Institute of Metals - IIM 2015 Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. SnO (dpeaa)DE-He213 nanoparticles (dpeaa)DE-He213 Hydrothermal (dpeaa)DE-He213 Solvothermal (dpeaa)DE-He213 Impedance spectroscopy (dpeaa)DE-He213 DSSC (dpeaa)DE-He213 Ramesh, D. aut Gunaseelan, M. aut Subalakshmi, K. aut Senthilselvan, J. aut Enthalten in Transactions of the Indian Institute of Metals [New Delhi] : Springer India, 2008 68(2015), Suppl 2 vom: 02. Juni, Seite 221-225 (DE-627)617807884 (DE-600)2535335-4 0975-1645 nnns volume:68 year:2015 number:Suppl 2 day:02 month:06 pages:221-225 https://dx.doi.org/10.1007/s12666-015-0563-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 68 2015 Suppl 2 02 06 221-225 |
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10.1007/s12666-015-0563-3 doi (DE-627)SPR026930854 (SPR)s12666-015-0563-3-e DE-627 ger DE-627 rakwb eng Ashok Kumar, K. verfasserin aut Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application 2015 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Indian Institute of Metals - IIM 2015 Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. SnO (dpeaa)DE-He213 nanoparticles (dpeaa)DE-He213 Hydrothermal (dpeaa)DE-He213 Solvothermal (dpeaa)DE-He213 Impedance spectroscopy (dpeaa)DE-He213 DSSC (dpeaa)DE-He213 Ramesh, D. aut Gunaseelan, M. aut Subalakshmi, K. aut Senthilselvan, J. aut Enthalten in Transactions of the Indian Institute of Metals [New Delhi] : Springer India, 2008 68(2015), Suppl 2 vom: 02. Juni, Seite 221-225 (DE-627)617807884 (DE-600)2535335-4 0975-1645 nnns volume:68 year:2015 number:Suppl 2 day:02 month:06 pages:221-225 https://dx.doi.org/10.1007/s12666-015-0563-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 68 2015 Suppl 2 02 06 221-225 |
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Ashok Kumar, K. @@aut@@ Ramesh, D. @@aut@@ Gunaseelan, M. @@aut@@ Subalakshmi, K. @@aut@@ Senthilselvan, J. @@aut@@ |
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The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. 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Ashok Kumar, K. |
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Ashok Kumar, K. misc SnO misc nanoparticles misc Hydrothermal misc Solvothermal misc Impedance spectroscopy misc DSSC Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application |
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Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application SnO (dpeaa)DE-He213 nanoparticles (dpeaa)DE-He213 Hydrothermal (dpeaa)DE-He213 Solvothermal (dpeaa)DE-He213 Impedance spectroscopy (dpeaa)DE-He213 DSSC (dpeaa)DE-He213 |
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Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application |
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Ashok Kumar, K. Ramesh, D. Gunaseelan, M. Subalakshmi, K. Senthilselvan, J. |
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structural, optical and impedance studies of hydrothermally and solvothermally prepared $ sno_{2} $ nanocrystallites for conducting electrode application |
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Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application |
| abstract |
Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. © The Indian Institute of Metals - IIM 2015 |
| abstractGer |
Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. © The Indian Institute of Metals - IIM 2015 |
| abstract_unstemmed |
Abstract Nanocrystalline $ SnO_{2} $ powders were synthesized by hydrolysis and solvolysis of $ SnCl_{2} $ followed by a fast nucleation process in Teflon lined autoclave. The as prepared samples were calcined at 400 °C for 4 h to attain stable phase. The X-ray diffraction pattern confirms tetragonal crystal structure for both hydrothermally and solvothermally prepared nanoparticles and the average crystallite size is calculated to be 14 and 30 nm respectively. Williamson–Hall plot (W–H plot) reveals low value of strain induced broadening using uniform deformation model. Absorption co-efficient of prepared $ SnO_{2} $ was determined using UV–Visible absorption spectrum. Nyquist plane plot shows the decreased electrical resistance of $ SnO_{2} $ with increasing the applied potential resulting in increased conductivity. The increasing conducting behavior of tin oxide nanoparticles can be used as conducting layer in photoelectrodes. © The Indian Institute of Metals - IIM 2015 |
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Suppl 2 |
| title_short |
Structural, Optical and Impedance Studies of Hydrothermally and Solvothermally Prepared $ SnO_{2} $ Nanocrystallites for Conducting Electrode Application |
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https://dx.doi.org/10.1007/s12666-015-0563-3 |
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Ramesh, D. Gunaseelan, M. Subalakshmi, K. Senthilselvan, J. |
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| score |
7.3987417 |