Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS)

Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG lase...
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Autor*in:	Arab, M. [verfasserIn] Bidin, N. Rizvi, Z. H. Safie, S. Alsaedi, M. A.

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2014

Schlagwörter:	Heavy metal spectrometer LIBS LOD

Anmerkung:	© The Author(s) 2013. This article is published under license to BioMed Central Ltd.

Übergeordnetes Werk:	Enthalten in: Photonic sensors - Berlin : Springer, 2011, 4(2014), 1 vom: 03. Jan., Seite 63-69
Übergeordnetes Werk:	volume:4 ; year:2014 ; number:1 ; day:03 ; month:01 ; pages:63-69

Links:	Volltext

DOI / URN:	10.1007/s13320-013-0144-1

Katalog-ID:	SPR03133220X

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520			\|a Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail.
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allfields	10.1007/s13320-013-0144-1 doi (DE-627)SPR03133220X (SPR)s13320-013-0144-1-e DE-627 ger DE-627 rakwb eng Arab, M. verfasserin aut Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS) 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s) 2013. This article is published under license to BioMed Central Ltd. Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. Heavy metal (dpeaa)DE-He213 spectrometer (dpeaa)DE-He213 LIBS (dpeaa)DE-He213 LOD (dpeaa)DE-He213 Bidin, N. aut Rizvi, Z. H. aut Safie, S. aut Alsaedi, M. A. aut Enthalten in Photonic sensors Berlin : Springer, 2011 4(2014), 1 vom: 03. Jan., Seite 63-69 (DE-627)638064023 (DE-600)2577939-4 2190-7439 nnns volume:4 year:2014 number:1 day:03 month:01 pages:63-69 https://dx.doi.org/10.1007/s13320-013-0144-1 kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 4 2014 1 03 01 63-69
spelling	10.1007/s13320-013-0144-1 doi (DE-627)SPR03133220X (SPR)s13320-013-0144-1-e DE-627 ger DE-627 rakwb eng Arab, M. verfasserin aut Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS) 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s) 2013. This article is published under license to BioMed Central Ltd. Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. Heavy metal (dpeaa)DE-He213 spectrometer (dpeaa)DE-He213 LIBS (dpeaa)DE-He213 LOD (dpeaa)DE-He213 Bidin, N. aut Rizvi, Z. H. aut Safie, S. aut Alsaedi, M. A. aut Enthalten in Photonic sensors Berlin : Springer, 2011 4(2014), 1 vom: 03. Jan., Seite 63-69 (DE-627)638064023 (DE-600)2577939-4 2190-7439 nnns volume:4 year:2014 number:1 day:03 month:01 pages:63-69 https://dx.doi.org/10.1007/s13320-013-0144-1 kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 4 2014 1 03 01 63-69
allfields_unstemmed	10.1007/s13320-013-0144-1 doi (DE-627)SPR03133220X (SPR)s13320-013-0144-1-e DE-627 ger DE-627 rakwb eng Arab, M. verfasserin aut Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS) 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s) 2013. This article is published under license to BioMed Central Ltd. Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. Heavy metal (dpeaa)DE-He213 spectrometer (dpeaa)DE-He213 LIBS (dpeaa)DE-He213 LOD (dpeaa)DE-He213 Bidin, N. aut Rizvi, Z. H. aut Safie, S. aut Alsaedi, M. A. aut Enthalten in Photonic sensors Berlin : Springer, 2011 4(2014), 1 vom: 03. Jan., Seite 63-69 (DE-627)638064023 (DE-600)2577939-4 2190-7439 nnns volume:4 year:2014 number:1 day:03 month:01 pages:63-69 https://dx.doi.org/10.1007/s13320-013-0144-1 kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 4 2014 1 03 01 63-69
allfieldsGer	10.1007/s13320-013-0144-1 doi (DE-627)SPR03133220X (SPR)s13320-013-0144-1-e DE-627 ger DE-627 rakwb eng Arab, M. verfasserin aut Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS) 2014 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s) 2013. This article is published under license to BioMed Central Ltd. Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. Heavy metal (dpeaa)DE-He213 spectrometer (dpeaa)DE-He213 LIBS (dpeaa)DE-He213 LOD (dpeaa)DE-He213 Bidin, N. aut Rizvi, Z. H. aut Safie, S. aut Alsaedi, M. A. aut Enthalten in Photonic sensors Berlin : Springer, 2011 4(2014), 1 vom: 03. Jan., Seite 63-69 (DE-627)638064023 (DE-600)2577939-4 2190-7439 nnns volume:4 year:2014 number:1 day:03 month:01 pages:63-69 https://dx.doi.org/10.1007/s13320-013-0144-1 kostenfrei Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 4 2014 1 03 01 63-69
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author	Arab, M.
spellingShingle	Arab, M. misc Heavy metal misc spectrometer misc LIBS misc LOD Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS)
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topic_title	Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS) Heavy metal (dpeaa)DE-He213 spectrometer (dpeaa)DE-He213 LIBS (dpeaa)DE-He213 LOD (dpeaa)DE-He213
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topic_unstemmed	misc Heavy metal misc spectrometer misc LIBS misc LOD
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title	Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS)
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title_full	Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS)
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author_browse	Arab, M. Bidin, N. Rizvi, Z. H. Safie, S. Alsaedi, M. A.
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title_sort	comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (libs)
title_auth	Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS)
abstract	Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. © The Author(s) 2013. This article is published under license to BioMed Central Ltd.
abstractGer	Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. © The Author(s) 2013. This article is published under license to BioMed Central Ltd.
abstract_unstemmed	Abstract The purpose of this paper is to compare the performance of two spectrometers that are manufactured from the same company. In this work, heavy metals like lead Pb and copper Cu in the KBr matrix were analyzed using the laser induced breakdown spectroscopic technique. A Q-switched Nd:YAG laser with 90 mJ per pulse operating at the fundamental wavelength of 1064 nm and pulse duration of 10 ns was used to generate plasma at the focal region. The important experimental parameters such as the laser energy, integration time, distance between the lens and sample, distance and angle of the optical fiber from the target were optimized. Two spectrometers manufactured by Ocean Optics namely as Maya2000Pro and USB 4000 were employed for anlyzing the spectral lines. The experimental setup and conditions were remained the same for both experiments. The production of spectral lines from each of the interested elements was analyzed and compared with the NIST (National Institute of Standards and Technology) database. The sensitivity, repeatability and limit of detection for each of the systems are discussed in detail. © The Author(s) 2013. This article is published under license to BioMed Central Ltd.
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title_short	Comparison study of two commercial spectrometers for heavy metal analysis of laser induced breakdown spectroscopy (LIBS)
url	https://dx.doi.org/10.1007/s13320-013-0144-1
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