Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy
Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared i...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Lee, Jeong Woo [verfasserIn] Lee, Byoung Wan [verfasserIn] Yeon, Yeung Kyu [verfasserIn] Lee, Ok Joo [verfasserIn] Park, Chan Hum [verfasserIn] Park, Jaehoon [verfasserIn] Ko, Jae-Hyeon [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2017 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of the Korean Physical Society - Berlin : Springer, 1968, 71(2017), 3 vom: Aug., Seite 144-149 |
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| Übergeordnetes Werk: |
volume:71 ; year:2017 ; number:3 ; month:08 ; pages:144-149 |
| Links: |
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| DOI / URN: |
10.3938/jkps.71.144 |
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| Katalog-ID: |
SPR032732155 |
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| 520 | |a Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. | ||
| 650 | 4 | |a Silk fibroin |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Water effect |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Brillouin scattering |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Elastic |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Lee, Byoung Wan |e verfasserin |4 aut | |
| 700 | 1 | |a Yeon, Yeung Kyu |e verfasserin |4 aut | |
| 700 | 1 | |a Lee, Ok Joo |e verfasserin |4 aut | |
| 700 | 1 | |a Park, Chan Hum |e verfasserin |4 aut | |
| 700 | 1 | |a Park, Jaehoon |e verfasserin |4 aut | |
| 700 | 1 | |a Ko, Jae-Hyeon |e verfasserin |4 aut | |
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10.3938/jkps.71.144 doi (DE-627)SPR032732155 (SPR)jkps.71.144-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Lee, Jeong Woo verfasserin aut Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. Silk fibroin (dpeaa)DE-He213 Water effect (dpeaa)DE-He213 Brillouin scattering (dpeaa)DE-He213 Elastic (dpeaa)DE-He213 Lee, Byoung Wan verfasserin aut Yeon, Yeung Kyu verfasserin aut Lee, Ok Joo verfasserin aut Park, Chan Hum verfasserin aut Park, Jaehoon verfasserin aut Ko, Jae-Hyeon verfasserin aut Enthalten in Journal of the Korean Physical Society Berlin : Springer, 1968 71(2017), 3 vom: Aug., Seite 144-149 (DE-627)328820865 (DE-600)2046361-3 1976-8524 nnns volume:71 year:2017 number:3 month:08 pages:144-149 https://dx.doi.org/10.3938/jkps.71.144 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.00 ASE AR 71 2017 3 08 144-149 |
| spelling |
10.3938/jkps.71.144 doi (DE-627)SPR032732155 (SPR)jkps.71.144-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Lee, Jeong Woo verfasserin aut Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. Silk fibroin (dpeaa)DE-He213 Water effect (dpeaa)DE-He213 Brillouin scattering (dpeaa)DE-He213 Elastic (dpeaa)DE-He213 Lee, Byoung Wan verfasserin aut Yeon, Yeung Kyu verfasserin aut Lee, Ok Joo verfasserin aut Park, Chan Hum verfasserin aut Park, Jaehoon verfasserin aut Ko, Jae-Hyeon verfasserin aut Enthalten in Journal of the Korean Physical Society Berlin : Springer, 1968 71(2017), 3 vom: Aug., Seite 144-149 (DE-627)328820865 (DE-600)2046361-3 1976-8524 nnns volume:71 year:2017 number:3 month:08 pages:144-149 https://dx.doi.org/10.3938/jkps.71.144 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.00 ASE AR 71 2017 3 08 144-149 |
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10.3938/jkps.71.144 doi (DE-627)SPR032732155 (SPR)jkps.71.144-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Lee, Jeong Woo verfasserin aut Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. Silk fibroin (dpeaa)DE-He213 Water effect (dpeaa)DE-He213 Brillouin scattering (dpeaa)DE-He213 Elastic (dpeaa)DE-He213 Lee, Byoung Wan verfasserin aut Yeon, Yeung Kyu verfasserin aut Lee, Ok Joo verfasserin aut Park, Chan Hum verfasserin aut Park, Jaehoon verfasserin aut Ko, Jae-Hyeon verfasserin aut Enthalten in Journal of the Korean Physical Society Berlin : Springer, 1968 71(2017), 3 vom: Aug., Seite 144-149 (DE-627)328820865 (DE-600)2046361-3 1976-8524 nnns volume:71 year:2017 number:3 month:08 pages:144-149 https://dx.doi.org/10.3938/jkps.71.144 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.00 ASE AR 71 2017 3 08 144-149 |
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10.3938/jkps.71.144 doi (DE-627)SPR032732155 (SPR)jkps.71.144-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Lee, Jeong Woo verfasserin aut Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. Silk fibroin (dpeaa)DE-He213 Water effect (dpeaa)DE-He213 Brillouin scattering (dpeaa)DE-He213 Elastic (dpeaa)DE-He213 Lee, Byoung Wan verfasserin aut Yeon, Yeung Kyu verfasserin aut Lee, Ok Joo verfasserin aut Park, Chan Hum verfasserin aut Park, Jaehoon verfasserin aut Ko, Jae-Hyeon verfasserin aut Enthalten in Journal of the Korean Physical Society Berlin : Springer, 1968 71(2017), 3 vom: Aug., Seite 144-149 (DE-627)328820865 (DE-600)2046361-3 1976-8524 nnns volume:71 year:2017 number:3 month:08 pages:144-149 https://dx.doi.org/10.3938/jkps.71.144 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.00 ASE AR 71 2017 3 08 144-149 |
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10.3938/jkps.71.144 doi (DE-627)SPR032732155 (SPR)jkps.71.144-e DE-627 ger DE-627 rakwb eng 530 ASE 33.00 bkl Lee, Jeong Woo verfasserin aut Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. Silk fibroin (dpeaa)DE-He213 Water effect (dpeaa)DE-He213 Brillouin scattering (dpeaa)DE-He213 Elastic (dpeaa)DE-He213 Lee, Byoung Wan verfasserin aut Yeon, Yeung Kyu verfasserin aut Lee, Ok Joo verfasserin aut Park, Chan Hum verfasserin aut Park, Jaehoon verfasserin aut Ko, Jae-Hyeon verfasserin aut Enthalten in Journal of the Korean Physical Society Berlin : Springer, 1968 71(2017), 3 vom: Aug., Seite 144-149 (DE-627)328820865 (DE-600)2046361-3 1976-8524 nnns volume:71 year:2017 number:3 month:08 pages:144-149 https://dx.doi.org/10.3938/jkps.71.144 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2070 GBV_ILN_2086 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2116 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.00 ASE AR 71 2017 3 08 144-149 |
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Enthalten in Journal of the Korean Physical Society 71(2017), 3 vom: Aug., Seite 144-149 volume:71 year:2017 number:3 month:08 pages:144-149 |
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Journal of the Korean Physical Society |
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Lee, Jeong Woo @@aut@@ Lee, Byoung Wan @@aut@@ Yeon, Yeung Kyu @@aut@@ Lee, Ok Joo @@aut@@ Park, Chan Hum @@aut@@ Park, Jaehoon @@aut@@ Ko, Jae-Hyeon @@aut@@ |
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| author |
Lee, Jeong Woo |
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Lee, Jeong Woo ddc 530 bkl 33.00 misc Silk fibroin misc Water effect misc Brillouin scattering misc Elastic Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy |
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530 ASE 33.00 bkl Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy Silk fibroin (dpeaa)DE-He213 Water effect (dpeaa)DE-He213 Brillouin scattering (dpeaa)DE-He213 Elastic (dpeaa)DE-He213 |
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ddc 530 bkl 33.00 misc Silk fibroin misc Water effect misc Brillouin scattering misc Elastic |
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Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy |
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Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy |
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Lee, Jeong Woo |
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Journal of the Korean Physical Society |
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Lee, Jeong Woo Lee, Byoung Wan Yeon, Yeung Kyu Lee, Ok Joo Park, Chan Hum Park, Jaehoon Ko, Jae-Hyeon |
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effect of crystallinity on acoustic behaviors of biocompatible silk studied by brillouin spectroscopy |
| title_auth |
Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy |
| abstract |
Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. |
| abstractGer |
Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. |
| abstract_unstemmed |
Abstract Temperature dependences of thermal, thermogravimetric, and acoustic properties were investigated for the crystalline silk fibroin films crystallized by methanol exposure. The crystallization peak in the thermal flow at ~ 225 ◦ C, which was prominent in the amorphous silk film, disappeared in the crystalline silk film. The heat-treatment at ~ 100 ◦ C for 1 h reduced the weight by ~5.5% due to the release of water molecules. The formation of beta-sheets in the film did not have any substantial effect on the acoustic properties of the longitudinal acoustic mode in the crystalline film. However, the heat treatment of the methanol-exposed silk film induced clear anomalies in the acoustic mode behaviors in a specific temperature range between −20 ~ 30 ◦ C. The existence of water molecules has more profound effect than the crystallinity does on the acoustic properties of silk fibroin films. |
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Effect of crystallinity on acoustic behaviors of biocompatible silk studied by Brillouin spectroscopy |
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https://dx.doi.org/10.3938/jkps.71.144 |
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Lee, Byoung Wan Yeon, Yeung Kyu Lee, Ok Joo Park, Chan Hum Park, Jaehoon Ko, Jae-Hyeon |
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Lee, Byoung Wan Yeon, Yeung Kyu Lee, Ok Joo Park, Chan Hum Park, Jaehoon Ko, Jae-Hyeon |
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10.3938/jkps.71.144 |
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2024-07-03T14:28:17.072Z |
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|
| score |
7.4012003 |