Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method
Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and...
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Gespeichert in:
| Autor*in: |
Sanatombi, S. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2017 |
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| Schlagwörter: |
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| Anmerkung: |
© Shiraz University 2017 |
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| Übergeordnetes Werk: |
Enthalten in: Iranian journal of science and technology - Cham, Switzerland : Springer International Pubishing, 2004, 42(2017), 4 vom: 19. Dez., Seite 2397-2406 |
|---|---|
| Übergeordnetes Werk: |
volume:42 ; year:2017 ; number:4 ; day:19 ; month:12 ; pages:2397-2406 |
| Links: |
|---|
| DOI / URN: |
10.1007/s40995-017-0405-8 |
|---|
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SPR038039400 |
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| 520 | |a Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. | ||
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10.1007/s40995-017-0405-8 doi (DE-627)SPR038039400 (SPR)s40995-017-0405-8-e DE-627 ger DE-627 rakwb eng Sanatombi, S. verfasserin aut Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Shiraz University 2017 Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. Ferrites (dpeaa)DE-He213 Sintering (dpeaa)DE-He213 Structural parameters (dpeaa)DE-He213 Electrical parameters and magnetic parameters (dpeaa)DE-He213 Sumitra, S. aut Ibetombi, S. aut Enthalten in Iranian journal of science and technology Cham, Switzerland : Springer International Pubishing, 2004 42(2017), 4 vom: 19. Dez., Seite 2397-2406 (DE-627)SPR038034816 (DE-600)2843077-3 2364-1819 nnns volume:42 year:2017 number:4 day:19 month:12 pages:2397-2406 https://dx.doi.org/10.1007/s40995-017-0405-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER AR 42 2017 4 19 12 2397-2406 |
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10.1007/s40995-017-0405-8 doi (DE-627)SPR038039400 (SPR)s40995-017-0405-8-e DE-627 ger DE-627 rakwb eng Sanatombi, S. verfasserin aut Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Shiraz University 2017 Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. Ferrites (dpeaa)DE-He213 Sintering (dpeaa)DE-He213 Structural parameters (dpeaa)DE-He213 Electrical parameters and magnetic parameters (dpeaa)DE-He213 Sumitra, S. aut Ibetombi, S. aut Enthalten in Iranian journal of science and technology Cham, Switzerland : Springer International Pubishing, 2004 42(2017), 4 vom: 19. Dez., Seite 2397-2406 (DE-627)SPR038034816 (DE-600)2843077-3 2364-1819 nnns volume:42 year:2017 number:4 day:19 month:12 pages:2397-2406 https://dx.doi.org/10.1007/s40995-017-0405-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER AR 42 2017 4 19 12 2397-2406 |
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10.1007/s40995-017-0405-8 doi (DE-627)SPR038039400 (SPR)s40995-017-0405-8-e DE-627 ger DE-627 rakwb eng Sanatombi, S. verfasserin aut Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Shiraz University 2017 Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. Ferrites (dpeaa)DE-He213 Sintering (dpeaa)DE-He213 Structural parameters (dpeaa)DE-He213 Electrical parameters and magnetic parameters (dpeaa)DE-He213 Sumitra, S. aut Ibetombi, S. aut Enthalten in Iranian journal of science and technology Cham, Switzerland : Springer International Pubishing, 2004 42(2017), 4 vom: 19. Dez., Seite 2397-2406 (DE-627)SPR038034816 (DE-600)2843077-3 2364-1819 nnns volume:42 year:2017 number:4 day:19 month:12 pages:2397-2406 https://dx.doi.org/10.1007/s40995-017-0405-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER AR 42 2017 4 19 12 2397-2406 |
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10.1007/s40995-017-0405-8 doi (DE-627)SPR038039400 (SPR)s40995-017-0405-8-e DE-627 ger DE-627 rakwb eng Sanatombi, S. verfasserin aut Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Shiraz University 2017 Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. Ferrites (dpeaa)DE-He213 Sintering (dpeaa)DE-He213 Structural parameters (dpeaa)DE-He213 Electrical parameters and magnetic parameters (dpeaa)DE-He213 Sumitra, S. aut Ibetombi, S. aut Enthalten in Iranian journal of science and technology Cham, Switzerland : Springer International Pubishing, 2004 42(2017), 4 vom: 19. Dez., Seite 2397-2406 (DE-627)SPR038034816 (DE-600)2843077-3 2364-1819 nnns volume:42 year:2017 number:4 day:19 month:12 pages:2397-2406 https://dx.doi.org/10.1007/s40995-017-0405-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER AR 42 2017 4 19 12 2397-2406 |
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10.1007/s40995-017-0405-8 doi (DE-627)SPR038039400 (SPR)s40995-017-0405-8-e DE-627 ger DE-627 rakwb eng Sanatombi, S. verfasserin aut Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method 2017 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Shiraz University 2017 Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. Ferrites (dpeaa)DE-He213 Sintering (dpeaa)DE-He213 Structural parameters (dpeaa)DE-He213 Electrical parameters and magnetic parameters (dpeaa)DE-He213 Sumitra, S. aut Ibetombi, S. aut Enthalten in Iranian journal of science and technology Cham, Switzerland : Springer International Pubishing, 2004 42(2017), 4 vom: 19. Dez., Seite 2397-2406 (DE-627)SPR038034816 (DE-600)2843077-3 2364-1819 nnns volume:42 year:2017 number:4 day:19 month:12 pages:2397-2406 https://dx.doi.org/10.1007/s40995-017-0405-8 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER AR 42 2017 4 19 12 2397-2406 |
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Sanatombi, S. Sumitra, S. Ibetombi, S. |
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42 |
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Elektronische Aufsätze |
| author-letter |
Sanatombi, S. |
| doi_str_mv |
10.1007/s40995-017-0405-8 |
| title_sort |
influence of sintering on the structural, electrical, and magnetic properties of li–ni–mn–zn ferrite synthesized by citrate precursor method |
| title_auth |
Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method |
| abstract |
Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. © Shiraz University 2017 |
| abstractGer |
Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. © Shiraz University 2017 |
| abstract_unstemmed |
Abstract Substituted lithium ferrites having the compositional formula $ Li_{0.35−0.5x} $ $ Ni_{x} $ $ Mn_{0.1} $ $ Zn_{0.2} $ $ Fe_{2.35−0.5x} $ $ O_{4} $ where 0.1 ≤ x ≤ 0.3 in steps of 0.05 had been synthesized by the citrate precursor method. The samples were given single sintering at 900 °C and double sintering, second sintering at 900 °C after a pre-sintering or first sintering at 600 °C. Spinel phase structure was confirmed from FTIR spectra and XRD patterns. A study on the structural parameters (lattice constant, density, porosity and crystallize size), electrical parameters (dielectric constant %$ \varepsilon^{'} %$, dielectric loss tangent %$ tan\delta %$, dc resistivity ρdc), and magnetic parameter (initial permeability %$ \mu_{i}^{'} %$) of single-sintered (SS) and double-sintered (DS) Li–Ni–Mn–Zn ferrite samples has been investigated. Structural studies reveal that DS samples enhance density and reduce porosity. Electrical studies showed lower value of dielectric constant, and dielectric losses while higher dc resistivity is observed in DS samples. However, in both series, an anomalous high increase in dielectric constant for x = 0.15 is observed. It was found from magnetic studies that the initial permeability is lower in the DS samples. The mechanism that involves in the results obtain above is being discussed. © Shiraz University 2017 |
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| title_short |
Influence of Sintering on the Structural, Electrical, and Magnetic Properties of Li–Ni–Mn–Zn Ferrite Synthesized by Citrate Precursor Method |
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