In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA

Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffra...
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Autor*in:	Manju, P. [verfasserIn] Krishnan, P. Santhana Gopala Nayak, S. K.

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2020

Schlagwörter:	In-situ polymerization Sepiolite Hydrogen bonding Bionanocomposites

Anmerkung:	© The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Übergeordnetes Werk:	Enthalten in: Journal of polymer research - Dordrecht : Springer Science + Business Media B.V., 1994, 27(2020), 5 vom: Mai
Übergeordnetes Werk:	volume:27 ; year:2020 ; number:5 ; month:05

Links:	Volltext

DOI / URN:	10.1007/s10965-020-02098-1

Katalog-ID:	SPR039616134

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520			\|a Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively.
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650		4	\|a Bionanocomposites \|7 (dpeaa)DE-He213
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allfields	10.1007/s10965-020-02098-1 doi (DE-627)SPR039616134 (SPR)s10965-020-02098-1-e DE-627 ger DE-627 rakwb eng Manju, P. verfasserin aut In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. In-situ polymerization (dpeaa)DE-He213 Sepiolite (dpeaa)DE-He213 Hydrogen bonding (dpeaa)DE-He213 Bionanocomposites (dpeaa)DE-He213 Krishnan, P. Santhana Gopala (orcid)0000-0001-6556-0007 aut Nayak, S. K. aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 27(2020), 5 vom: Mai (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:27 year:2020 number:5 month:05 https://dx.doi.org/10.1007/s10965-020-02098-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 27 2020 5 05
spelling	10.1007/s10965-020-02098-1 doi (DE-627)SPR039616134 (SPR)s10965-020-02098-1-e DE-627 ger DE-627 rakwb eng Manju, P. verfasserin aut In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. In-situ polymerization (dpeaa)DE-He213 Sepiolite (dpeaa)DE-He213 Hydrogen bonding (dpeaa)DE-He213 Bionanocomposites (dpeaa)DE-He213 Krishnan, P. Santhana Gopala (orcid)0000-0001-6556-0007 aut Nayak, S. K. aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 27(2020), 5 vom: Mai (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:27 year:2020 number:5 month:05 https://dx.doi.org/10.1007/s10965-020-02098-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 27 2020 5 05
allfields_unstemmed	10.1007/s10965-020-02098-1 doi (DE-627)SPR039616134 (SPR)s10965-020-02098-1-e DE-627 ger DE-627 rakwb eng Manju, P. verfasserin aut In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. In-situ polymerization (dpeaa)DE-He213 Sepiolite (dpeaa)DE-He213 Hydrogen bonding (dpeaa)DE-He213 Bionanocomposites (dpeaa)DE-He213 Krishnan, P. Santhana Gopala (orcid)0000-0001-6556-0007 aut Nayak, S. K. aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 27(2020), 5 vom: Mai (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:27 year:2020 number:5 month:05 https://dx.doi.org/10.1007/s10965-020-02098-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 27 2020 5 05
allfieldsGer	10.1007/s10965-020-02098-1 doi (DE-627)SPR039616134 (SPR)s10965-020-02098-1-e DE-627 ger DE-627 rakwb eng Manju, P. verfasserin aut In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. In-situ polymerization (dpeaa)DE-He213 Sepiolite (dpeaa)DE-He213 Hydrogen bonding (dpeaa)DE-He213 Bionanocomposites (dpeaa)DE-He213 Krishnan, P. Santhana Gopala (orcid)0000-0001-6556-0007 aut Nayak, S. K. aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 27(2020), 5 vom: Mai (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:27 year:2020 number:5 month:05 https://dx.doi.org/10.1007/s10965-020-02098-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 27 2020 5 05
allfieldsSound	10.1007/s10965-020-02098-1 doi (DE-627)SPR039616134 (SPR)s10965-020-02098-1-e DE-627 ger DE-627 rakwb eng Manju, P. verfasserin aut In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. In-situ polymerization (dpeaa)DE-He213 Sepiolite (dpeaa)DE-He213 Hydrogen bonding (dpeaa)DE-He213 Bionanocomposites (dpeaa)DE-He213 Krishnan, P. Santhana Gopala (orcid)0000-0001-6556-0007 aut Nayak, S. K. aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 27(2020), 5 vom: Mai (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:27 year:2020 number:5 month:05 https://dx.doi.org/10.1007/s10965-020-02098-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 27 2020 5 05
language	English
source	Enthalten in Journal of polymer research 27(2020), 5 vom: Mai volume:27 year:2020 number:5 month:05
sourceStr	Enthalten in Journal of polymer research 27(2020), 5 vom: Mai volume:27 year:2020 number:5 month:05
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	In-situ polymerization Sepiolite Hydrogen bonding Bionanocomposites
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container_title	Journal of polymer research
authorswithroles_txt_mv	Manju, P. @@aut@@ Krishnan, P. Santhana Gopala @@aut@@ Nayak, S. K. @@aut@@
publishDateDaySort_date	2020-05-01T00:00:00Z
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Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). 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author	Manju, P.
spellingShingle	Manju, P. misc In-situ polymerization misc Sepiolite misc Hydrogen bonding misc Bionanocomposites In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA
authorStr	Manju, P.
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topic_title	In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA In-situ polymerization (dpeaa)DE-He213 Sepiolite (dpeaa)DE-He213 Hydrogen bonding (dpeaa)DE-He213 Bionanocomposites (dpeaa)DE-He213
topic	misc In-situ polymerization misc Sepiolite misc Hydrogen bonding misc Bionanocomposites
topic_unstemmed	misc In-situ polymerization misc Sepiolite misc Hydrogen bonding misc Bionanocomposites
topic_browse	misc In-situ polymerization misc Sepiolite misc Hydrogen bonding misc Bionanocomposites
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title	In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA
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title_full	In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA
author_sort	Manju, P.
journal	Journal of polymer research
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author_browse	Manju, P. Krishnan, P. Santhana Gopala Nayak, S. K.
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author-letter	Manju, P.
doi_str_mv	10.1007/s10965-020-02098-1
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title_sort	in-situ polymerised pla-sep bionanocomposites: effect of silanol groups on the properties of pla
title_auth	In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA
abstract	Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstractGer	Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstract_unstemmed	Abstract Poly(lactic acid)-Sepiolite bionanocomposites (PLA-SEP BNCs) with different weight percentages of SEP starting from 1 to 7 wt.% were synthesized by following in-situ polymerization technique. BNCs were characterized by fourier transform infrared spectroscopy (FT-IR), wide angle x-ray diffraction (WAXD), 29Si-nuclear magnetic resonance spectroscopy analysis (29Si-NMR). FT-IR studies indicated the existence of hydrogen bonding between SEP and PLA whereas WAXD analysis indicated the formation of BNCs. 29Si-NMR analysis supported existence of hydrogen bonding between SEP and PLA. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed that there was no significant agglomeration of SEP in BNCs. Upon incorporation of SEP, melting point of PLA increased. Melting point of PLA and SP7 indicated the formation of β- and α- crystals respectively. © The Polymer Society, Taipei 2020. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
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container_issue	5
title_short	In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA
url	https://dx.doi.org/10.1007/s10965-020-02098-1
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author2	Krishnan, P. Santhana Gopala Nayak, S. K.
author2Str	Krishnan, P. Santhana Gopala Nayak, S. K.
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doi_str	10.1007/s10965-020-02098-1
up_date	2024-07-04T00:45:49.901Z
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In-situ polymerised PLA-SEP bionanocomposites: effect of silanol groups on the properties of PLA

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