Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage
Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second pha...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Silva, E. C. [verfasserIn] da Costa, J. C. M. [verfasserIn] Nascimento, M. C. [verfasserIn] Pereira, B. L. [verfasserIn] Passos, R. R. [verfasserIn] Pocrifka, L. A. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of solid state electrochemistry - Berlin : Springer, 1997, 24(2020), 8 vom: 07. Mai, Seite 1961-1968 |
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| Übergeordnetes Werk: |
volume:24 ; year:2020 ; number:8 ; day:07 ; month:05 ; pages:1961-1968 |
| Links: |
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| DOI / URN: |
10.1007/s10008-020-04616-z |
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| Katalog-ID: |
SPR040251330 |
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| 245 | 1 | 0 | |a Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage |
| 264 | 1 | |c 2020 | |
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| 520 | |a Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. | ||
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| 700 | 1 | |a da Costa, J. C. M. |e verfasserin |4 aut | |
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| 700 | 1 | |a Pereira, B. L. |e verfasserin |4 aut | |
| 700 | 1 | |a Passos, R. R. |e verfasserin |4 aut | |
| 700 | 1 | |a Pocrifka, L. A. |e verfasserin |4 aut | |
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10.1007/s10008-020-04616-z doi (DE-627)SPR040251330 (SPR)s10008-020-04616-z-e DE-627 ger DE-627 rakwb eng 540 ASE 35.14 bkl 35.90 bkl Silva, E. C. verfasserin aut Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. Ferrites (dpeaa)DE-He213 Energy storage (dpeaa)DE-He213 Stable structure (dpeaa)DE-He213 Pseudocapacitors (dpeaa)DE-He213 da Costa, J. C. M. verfasserin aut Nascimento, M. C. verfasserin aut Pereira, B. L. verfasserin aut Passos, R. R. verfasserin aut Pocrifka, L. A. verfasserin aut Enthalten in Journal of solid state electrochemistry Berlin : Springer, 1997 24(2020), 8 vom: 07. Mai, Seite 1961-1968 (DE-627)271175400 (DE-600)1478940-1 1433-0768 nnns volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 https://dx.doi.org/10.1007/s10008-020-04616-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.14 ASE 35.90 ASE AR 24 2020 8 07 05 1961-1968 |
| spelling |
10.1007/s10008-020-04616-z doi (DE-627)SPR040251330 (SPR)s10008-020-04616-z-e DE-627 ger DE-627 rakwb eng 540 ASE 35.14 bkl 35.90 bkl Silva, E. C. verfasserin aut Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. Ferrites (dpeaa)DE-He213 Energy storage (dpeaa)DE-He213 Stable structure (dpeaa)DE-He213 Pseudocapacitors (dpeaa)DE-He213 da Costa, J. C. M. verfasserin aut Nascimento, M. C. verfasserin aut Pereira, B. L. verfasserin aut Passos, R. R. verfasserin aut Pocrifka, L. A. verfasserin aut Enthalten in Journal of solid state electrochemistry Berlin : Springer, 1997 24(2020), 8 vom: 07. Mai, Seite 1961-1968 (DE-627)271175400 (DE-600)1478940-1 1433-0768 nnns volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 https://dx.doi.org/10.1007/s10008-020-04616-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.14 ASE 35.90 ASE AR 24 2020 8 07 05 1961-1968 |
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10.1007/s10008-020-04616-z doi (DE-627)SPR040251330 (SPR)s10008-020-04616-z-e DE-627 ger DE-627 rakwb eng 540 ASE 35.14 bkl 35.90 bkl Silva, E. C. verfasserin aut Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. Ferrites (dpeaa)DE-He213 Energy storage (dpeaa)DE-He213 Stable structure (dpeaa)DE-He213 Pseudocapacitors (dpeaa)DE-He213 da Costa, J. C. M. verfasserin aut Nascimento, M. C. verfasserin aut Pereira, B. L. verfasserin aut Passos, R. R. verfasserin aut Pocrifka, L. A. verfasserin aut Enthalten in Journal of solid state electrochemistry Berlin : Springer, 1997 24(2020), 8 vom: 07. Mai, Seite 1961-1968 (DE-627)271175400 (DE-600)1478940-1 1433-0768 nnns volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 https://dx.doi.org/10.1007/s10008-020-04616-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.14 ASE 35.90 ASE AR 24 2020 8 07 05 1961-1968 |
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10.1007/s10008-020-04616-z doi (DE-627)SPR040251330 (SPR)s10008-020-04616-z-e DE-627 ger DE-627 rakwb eng 540 ASE 35.14 bkl 35.90 bkl Silva, E. C. verfasserin aut Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. Ferrites (dpeaa)DE-He213 Energy storage (dpeaa)DE-He213 Stable structure (dpeaa)DE-He213 Pseudocapacitors (dpeaa)DE-He213 da Costa, J. C. M. verfasserin aut Nascimento, M. C. verfasserin aut Pereira, B. L. verfasserin aut Passos, R. R. verfasserin aut Pocrifka, L. A. verfasserin aut Enthalten in Journal of solid state electrochemistry Berlin : Springer, 1997 24(2020), 8 vom: 07. Mai, Seite 1961-1968 (DE-627)271175400 (DE-600)1478940-1 1433-0768 nnns volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 https://dx.doi.org/10.1007/s10008-020-04616-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.14 ASE 35.90 ASE AR 24 2020 8 07 05 1961-1968 |
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10.1007/s10008-020-04616-z doi (DE-627)SPR040251330 (SPR)s10008-020-04616-z-e DE-627 ger DE-627 rakwb eng 540 ASE 35.14 bkl 35.90 bkl Silva, E. C. verfasserin aut Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. Ferrites (dpeaa)DE-He213 Energy storage (dpeaa)DE-He213 Stable structure (dpeaa)DE-He213 Pseudocapacitors (dpeaa)DE-He213 da Costa, J. C. M. verfasserin aut Nascimento, M. C. verfasserin aut Pereira, B. L. verfasserin aut Passos, R. R. verfasserin aut Pocrifka, L. A. verfasserin aut Enthalten in Journal of solid state electrochemistry Berlin : Springer, 1997 24(2020), 8 vom: 07. Mai, Seite 1961-1968 (DE-627)271175400 (DE-600)1478940-1 1433-0768 nnns volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 https://dx.doi.org/10.1007/s10008-020-04616-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.14 ASE 35.90 ASE AR 24 2020 8 07 05 1961-1968 |
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English |
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Enthalten in Journal of solid state electrochemistry 24(2020), 8 vom: 07. Mai, Seite 1961-1968 volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 |
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Enthalten in Journal of solid state electrochemistry 24(2020), 8 vom: 07. Mai, Seite 1961-1968 volume:24 year:2020 number:8 day:07 month:05 pages:1961-1968 |
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Silva, E. C. @@aut@@ da Costa, J. C. M. @@aut@@ Nascimento, M. C. @@aut@@ Pereira, B. L. @@aut@@ Passos, R. R. @@aut@@ Pocrifka, L. A. @@aut@@ |
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C.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2020</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Ferrites</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Energy storage</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Stable structure</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pseudocapacitors</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">da Costa, J. C. 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Silva, E. C. |
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Silva, E. C. ddc 540 bkl 35.14 bkl 35.90 misc Ferrites misc Energy storage misc Stable structure misc Pseudocapacitors Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage |
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influence of temperature on the preparation of $ cofe_{2} %$ o_{4} $ by the sol-gel method and its application in electrochemical energy storage |
| title_auth |
Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage |
| abstract |
Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. |
| abstractGer |
Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. |
| abstract_unstemmed |
Abstract $ CoFe_{2} %$ O_{4} $ particles were successfully synthesized by a sol-gel proteic route in three different temperatures, and their structural and morphological properties were studied in detail. The XRD pattern results confirmed $ CoFe_{2} %$ O_{4} $ formation with some residual second phase of αCo–Fe in low temperature calcined materials. FTIR spectra showed the strong absorption bands in the range of 440 to 650 $ cm^{−1} $, which are related to Fe–O and Fe–Co bonds. SEM images illustrated that the cobalt ferrite particles exhibit a porous structure are formed by a hexagonal morphology. It was observed that the increase of calcination temperature resulted in more crystalline and better organized materials. $ CoFe_{2} %$ O_{4} $ specific capacity was 76.52 mA h $ g^{−1} $at current density of 1 $ Ag^{−1} $. This was the best result obtained with the 1000 °C material, which was based on the fact that temperature has a great influence on the electrochemical response of cobalt ferrite synthesized by proteic sol gel. It was also observed that 75% of the initial capacity remains the same for 5000 continuous cyclic voltammetry at the scan rate of 25 $ mVs^{−1} $which confirms the superior performance of the prepared electrode as energy storage material. |
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8 |
| title_short |
Influence of temperature on the preparation of $ CoFe_{2} %$ O_{4} $ by the sol-gel method and its application in electrochemical energy storage |
| url |
https://dx.doi.org/10.1007/s10008-020-04616-z |
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da Costa, J. C. M. Nascimento, M. C. Pereira, B. L. Passos, R. R. Pocrifka, L. A. |
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da Costa, J. C. M. Nascimento, M. C. Pereira, B. L. Passos, R. R. Pocrifka, L. A. |
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2024-07-03T14:46:33.255Z |
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| score |
7.401268 |