Preparation of High Surface Area Ni-SDC Cermets Using a Surfactant-Assisted Co-Precipitation Method
Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Park, Sang Joon [verfasserIn] Eom, Tae Wook [verfasserIn] Oh, Jae Eun [verfasserIn] Yang, Hae Kwang [verfasserIn] Kim, Kyung Hwan [verfasserIn] |
|---|
| Format: |
E-Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2006 |
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| Übergeordnetes Werk: |
Enthalten in: MRS online proceedings library - Warrendale, Pa. : MRS, 1998, 942(2006), 1 vom: 01. Nov. |
|---|---|
| Übergeordnetes Werk: |
volume:942 ; year:2006 ; number:1 ; day:01 ; month:11 |
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| DOI / URN: |
10.1557/PROC-0942-W11-31 |
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SPR042561957 |
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| 520 | |a Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. | ||
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10.1557/PROC-0942-W11-31 doi (DE-627)SPR042561957 (DE-599)SPRPROC-0942-W11-31-e (SPR)PROC-0942-W11-31-e DE-627 ger DE-627 rakwb eng 670 ASE Park, Sang Joon verfasserin aut Preparation of High Surface Area Ni-SDC Cermets Using a Surfactant-Assisted Co-Precipitation Method 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. Eom, Tae Wook verfasserin aut Oh, Jae Eun verfasserin aut Yang, Hae Kwang verfasserin aut Kim, Kyung Hwan verfasserin aut Enthalten in MRS online proceedings library Warrendale, Pa. : MRS, 1998 942(2006), 1 vom: 01. Nov. (DE-627)57782046X (DE-600)2451008-7 1946-4274 nnns volume:942 year:2006 number:1 day:01 month:11 https://dx.doi.org/10.1557/PROC-0942-W11-31 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_2005 AR 942 2006 1 01 11 |
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10.1557/PROC-0942-W11-31 doi (DE-627)SPR042561957 (DE-599)SPRPROC-0942-W11-31-e (SPR)PROC-0942-W11-31-e DE-627 ger DE-627 rakwb eng 670 ASE Park, Sang Joon verfasserin aut Preparation of High Surface Area Ni-SDC Cermets Using a Surfactant-Assisted Co-Precipitation Method 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. Eom, Tae Wook verfasserin aut Oh, Jae Eun verfasserin aut Yang, Hae Kwang verfasserin aut Kim, Kyung Hwan verfasserin aut Enthalten in MRS online proceedings library Warrendale, Pa. : MRS, 1998 942(2006), 1 vom: 01. Nov. (DE-627)57782046X (DE-600)2451008-7 1946-4274 nnns volume:942 year:2006 number:1 day:01 month:11 https://dx.doi.org/10.1557/PROC-0942-W11-31 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_2005 AR 942 2006 1 01 11 |
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10.1557/PROC-0942-W11-31 doi (DE-627)SPR042561957 (DE-599)SPRPROC-0942-W11-31-e (SPR)PROC-0942-W11-31-e DE-627 ger DE-627 rakwb eng 670 ASE Park, Sang Joon verfasserin aut Preparation of High Surface Area Ni-SDC Cermets Using a Surfactant-Assisted Co-Precipitation Method 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. Eom, Tae Wook verfasserin aut Oh, Jae Eun verfasserin aut Yang, Hae Kwang verfasserin aut Kim, Kyung Hwan verfasserin aut Enthalten in MRS online proceedings library Warrendale, Pa. : MRS, 1998 942(2006), 1 vom: 01. Nov. (DE-627)57782046X (DE-600)2451008-7 1946-4274 nnns volume:942 year:2006 number:1 day:01 month:11 https://dx.doi.org/10.1557/PROC-0942-W11-31 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_2005 AR 942 2006 1 01 11 |
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10.1557/PROC-0942-W11-31 doi (DE-627)SPR042561957 (DE-599)SPRPROC-0942-W11-31-e (SPR)PROC-0942-W11-31-e DE-627 ger DE-627 rakwb eng 670 ASE Park, Sang Joon verfasserin aut Preparation of High Surface Area Ni-SDC Cermets Using a Surfactant-Assisted Co-Precipitation Method 2006 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. Eom, Tae Wook verfasserin aut Oh, Jae Eun verfasserin aut Yang, Hae Kwang verfasserin aut Kim, Kyung Hwan verfasserin aut Enthalten in MRS online proceedings library Warrendale, Pa. : MRS, 1998 942(2006), 1 vom: 01. Nov. (DE-627)57782046X (DE-600)2451008-7 1946-4274 nnns volume:942 year:2006 number:1 day:01 month:11 https://dx.doi.org/10.1557/PROC-0942-W11-31 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_2005 AR 942 2006 1 01 11 |
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Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. |
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Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. |
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Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification. |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR042561957</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220112053359.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">210105s2006 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1557/PROC-0942-W11-31</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR042561957</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)SPRPROC-0942-W11-31-e</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)PROC-0942-W11-31-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">670</subfield><subfield code="q">ASE</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Park, Sang Joon</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Preparation of High Surface Area Ni-SDC Cermets Using a Surfactant-Assisted Co-Precipitation Method</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2006</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract A surfactant-assisted co-precipitation method was employed for obtaining high surface area Ni-SDC with improved structural properties for SOFC applications. In the work, a cationic surfactant, cetyltrimethylammonium bromide(CTAB) was employed with $ NiCl_{2} $, $ SmCl_{3} $ and $ CeCl_{3} $ as precursors and $ NH_{4} $OH as mineralizer. The elimination of surfactants upon calcination gives rise to the formation of high surface area NiO-SDC. When calcined at 600°C, the powders with surface area of 249 $ m^{2} $/g, were obtained and the pore size was 14.45 nm. The powders consist of two phases, the cubic NiO and SDC confirmed with X-ray diffraction identification.</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Eom, Tae Wook</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Oh, Jae Eun</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Yang, Hae Kwang</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kim, Kyung Hwan</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">MRS online proceedings library</subfield><subfield code="d">Warrendale, Pa. : MRS, 1998</subfield><subfield code="g">942(2006), 1 vom: 01. Nov.</subfield><subfield code="w">(DE-627)57782046X</subfield><subfield code="w">(DE-600)2451008-7</subfield><subfield code="x">1946-4274</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:942</subfield><subfield code="g">year:2006</subfield><subfield code="g">number:1</subfield><subfield code="g">day:01</subfield><subfield code="g">month:11</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://dx.doi.org/10.1557/PROC-0942-W11-31</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_SPRINGER</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2005</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">942</subfield><subfield code="j">2006</subfield><subfield code="e">1</subfield><subfield code="b">01</subfield><subfield code="c">11</subfield></datafield></record></collection>
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