Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals
Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Sagar, Raghavendra [verfasserIn] Rao, Asha [verfasserIn] Prathap, Chithrakshi [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021 |
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| Schlagwörter: |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
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| Übergeordnetes Werk: |
Enthalten in: Optical and quantum electronics - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1969, 53(2021), 9 vom: 14. Aug. |
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| Übergeordnetes Werk: |
volume:53 ; year:2021 ; number:9 ; day:14 ; month:08 |
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| DOI / URN: |
10.1007/s11082-021-03177-3 |
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| Katalog-ID: |
SPR044835124 |
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| 245 | 1 | 0 | |a Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals |
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| 520 | |a Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. | ||
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| 650 | 4 | |a SHG efficiency |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Slow evaporation |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Manganese sulfate monohydrate crystal |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Rao, Asha |e verfasserin |4 aut | |
| 700 | 1 | |a Prathap, Chithrakshi |e verfasserin |4 aut | |
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10.1007/s11082-021-03177-3 doi (DE-627)SPR044835124 (SPR)s11082-021-03177-3-e DE-627 ger DE-627 rakwb eng 500 620 ASE 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 bkl Sagar, Raghavendra verfasserin aut Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. Single crystal (dpeaa)DE-He213 Optical characterization (dpeaa)DE-He213 SHG efficiency (dpeaa)DE-He213 Slow evaporation (dpeaa)DE-He213 Manganese sulfate monohydrate crystal (dpeaa)DE-He213 Rao, Asha verfasserin aut Prathap, Chithrakshi verfasserin aut Enthalten in Optical and quantum electronics Dordrecht [u.a.] : Springer Science + Business Media B.V, 1969 53(2021), 9 vom: 14. Aug. (DE-627)312693869 (DE-600)2000642-1 1572-817X nnns volume:53 year:2021 number:9 day:14 month:08 https://dx.doi.org/10.1007/s11082-021-03177-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.38 ASE 33.18 ASE 33.23 ASE 53.54 ASE 52.88 ASE 33.72 ASE AR 53 2021 9 14 08 |
| spelling |
10.1007/s11082-021-03177-3 doi (DE-627)SPR044835124 (SPR)s11082-021-03177-3-e DE-627 ger DE-627 rakwb eng 500 620 ASE 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 bkl Sagar, Raghavendra verfasserin aut Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. Single crystal (dpeaa)DE-He213 Optical characterization (dpeaa)DE-He213 SHG efficiency (dpeaa)DE-He213 Slow evaporation (dpeaa)DE-He213 Manganese sulfate monohydrate crystal (dpeaa)DE-He213 Rao, Asha verfasserin aut Prathap, Chithrakshi verfasserin aut Enthalten in Optical and quantum electronics Dordrecht [u.a.] : Springer Science + Business Media B.V, 1969 53(2021), 9 vom: 14. Aug. (DE-627)312693869 (DE-600)2000642-1 1572-817X nnns volume:53 year:2021 number:9 day:14 month:08 https://dx.doi.org/10.1007/s11082-021-03177-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.38 ASE 33.18 ASE 33.23 ASE 53.54 ASE 52.88 ASE 33.72 ASE AR 53 2021 9 14 08 |
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10.1007/s11082-021-03177-3 doi (DE-627)SPR044835124 (SPR)s11082-021-03177-3-e DE-627 ger DE-627 rakwb eng 500 620 ASE 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 bkl Sagar, Raghavendra verfasserin aut Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. Single crystal (dpeaa)DE-He213 Optical characterization (dpeaa)DE-He213 SHG efficiency (dpeaa)DE-He213 Slow evaporation (dpeaa)DE-He213 Manganese sulfate monohydrate crystal (dpeaa)DE-He213 Rao, Asha verfasserin aut Prathap, Chithrakshi verfasserin aut Enthalten in Optical and quantum electronics Dordrecht [u.a.] : Springer Science + Business Media B.V, 1969 53(2021), 9 vom: 14. Aug. (DE-627)312693869 (DE-600)2000642-1 1572-817X nnns volume:53 year:2021 number:9 day:14 month:08 https://dx.doi.org/10.1007/s11082-021-03177-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.38 ASE 33.18 ASE 33.23 ASE 53.54 ASE 52.88 ASE 33.72 ASE AR 53 2021 9 14 08 |
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10.1007/s11082-021-03177-3 doi (DE-627)SPR044835124 (SPR)s11082-021-03177-3-e DE-627 ger DE-627 rakwb eng 500 620 ASE 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 bkl Sagar, Raghavendra verfasserin aut Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. Single crystal (dpeaa)DE-He213 Optical characterization (dpeaa)DE-He213 SHG efficiency (dpeaa)DE-He213 Slow evaporation (dpeaa)DE-He213 Manganese sulfate monohydrate crystal (dpeaa)DE-He213 Rao, Asha verfasserin aut Prathap, Chithrakshi verfasserin aut Enthalten in Optical and quantum electronics Dordrecht [u.a.] : Springer Science + Business Media B.V, 1969 53(2021), 9 vom: 14. Aug. (DE-627)312693869 (DE-600)2000642-1 1572-817X nnns volume:53 year:2021 number:9 day:14 month:08 https://dx.doi.org/10.1007/s11082-021-03177-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.38 ASE 33.18 ASE 33.23 ASE 53.54 ASE 52.88 ASE 33.72 ASE AR 53 2021 9 14 08 |
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10.1007/s11082-021-03177-3 doi (DE-627)SPR044835124 (SPR)s11082-021-03177-3-e DE-627 ger DE-627 rakwb eng 500 620 ASE 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 bkl Sagar, Raghavendra verfasserin aut Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals 2021 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. Single crystal (dpeaa)DE-He213 Optical characterization (dpeaa)DE-He213 SHG efficiency (dpeaa)DE-He213 Slow evaporation (dpeaa)DE-He213 Manganese sulfate monohydrate crystal (dpeaa)DE-He213 Rao, Asha verfasserin aut Prathap, Chithrakshi verfasserin aut Enthalten in Optical and quantum electronics Dordrecht [u.a.] : Springer Science + Business Media B.V, 1969 53(2021), 9 vom: 14. Aug. (DE-627)312693869 (DE-600)2000642-1 1572-817X nnns volume:53 year:2021 number:9 day:14 month:08 https://dx.doi.org/10.1007/s11082-021-03177-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 33.38 ASE 33.18 ASE 33.23 ASE 53.54 ASE 52.88 ASE 33.72 ASE AR 53 2021 9 14 08 |
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Enthalten in Optical and quantum electronics 53(2021), 9 vom: 14. Aug. volume:53 year:2021 number:9 day:14 month:08 |
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The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. 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Sagar, Raghavendra |
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Sagar, Raghavendra ddc 500 bkl 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 misc Single crystal misc Optical characterization misc SHG efficiency misc Slow evaporation misc Manganese sulfate monohydrate crystal Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals |
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500 620 ASE 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 bkl Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals Single crystal (dpeaa)DE-He213 Optical characterization (dpeaa)DE-He213 SHG efficiency (dpeaa)DE-He213 Slow evaporation (dpeaa)DE-He213 Manganese sulfate monohydrate crystal (dpeaa)DE-He213 |
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ddc 500 bkl 33.38 bkl 33.18 bkl 33.23 bkl 53.54 bkl 52.88 bkl 33.72 misc Single crystal misc Optical characterization misc SHG efficiency misc Slow evaporation misc Manganese sulfate monohydrate crystal |
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growth, characterization and shg studies of cu (ii) doped manganese sulfate monohydrate crystals |
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Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals |
| abstract |
Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
| abstractGer |
Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
| abstract_unstemmed |
Abstract Copper incorporated manganese sulfate single crystals have been grown by a conventional slow evaporation solution technique using water as solvent. The crystal size improves noticeably with increasing Cu (II) sulfate with decrease in optical transparency. The atomic absorption spectroscopy of grown crystals conform the presence of copper and increase in its concentration after successive increase after incorporation. The phase identification exercised for all grown crystals using single crystal x-ray diffraction shows the crystallization in orthorhombic phase with almost same lattice parameters. The study of optical transmission of grown crystals carried out using UV–visible spectrophotometer shows anomalous behavior above 400. However, the transmission behavior was almost stable for 10 mol% copper (II) sulfate incorporated manganese sulfate ranging between 30 and 40% compared to other two crystals. The presence of functional groups and variations in peak position especially of O–H and sulfonate stretching was determined using FT-IR spectroscopy. The amount of water released and increase in decomposition temperature as a function Cu (II) sulfate incorporation was conformed using TGA/DSC respectively. The microhardness test of grown crystals using Vickers diamond pyramid indenter shows improved hardness as a function of Cu (II) sulfate incorporation. The second harmonic generation study shows decrease in relative conversion efficiency with increase in Cu (II) sulfate incorporation in crystals. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2021 |
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Growth, characterization and SHG studies of Cu (II) doped manganese sulfate monohydrate crystals |
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| score |
7.3972845 |