A portable electroanalytical procedure to determine paracetamol in organic fertilizers
Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in co...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Silva, Luiz R. G. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 |
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| Übergeordnetes Werk: |
Enthalten in: Ionics - Berlin : Springer, 1995, 28(2022), 3 vom: 10. Jan., Seite 1451-1460 |
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| Übergeordnetes Werk: |
volume:28 ; year:2022 ; number:3 ; day:10 ; month:01 ; pages:1451-1460 |
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| DOI / URN: |
10.1007/s11581-021-04388-0 |
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| Katalog-ID: |
SPR046278672 |
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| 100 | 1 | |a Silva, Luiz R. G. |e verfasserin |4 aut | |
| 245 | 1 | 2 | |a A portable electroanalytical procedure to determine paracetamol in organic fertilizers |
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| 520 | |a Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. | ||
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| 650 | 4 | |a Paracetamol |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Screen-printed carbon electrodes |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Vasconcellos, Maria de L. S. |4 aut | |
| 700 | 1 | |a Ferreira, Rafael de Q. |4 aut | |
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10.1007/s11581-021-04388-0 doi (DE-627)SPR046278672 (SPR)s11581-021-04388-0-e DE-627 ger DE-627 rakwb eng Silva, Luiz R. G. verfasserin aut A portable electroanalytical procedure to determine paracetamol in organic fertilizers 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. Organic fertilizer (dpeaa)DE-He213 Urine (dpeaa)DE-He213 Struvite (dpeaa)DE-He213 Paracetamol (dpeaa)DE-He213 Screen-printed carbon electrodes (dpeaa)DE-He213 Vasconcellos, Maria de L. S. aut Ferreira, Rafael de Q. aut Enthalten in Ionics Berlin : Springer, 1995 28(2022), 3 vom: 10. Jan., Seite 1451-1460 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:28 year:2022 number:3 day:10 month:01 pages:1451-1460 https://dx.doi.org/10.1007/s11581-021-04388-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 28 2022 3 10 01 1451-1460 |
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10.1007/s11581-021-04388-0 doi (DE-627)SPR046278672 (SPR)s11581-021-04388-0-e DE-627 ger DE-627 rakwb eng Silva, Luiz R. G. verfasserin aut A portable electroanalytical procedure to determine paracetamol in organic fertilizers 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. Organic fertilizer (dpeaa)DE-He213 Urine (dpeaa)DE-He213 Struvite (dpeaa)DE-He213 Paracetamol (dpeaa)DE-He213 Screen-printed carbon electrodes (dpeaa)DE-He213 Vasconcellos, Maria de L. S. aut Ferreira, Rafael de Q. aut Enthalten in Ionics Berlin : Springer, 1995 28(2022), 3 vom: 10. Jan., Seite 1451-1460 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:28 year:2022 number:3 day:10 month:01 pages:1451-1460 https://dx.doi.org/10.1007/s11581-021-04388-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 28 2022 3 10 01 1451-1460 |
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10.1007/s11581-021-04388-0 doi (DE-627)SPR046278672 (SPR)s11581-021-04388-0-e DE-627 ger DE-627 rakwb eng Silva, Luiz R. G. verfasserin aut A portable electroanalytical procedure to determine paracetamol in organic fertilizers 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. Organic fertilizer (dpeaa)DE-He213 Urine (dpeaa)DE-He213 Struvite (dpeaa)DE-He213 Paracetamol (dpeaa)DE-He213 Screen-printed carbon electrodes (dpeaa)DE-He213 Vasconcellos, Maria de L. S. aut Ferreira, Rafael de Q. aut Enthalten in Ionics Berlin : Springer, 1995 28(2022), 3 vom: 10. Jan., Seite 1451-1460 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:28 year:2022 number:3 day:10 month:01 pages:1451-1460 https://dx.doi.org/10.1007/s11581-021-04388-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 28 2022 3 10 01 1451-1460 |
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10.1007/s11581-021-04388-0 doi (DE-627)SPR046278672 (SPR)s11581-021-04388-0-e DE-627 ger DE-627 rakwb eng Silva, Luiz R. G. verfasserin aut A portable electroanalytical procedure to determine paracetamol in organic fertilizers 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. Organic fertilizer (dpeaa)DE-He213 Urine (dpeaa)DE-He213 Struvite (dpeaa)DE-He213 Paracetamol (dpeaa)DE-He213 Screen-printed carbon electrodes (dpeaa)DE-He213 Vasconcellos, Maria de L. S. aut Ferreira, Rafael de Q. aut Enthalten in Ionics Berlin : Springer, 1995 28(2022), 3 vom: 10. Jan., Seite 1451-1460 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:28 year:2022 number:3 day:10 month:01 pages:1451-1460 https://dx.doi.org/10.1007/s11581-021-04388-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 28 2022 3 10 01 1451-1460 |
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10.1007/s11581-021-04388-0 doi (DE-627)SPR046278672 (SPR)s11581-021-04388-0-e DE-627 ger DE-627 rakwb eng Silva, Luiz R. G. verfasserin aut A portable electroanalytical procedure to determine paracetamol in organic fertilizers 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. Organic fertilizer (dpeaa)DE-He213 Urine (dpeaa)DE-He213 Struvite (dpeaa)DE-He213 Paracetamol (dpeaa)DE-He213 Screen-printed carbon electrodes (dpeaa)DE-He213 Vasconcellos, Maria de L. S. aut Ferreira, Rafael de Q. aut Enthalten in Ionics Berlin : Springer, 1995 28(2022), 3 vom: 10. Jan., Seite 1451-1460 (DE-627)509398944 (DE-600)2226746-3 1862-0760 nnns volume:28 year:2022 number:3 day:10 month:01 pages:1451-1460 https://dx.doi.org/10.1007/s11581-021-04388-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 28 2022 3 10 01 1451-1460 |
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Silva, Luiz R. G. @@aut@@ Vasconcellos, Maria de L. S. @@aut@@ Ferreira, Rafael de Q. @@aut@@ |
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Silva, Luiz R. G. |
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Silva, Luiz R. G. misc Organic fertilizer misc Urine misc Struvite misc Paracetamol misc Screen-printed carbon electrodes A portable electroanalytical procedure to determine paracetamol in organic fertilizers |
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A portable electroanalytical procedure to determine paracetamol in organic fertilizers Organic fertilizer (dpeaa)DE-He213 Urine (dpeaa)DE-He213 Struvite (dpeaa)DE-He213 Paracetamol (dpeaa)DE-He213 Screen-printed carbon electrodes (dpeaa)DE-He213 |
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A portable electroanalytical procedure to determine paracetamol in organic fertilizers |
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Silva, Luiz R. G. |
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portable electroanalytical procedure to determine paracetamol in organic fertilizers |
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A portable electroanalytical procedure to determine paracetamol in organic fertilizers |
| abstract |
Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 |
| abstractGer |
Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 |
| abstract_unstemmed |
Abstract The present study developed an electroanalytical procedure employing a portable, fast, sensitive, relatively low-cost, and sustainable system for the determination of acetaminophen in human urine and struvite used as organic fertilizer. Thus, screen-printed carbon electrodes were used in conjunction with optimized square-wave voltammetry to develop a procedure capable of monitoring acetaminophen levels in urine and struvite used as organic fertilizer, ensuring safer products for agricultural application. The study with different electrolytes in a wide pH range (1 to 12) and the proposed procedure presented a limit of detection of 0.06 µmol $ L^{−1} $. The method demonstrates a good selectivity for determining paracetamol, compared to the studied interferents. Furthermore, recovery tests on different samples showed values between 92 and 106%. These results demonstrate the possibility of applying the proposed procedure in a practical and fast way, and with the possibility of on-site application. © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2021 |
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A portable electroanalytical procedure to determine paracetamol in organic fertilizers |
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https://dx.doi.org/10.1007/s11581-021-04388-0 |
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Vasconcellos, Maria de L. S. Ferreira, Rafael de Q. |
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10.1007/s11581-021-04388-0 |
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2024-07-03T21:32:07.261Z |
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