Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization
Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-,...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Singh, Sandip K. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Nature B.V. 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Waste and biomass valorization - [Dordrecht] : Springer Netherlands, 2010, 13(2022), 6 vom: 13. Feb., Seite 2963-2977 |
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| Übergeordnetes Werk: |
volume:13 ; year:2022 ; number:6 ; day:13 ; month:02 ; pages:2963-2977 |
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| DOI / URN: |
10.1007/s12649-022-01704-1 |
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| Katalog-ID: |
SPR046947507 |
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| 520 | |a Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. | ||
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10.1007/s12649-022-01704-1 doi (DE-627)SPR046947507 (SPR)s12649-022-01704-1-e DE-627 ger DE-627 rakwb eng Singh, Sandip K. verfasserin aut Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Nature B.V. 2022 Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. Rice husks (dpeaa)DE-He213 Holocellulose (dpeaa)DE-He213 Lignin (dpeaa)DE-He213 Homogeneous and heterogeneous catalysts (dpeaa)DE-He213 Dhepe, Paresh L. (orcid)0000-0001-6111-8916 aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 13(2022), 6 vom: 13. Feb., Seite 2963-2977 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:13 year:2022 number:6 day:13 month:02 pages:2963-2977 https://dx.doi.org/10.1007/s12649-022-01704-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 13 2022 6 13 02 2963-2977 |
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10.1007/s12649-022-01704-1 doi (DE-627)SPR046947507 (SPR)s12649-022-01704-1-e DE-627 ger DE-627 rakwb eng Singh, Sandip K. verfasserin aut Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Nature B.V. 2022 Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. Rice husks (dpeaa)DE-He213 Holocellulose (dpeaa)DE-He213 Lignin (dpeaa)DE-He213 Homogeneous and heterogeneous catalysts (dpeaa)DE-He213 Dhepe, Paresh L. (orcid)0000-0001-6111-8916 aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 13(2022), 6 vom: 13. Feb., Seite 2963-2977 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:13 year:2022 number:6 day:13 month:02 pages:2963-2977 https://dx.doi.org/10.1007/s12649-022-01704-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 13 2022 6 13 02 2963-2977 |
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10.1007/s12649-022-01704-1 doi (DE-627)SPR046947507 (SPR)s12649-022-01704-1-e DE-627 ger DE-627 rakwb eng Singh, Sandip K. verfasserin aut Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Nature B.V. 2022 Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. Rice husks (dpeaa)DE-He213 Holocellulose (dpeaa)DE-He213 Lignin (dpeaa)DE-He213 Homogeneous and heterogeneous catalysts (dpeaa)DE-He213 Dhepe, Paresh L. (orcid)0000-0001-6111-8916 aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 13(2022), 6 vom: 13. Feb., Seite 2963-2977 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:13 year:2022 number:6 day:13 month:02 pages:2963-2977 https://dx.doi.org/10.1007/s12649-022-01704-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 13 2022 6 13 02 2963-2977 |
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10.1007/s12649-022-01704-1 doi (DE-627)SPR046947507 (SPR)s12649-022-01704-1-e DE-627 ger DE-627 rakwb eng Singh, Sandip K. verfasserin aut Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Nature B.V. 2022 Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. Rice husks (dpeaa)DE-He213 Holocellulose (dpeaa)DE-He213 Lignin (dpeaa)DE-He213 Homogeneous and heterogeneous catalysts (dpeaa)DE-He213 Dhepe, Paresh L. (orcid)0000-0001-6111-8916 aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 13(2022), 6 vom: 13. Feb., Seite 2963-2977 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:13 year:2022 number:6 day:13 month:02 pages:2963-2977 https://dx.doi.org/10.1007/s12649-022-01704-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 13 2022 6 13 02 2963-2977 |
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10.1007/s12649-022-01704-1 doi (DE-627)SPR046947507 (SPR)s12649-022-01704-1-e DE-627 ger DE-627 rakwb eng Singh, Sandip K. verfasserin aut Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Nature B.V. 2022 Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. Rice husks (dpeaa)DE-He213 Holocellulose (dpeaa)DE-He213 Lignin (dpeaa)DE-He213 Homogeneous and heterogeneous catalysts (dpeaa)DE-He213 Dhepe, Paresh L. (orcid)0000-0001-6111-8916 aut Enthalten in Waste and biomass valorization [Dordrecht] : Springer Netherlands, 2010 13(2022), 6 vom: 13. Feb., Seite 2963-2977 (DE-627)620147245 (DE-600)2541900-6 1877-265X nnns volume:13 year:2022 number:6 day:13 month:02 pages:2963-2977 https://dx.doi.org/10.1007/s12649-022-01704-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 13 2022 6 13 02 2963-2977 |
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Singh, Sandip K. |
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Singh, Sandip K. misc Rice husks misc Holocellulose misc Lignin misc Homogeneous and heterogeneous catalysts Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization |
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Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization Rice husks (dpeaa)DE-He213 Holocellulose (dpeaa)DE-He213 Lignin (dpeaa)DE-He213 Homogeneous and heterogeneous catalysts (dpeaa)DE-He213 |
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Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization |
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Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization |
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alpha-, beta- and gamma-cellulose quantification and two-stage concentrated-dilute acid lignin recovery from three rice husks: lignin characterization and depolymerization |
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Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization |
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Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. © The Author(s), under exclusive licence to Springer Nature B.V. 2022 |
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Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. © The Author(s), under exclusive licence to Springer Nature B.V. 2022 |
| abstract_unstemmed |
Investigations on the compositional analysis of lignocellulosic materials and their properties upon recovery are essential to be studied in order to examine the effects of recovery method, their dependency on the substrate, etc. In this work, three rice husks (RHs) samples were subjected for alpha-, beta- and gamma-cellulose, pentosan, and silica quantifications. Correlations between the source of biomass, lignin recovery by two-stage concentrated and dilute sulphuric acid treatment, their properties and their depolymerization into low molecular mass aromatic fractions using homogeneous and heterogeneous Brønsted acidic ionic liquids as catalysts, is carried out. Correlation between the properties of RHs and recovered lignin were performed using destructive (CHNS, TGA, ICP-OES, etc.) and non-destructive (XRD, UV–Visible, FT-IR, and 13C CP-MAS NMR) analytical techniques. It was observed that the recovered lignin was polysaccharides free and associated with dibenzodioxocin, spirodienone, and tricin type moieties with variable intensities. The effects of lignin structures showed a change of depolymerisation product pattern. Graphical Abstract The quantification of α-, β- and γ-cellulose and two-stage concentrated-dilute acid lignin recovery from three rice husks, was performed and the effect of lignin properties during homogeneous and heterogenous depolymerization was correlated. © The Author(s), under exclusive licence to Springer Nature B.V. 2022 |
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Alpha-, Beta- and Gamma-Cellulose Quantification and Two-Stage Concentrated-Dilute Acid Lignin Recovery from Three Rice Husks: Lignin Characterization and Depolymerization |
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https://dx.doi.org/10.1007/s12649-022-01704-1 |
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| score |
7.4010506 |