Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water

Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dich...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Katsuta, Shoichi [verfasserIn] Saito, Yuki Takahashi, Suguru

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2018

Schlagwörter:	Lithium seawater extraction–spectrophotometric determination metallacrown

Anmerkung:	© The Japan Society for Analytical Chemistry 2018

Übergeordnetes Werk:	Enthalten in: Analytical sciences - [Cham] : Springer International Publishing, 1985, 34(2018), 2 vom: Feb., Seite 189-193
Übergeordnetes Werk:	volume:34 ; year:2018 ; number:2 ; month:02 ; pages:189-193

Links:	Volltext

DOI / URN:	10.2116/analsci.34.189

Katalog-ID:	SPR047302186

Internformat


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100	1		\|a Katsuta, Shoichi \|e verfasserin \|4 aut
245	1	0	\|a Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water
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520			\|a Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible.
650		4	\|a Lithium \|7 (dpeaa)DE-He213
650		4	\|a seawater \|7 (dpeaa)DE-He213
650		4	\|a extraction–spectrophotometric determination \|7 (dpeaa)DE-He213
650		4	\|a metallacrown \|7 (dpeaa)DE-He213
700	1		\|a Saito, Yuki \|4 aut
700	1		\|a Takahashi, Suguru \|4 aut
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912			\|a GBV_ILN_39
912			\|a GBV_ILN_40
912			\|a GBV_ILN_60
912			\|a GBV_ILN_62
912			\|a GBV_ILN_63
912			\|a GBV_ILN_65
912			\|a GBV_ILN_69
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912			\|a GBV_ILN_73
912			\|a GBV_ILN_74
912			\|a GBV_ILN_90
912			\|a GBV_ILN_95
912			\|a GBV_ILN_100
912			\|a GBV_ILN_101
912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_138
912			\|a GBV_ILN_151
912			\|a GBV_ILN_152
912			\|a GBV_ILN_161
912			\|a GBV_ILN_170
912			\|a GBV_ILN_171
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_250
912			\|a GBV_ILN_281
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2008
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2056
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2113
912			\|a GBV_ILN_2118
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2144
912			\|a GBV_ILN_2147
912			\|a GBV_ILN_2148
912			\|a GBV_ILN_2152
912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2360
912			\|a GBV_ILN_2446
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2472
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_2522
912			\|a GBV_ILN_4012
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4046
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
912			\|a GBV_ILN_4126
912			\|a GBV_ILN_4242
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912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4306
912			\|a GBV_ILN_4307
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4322
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
912			\|a GBV_ILN_4326
912			\|a GBV_ILN_4328
912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4335
912			\|a GBV_ILN_4336
912			\|a GBV_ILN_4338
912			\|a GBV_ILN_4367
912			\|a GBV_ILN_4393
912			\|a GBV_ILN_4700
951			\|a AR
952			\|d 34 \|j 2018 \|e 2 \|c 02 \|h 189-193

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author_variant	s k sk y s ys s t st
matchkey_str	article:13482246:2018----::plctooaihuineetvmtlarwtetatosetohtmtidtr
hierarchy_sort_str	2018
publishDate	2018
allfields	10.2116/analsci.34.189 doi (DE-627)SPR047302186 (SPR)analsci.34.189-e DE-627 ger DE-627 rakwb eng Katsuta, Shoichi verfasserin aut Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2018 Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. Lithium (dpeaa)DE-He213 seawater (dpeaa)DE-He213 extraction–spectrophotometric determination (dpeaa)DE-He213 metallacrown (dpeaa)DE-He213 Saito, Yuki aut Takahashi, Suguru aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 34(2018), 2 vom: Feb., Seite 189-193 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:34 year:2018 number:2 month:02 pages:189-193 https://dx.doi.org/10.2116/analsci.34.189 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 34 2018 2 02 189-193
spelling	10.2116/analsci.34.189 doi (DE-627)SPR047302186 (SPR)analsci.34.189-e DE-627 ger DE-627 rakwb eng Katsuta, Shoichi verfasserin aut Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2018 Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. Lithium (dpeaa)DE-He213 seawater (dpeaa)DE-He213 extraction–spectrophotometric determination (dpeaa)DE-He213 metallacrown (dpeaa)DE-He213 Saito, Yuki aut Takahashi, Suguru aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 34(2018), 2 vom: Feb., Seite 189-193 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:34 year:2018 number:2 month:02 pages:189-193 https://dx.doi.org/10.2116/analsci.34.189 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 34 2018 2 02 189-193
allfields_unstemmed	10.2116/analsci.34.189 doi (DE-627)SPR047302186 (SPR)analsci.34.189-e DE-627 ger DE-627 rakwb eng Katsuta, Shoichi verfasserin aut Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2018 Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. Lithium (dpeaa)DE-He213 seawater (dpeaa)DE-He213 extraction–spectrophotometric determination (dpeaa)DE-He213 metallacrown (dpeaa)DE-He213 Saito, Yuki aut Takahashi, Suguru aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 34(2018), 2 vom: Feb., Seite 189-193 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:34 year:2018 number:2 month:02 pages:189-193 https://dx.doi.org/10.2116/analsci.34.189 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 34 2018 2 02 189-193
allfieldsGer	10.2116/analsci.34.189 doi (DE-627)SPR047302186 (SPR)analsci.34.189-e DE-627 ger DE-627 rakwb eng Katsuta, Shoichi verfasserin aut Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2018 Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. Lithium (dpeaa)DE-He213 seawater (dpeaa)DE-He213 extraction–spectrophotometric determination (dpeaa)DE-He213 metallacrown (dpeaa)DE-He213 Saito, Yuki aut Takahashi, Suguru aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 34(2018), 2 vom: Feb., Seite 189-193 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:34 year:2018 number:2 month:02 pages:189-193 https://dx.doi.org/10.2116/analsci.34.189 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 34 2018 2 02 189-193
allfieldsSound	10.2116/analsci.34.189 doi (DE-627)SPR047302186 (SPR)analsci.34.189-e DE-627 ger DE-627 rakwb eng Katsuta, Shoichi verfasserin aut Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water 2018 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2018 Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. Lithium (dpeaa)DE-He213 seawater (dpeaa)DE-He213 extraction–spectrophotometric determination (dpeaa)DE-He213 metallacrown (dpeaa)DE-He213 Saito, Yuki aut Takahashi, Suguru aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 34(2018), 2 vom: Feb., Seite 189-193 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:34 year:2018 number:2 month:02 pages:189-193 https://dx.doi.org/10.2116/analsci.34.189 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 34 2018 2 02 189-193
language	English
source	Enthalten in Analytical sciences 34(2018), 2 vom: Feb., Seite 189-193 volume:34 year:2018 number:2 month:02 pages:189-193
sourceStr	Enthalten in Analytical sciences 34(2018), 2 vom: Feb., Seite 189-193 volume:34 year:2018 number:2 month:02 pages:189-193
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Lithium seawater extraction–spectrophotometric determination metallacrown
isfreeaccess_bool	false
container_title	Analytical sciences
authorswithroles_txt_mv	Katsuta, Shoichi @@aut@@ Saito, Yuki @@aut@@ Takahashi, Suguru @@aut@@
publishDateDaySort_date	2018-02-01T00:00:00Z
hierarchy_top_id	300895925
id	SPR047302186
language_de	englisch
fullrecord	<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR047302186</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230809064810.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">220616s2018 xx \|\|\|\|\|o 00\| \|\|eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.2116/analsci.34.189</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR047302186</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)analsci.34.189-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Katsuta, Shoichi</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2018</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© The Japan Society for Analytical Chemistry 2018</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). 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author	Katsuta, Shoichi
spellingShingle	Katsuta, Shoichi misc Lithium misc seawater misc extraction–spectrophotometric determination misc metallacrown Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water
authorStr	Katsuta, Shoichi
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topic_title	Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water Lithium (dpeaa)DE-He213 seawater (dpeaa)DE-He213 extraction–spectrophotometric determination (dpeaa)DE-He213 metallacrown (dpeaa)DE-He213
topic	misc Lithium misc seawater misc extraction–spectrophotometric determination misc metallacrown
topic_unstemmed	misc Lithium misc seawater misc extraction–spectrophotometric determination misc metallacrown
topic_browse	misc Lithium misc seawater misc extraction–spectrophotometric determination misc metallacrown
format_facet	Elektronische Aufsätze Aufsätze Elektronische Ressource
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title	Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water
ctrlnum	(DE-627)SPR047302186 (SPR)analsci.34.189-e
title_full	Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water
author_sort	Katsuta, Shoichi
journal	Analytical sciences
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container_start_page	189
author_browse	Katsuta, Shoichi Saito, Yuki Takahashi, Suguru
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author-letter	Katsuta, Shoichi
doi_str_mv	10.2116/analsci.34.189
title_sort	application of a lithium-ion selective metallacrown to extraction-spectrophotometric determination of lithium in saline water
title_auth	Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water
abstract	Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. © The Japan Society for Analytical Chemistry 2018
abstractGer	Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. © The Japan Society for Analytical Chemistry 2018
abstract_unstemmed	Abstract The solvent-extraction behavior of $ Li^{+} $ and $ Na^{+} $ with a $ Li^{+} $ selective metallacrown, [{Ru($ η^{6} $-3,5-dimethylanisole) (2,3- pyridinediolate)}3], was investigated in the presence of organic dye anions, 3′,3″,5′,5″-tetrabromophenolphthalein ethyl ester ([TBPE]–), 2,6-dichloroindophenolate, and picrate ([pic]–). Each alkali metal ion was extracted as a 1:1:1 ternary complex of the metal ion, metallacrown, and anion. The $ Li^{+} $/$ Na^{+} $ extraction selectivity is anion dependent and highest with [pic]–. Therefore, we devised an extraction–spectrophotometric determination method for $ Li^{+} $ in saline water based on the extraction of Li+ using the metallacrown and [pic]– for high selectivity and subsequent replacement of [pic]– in the extracted species with [TBPE]– for high sensitivity. When applying this to artificial seawater samples containing known concentrations of $ Li^{+} $, a linear relationship was observed between the absorbance at 571 nm of the organic phase and the $ Li^{+} $ concentration in the samples. By this method, the determination of $ Li^{+} $ at the sub-ppm level in natural seawater is possible. © The Japan Society for Analytical Chemistry 2018
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title_short	Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water
url	https://dx.doi.org/10.2116/analsci.34.189
remote_bool	true
author2	Saito, Yuki Takahashi, Suguru
author2Str	Saito, Yuki Takahashi, Suguru
ppnlink	300895925
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doi_str	10.2116/analsci.34.189
up_date	2024-07-04T02:39:32.743Z
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Application of a Lithium-ion Selective Metallacrown to Extraction-Spectrophotometric Determination of Lithium in Saline Water

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