Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device
Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was pr...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ueta, Ikuo [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020 |
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| Schlagwörter: |
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| Anmerkung: |
© The Japan Society for Analytical Chemistry 2020 |
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| Übergeordnetes Werk: |
Enthalten in: Analytical sciences - [Cham] : Springer International Publishing, 1985, 36(2020), 9 vom: 17. Apr., Seite 1071-1074 |
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| Übergeordnetes Werk: |
volume:36 ; year:2020 ; number:9 ; day:17 ; month:04 ; pages:1071-1074 |
| Links: |
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| DOI / URN: |
10.2116/analsci.20P022 |
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| Katalog-ID: |
SPR047479205 |
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| 520 | |a Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. | ||
| 650 | 4 | |a Volatile organic compounds |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a semi-volatile organic compounds |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a sick house syndrome |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a gas chromatography |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Takenaka, Risa |4 aut | |
| 700 | 1 | |a Fujimura, Koji |4 aut | |
| 700 | 1 | |a Yoshimura, Tomotaka |4 aut | |
| 700 | 1 | |a Narukami, Shoji |4 aut | |
| 700 | 1 | |a Mochizuki, Suguru |4 aut | |
| 700 | 1 | |a Maeda, Tsuneaki |4 aut | |
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10.2116/analsci.20P022 doi (DE-627)SPR047479205 (SPR)analsci.20P022-e DE-627 ger DE-627 rakwb eng Ueta, Ikuo verfasserin aut Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2020 Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. Volatile organic compounds (dpeaa)DE-He213 semi-volatile organic compounds (dpeaa)DE-He213 sick house syndrome (dpeaa)DE-He213 gas chromatography (dpeaa)DE-He213 Takenaka, Risa aut Fujimura, Koji aut Yoshimura, Tomotaka aut Narukami, Shoji aut Mochizuki, Suguru aut Maeda, Tsuneaki aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 36(2020), 9 vom: 17. Apr., Seite 1071-1074 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:36 year:2020 number:9 day:17 month:04 pages:1071-1074 https://dx.doi.org/10.2116/analsci.20P022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 36 2020 9 17 04 1071-1074 |
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10.2116/analsci.20P022 doi (DE-627)SPR047479205 (SPR)analsci.20P022-e DE-627 ger DE-627 rakwb eng Ueta, Ikuo verfasserin aut Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2020 Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. Volatile organic compounds (dpeaa)DE-He213 semi-volatile organic compounds (dpeaa)DE-He213 sick house syndrome (dpeaa)DE-He213 gas chromatography (dpeaa)DE-He213 Takenaka, Risa aut Fujimura, Koji aut Yoshimura, Tomotaka aut Narukami, Shoji aut Mochizuki, Suguru aut Maeda, Tsuneaki aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 36(2020), 9 vom: 17. Apr., Seite 1071-1074 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:36 year:2020 number:9 day:17 month:04 pages:1071-1074 https://dx.doi.org/10.2116/analsci.20P022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 36 2020 9 17 04 1071-1074 |
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10.2116/analsci.20P022 doi (DE-627)SPR047479205 (SPR)analsci.20P022-e DE-627 ger DE-627 rakwb eng Ueta, Ikuo verfasserin aut Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2020 Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. Volatile organic compounds (dpeaa)DE-He213 semi-volatile organic compounds (dpeaa)DE-He213 sick house syndrome (dpeaa)DE-He213 gas chromatography (dpeaa)DE-He213 Takenaka, Risa aut Fujimura, Koji aut Yoshimura, Tomotaka aut Narukami, Shoji aut Mochizuki, Suguru aut Maeda, Tsuneaki aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 36(2020), 9 vom: 17. Apr., Seite 1071-1074 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:36 year:2020 number:9 day:17 month:04 pages:1071-1074 https://dx.doi.org/10.2116/analsci.20P022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 36 2020 9 17 04 1071-1074 |
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10.2116/analsci.20P022 doi (DE-627)SPR047479205 (SPR)analsci.20P022-e DE-627 ger DE-627 rakwb eng Ueta, Ikuo verfasserin aut Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2020 Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. Volatile organic compounds (dpeaa)DE-He213 semi-volatile organic compounds (dpeaa)DE-He213 sick house syndrome (dpeaa)DE-He213 gas chromatography (dpeaa)DE-He213 Takenaka, Risa aut Fujimura, Koji aut Yoshimura, Tomotaka aut Narukami, Shoji aut Mochizuki, Suguru aut Maeda, Tsuneaki aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 36(2020), 9 vom: 17. Apr., Seite 1071-1074 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:36 year:2020 number:9 day:17 month:04 pages:1071-1074 https://dx.doi.org/10.2116/analsci.20P022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 36 2020 9 17 04 1071-1074 |
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10.2116/analsci.20P022 doi (DE-627)SPR047479205 (SPR)analsci.20P022-e DE-627 ger DE-627 rakwb eng Ueta, Ikuo verfasserin aut Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device 2020 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2020 Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. Volatile organic compounds (dpeaa)DE-He213 semi-volatile organic compounds (dpeaa)DE-He213 sick house syndrome (dpeaa)DE-He213 gas chromatography (dpeaa)DE-He213 Takenaka, Risa aut Fujimura, Koji aut Yoshimura, Tomotaka aut Narukami, Shoji aut Mochizuki, Suguru aut Maeda, Tsuneaki aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 36(2020), 9 vom: 17. Apr., Seite 1071-1074 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:36 year:2020 number:9 day:17 month:04 pages:1071-1074 https://dx.doi.org/10.2116/analsci.20P022 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2360 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 36 2020 9 17 04 1071-1074 |
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Ueta, Ikuo @@aut@@ Takenaka, Risa @@aut@@ Fujimura, Koji @@aut@@ Yoshimura, Tomotaka @@aut@@ Narukami, Shoji @@aut@@ Mochizuki, Suguru @@aut@@ Maeda, Tsuneaki @@aut@@ |
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Ueta, Ikuo |
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Ueta, Ikuo misc Volatile organic compounds misc semi-volatile organic compounds misc sick house syndrome misc gas chromatography Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device |
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Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device Volatile organic compounds (dpeaa)DE-He213 semi-volatile organic compounds (dpeaa)DE-He213 sick house syndrome (dpeaa)DE-He213 gas chromatography (dpeaa)DE-He213 |
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Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device |
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Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device |
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Ueta, Ikuo Takenaka, Risa Fujimura, Koji Yoshimura, Tomotaka Narukami, Shoji Mochizuki, Suguru Maeda, Tsuneaki |
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simultaneous extraction and determination of volatile organic compounds and semi-volatile organic compounds in indoor air using multi-bed solid phase extraction device |
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Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device |
| abstract |
Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. © The Japan Society for Analytical Chemistry 2020 |
| abstractGer |
Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. © The Japan Society for Analytical Chemistry 2020 |
| abstract_unstemmed |
Abstract A method for the simultaneous extraction and determination of indoor volatile compounds, including volatile organic compounds (VOCs) and semi-volatile organic compounds (SVOCs), was developed using a multi-bed solid phase extraction (SPE)-type collection device. The collection device was prepared by packing styrene-divinylbenzene polymer particles and activated carbon particles. The collected analytes were completely desorbed by passing 7 mL of acetone, and the solvent was then injected into a gas chromatograph-mass spectrometry without the concentration process. Because the proposed method does not require ultrasonication and a concentration process of eluted solvent, quantitative determination of a relatively volatile compound could be achieved. The total recovery including extraction and elution recoveries for all the investigated analytes were in the range from 91.6 to 109%. The limit of quantification was less than 4.0 ng $ L^{−1} $ for all the investigated analytes, and relative standard deviations of the peak area of the analytes in indoor air were less than 12%. The collection device could be reused for over 50 samplings. © The Japan Society for Analytical Chemistry 2020 |
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Simultaneous Extraction and Determination of Volatile Organic Compounds and Semi-volatile Organic Compounds in Indoor Air Using Multi-bed Solid Phase Extraction Device |
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Takenaka, Risa Fujimura, Koji Yoshimura, Tomotaka Narukami, Shoji Mochizuki, Suguru Maeda, Tsuneaki |
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Takenaka, Risa Fujimura, Koji Yoshimura, Tomotaka Narukami, Shoji Mochizuki, Suguru Maeda, Tsuneaki |
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10.2116/analsci.20P022 |
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2024-07-04T03:15:38.799Z |
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