Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon
Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the...
Ausführliche Beschreibung
Autor*in: |
Asada, Takashi [verfasserIn] |
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Format: |
E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2004 |
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Anmerkung: |
© The Japan Society for Analytical Chemistry 2004 |
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Übergeordnetes Werk: |
Enthalten in: Analytical sciences - [Cham] : Springer International Publishing, 1985, 20(2004), 1 vom: Jan., Seite 125-128 |
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Übergeordnetes Werk: |
volume:20 ; year:2004 ; number:1 ; month:01 ; pages:125-128 |
Links: |
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DOI / URN: |
10.2116/analsci.20.125 |
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Katalog-ID: |
SPR047484225 |
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520 | |a Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. | ||
700 | 1 | |a Oikawa, Kikuo |4 aut | |
700 | 1 | |a Kawata, Kuniaki |4 aut | |
700 | 1 | |a Iyobe, Tsutomu |4 aut | |
700 | 1 | |a Yamada, Akifumi |4 aut | |
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10.2116/analsci.20.125 doi (DE-627)SPR047484225 (SPR)analsci.20.125-e DE-627 ger DE-627 rakwb eng Asada, Takashi verfasserin aut Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2004 Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. Oikawa, Kikuo aut Kawata, Kuniaki aut Iyobe, Tsutomu aut Yamada, Akifumi aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 20(2004), 1 vom: Jan., Seite 125-128 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:20 year:2004 number:1 month:01 pages:125-128 https://dx.doi.org/10.2116/analsci.20.125 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 20 2004 1 01 125-128 |
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10.2116/analsci.20.125 doi (DE-627)SPR047484225 (SPR)analsci.20.125-e DE-627 ger DE-627 rakwb eng Asada, Takashi verfasserin aut Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2004 Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. Oikawa, Kikuo aut Kawata, Kuniaki aut Iyobe, Tsutomu aut Yamada, Akifumi aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 20(2004), 1 vom: Jan., Seite 125-128 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:20 year:2004 number:1 month:01 pages:125-128 https://dx.doi.org/10.2116/analsci.20.125 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 20 2004 1 01 125-128 |
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10.2116/analsci.20.125 doi (DE-627)SPR047484225 (SPR)analsci.20.125-e DE-627 ger DE-627 rakwb eng Asada, Takashi verfasserin aut Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2004 Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. Oikawa, Kikuo aut Kawata, Kuniaki aut Iyobe, Tsutomu aut Yamada, Akifumi aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 20(2004), 1 vom: Jan., Seite 125-128 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:20 year:2004 number:1 month:01 pages:125-128 https://dx.doi.org/10.2116/analsci.20.125 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 20 2004 1 01 125-128 |
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10.2116/analsci.20.125 doi (DE-627)SPR047484225 (SPR)analsci.20.125-e DE-627 ger DE-627 rakwb eng Asada, Takashi verfasserin aut Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2004 Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. Oikawa, Kikuo aut Kawata, Kuniaki aut Iyobe, Tsutomu aut Yamada, Akifumi aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 20(2004), 1 vom: Jan., Seite 125-128 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:20 year:2004 number:1 month:01 pages:125-128 https://dx.doi.org/10.2116/analsci.20.125 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 20 2004 1 01 125-128 |
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10.2116/analsci.20.125 doi (DE-627)SPR047484225 (SPR)analsci.20.125-e DE-627 ger DE-627 rakwb eng Asada, Takashi verfasserin aut Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon 2004 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 2004 Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. Oikawa, Kikuo aut Kawata, Kuniaki aut Iyobe, Tsutomu aut Yamada, Akifumi aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 20(2004), 1 vom: Jan., Seite 125-128 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:20 year:2004 number:1 month:01 pages:125-128 https://dx.doi.org/10.2116/analsci.20.125 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_138 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 AR 20 2004 1 01 125-128 |
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Asada, Takashi @@aut@@ Oikawa, Kikuo @@aut@@ Kawata, Kuniaki @@aut@@ Iyobe, Tsutomu @@aut@@ Yamada, Akifumi @@aut@@ |
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Asada, Takashi Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon |
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Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon |
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ion chromatographic determination of ammonia in air using a sampling tube of porous carbon |
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Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon |
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Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. © The Japan Society for Analytical Chemistry 2004 |
abstractGer |
Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. © The Japan Society for Analytical Chemistry 2004 |
abstract_unstemmed |
Abstract The ion chromatographic determination of ammonia in air using a sampling tube of porous carbon carbonized at 500˚C was examined. When the mean recovery and the reproducibility for a series of five determinations were examined for 1 and 10 ppm ammonia gases, the mean recovery (n = 5) and the relative standard deviation were 97.0% and 3.5% for 1 ppm and 86.9% and 2.8% for 10 ppm, respectively. Furthermore, the recovery from 10 ppm ammonia gas increased with an increase in the extraction time, and a recovery of 99.7% was obtained for 180 min of extraction time. The mean collection efficiency for 1 and 10 ppm ammonia gas was 102.5% and 96.5%, respectively. The relation between the sampling volume and the peak area was linear, and the linearity was 0.999 of the correlation coefficient. The ammonia gas concentration in an actual goat shed could be determined by this sampling device for a sampling volume of 5 L at a flow rate of 1 L/min; 0.79 ppm of the determination value practically agreed as compare with 0.78 ppm from collection by a boric acid solution. © The Japan Society for Analytical Chemistry 2004 |
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Ion Chromatographic Determination of Ammonia in Air Using a Sampling Tube of Porous Carbon |
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