Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment
Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carb...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Masuda, Mitsuhiro [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1993 |
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| Schlagwörter: |
Supercritical fluid extraction |
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| Anmerkung: |
© The Japan Society for Analytical Chemistry 1993 |
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| Übergeordnetes Werk: |
Enthalten in: Analytical sciences - [Cham] : Springer International Publishing, 1985, 9(1993), 1 vom: Feb., Seite 29-32 |
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| Übergeordnetes Werk: |
volume:9 ; year:1993 ; number:1 ; month:02 ; pages:29-32 |
| Links: |
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| DOI / URN: |
10.2116/analsci.9.29 |
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SPR047560738 |
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| 520 | |a Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. | ||
| 650 | 4 | |a Supercritical fluid extraction |7 (dpeaa)DE-He213 | |
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| 650 | 4 | |a fat-soluble vitamin |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a retinol palmitate |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a tocopherol acetate |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Koike, Shinichi |4 aut | |
| 700 | 1 | |a Handa, Mitsuichi |4 aut | |
| 700 | 1 | |a Sagara, Kazuhiko |4 aut | |
| 700 | 1 | |a Mizutani, Taku |4 aut | |
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10.2116/analsci.9.29 doi (DE-627)SPR047560738 (SPR)analsci.9.29-e DE-627 ger DE-627 rakwb eng Masuda, Mitsuhiro verfasserin aut Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment 1993 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1993 Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 fat-soluble vitamin (dpeaa)DE-He213 retinol palmitate (dpeaa)DE-He213 tocopherol acetate (dpeaa)DE-He213 Koike, Shinichi aut Handa, Mitsuichi aut Sagara, Kazuhiko aut Mizutani, Taku aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 9(1993), 1 vom: Feb., Seite 29-32 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:9 year:1993 number:1 month:02 pages:29-32 https://dx.doi.org/10.2116/analsci.9.29 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 9 1993 1 02 29-32 |
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10.2116/analsci.9.29 doi (DE-627)SPR047560738 (SPR)analsci.9.29-e DE-627 ger DE-627 rakwb eng Masuda, Mitsuhiro verfasserin aut Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment 1993 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1993 Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 fat-soluble vitamin (dpeaa)DE-He213 retinol palmitate (dpeaa)DE-He213 tocopherol acetate (dpeaa)DE-He213 Koike, Shinichi aut Handa, Mitsuichi aut Sagara, Kazuhiko aut Mizutani, Taku aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 9(1993), 1 vom: Feb., Seite 29-32 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:9 year:1993 number:1 month:02 pages:29-32 https://dx.doi.org/10.2116/analsci.9.29 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 9 1993 1 02 29-32 |
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10.2116/analsci.9.29 doi (DE-627)SPR047560738 (SPR)analsci.9.29-e DE-627 ger DE-627 rakwb eng Masuda, Mitsuhiro verfasserin aut Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment 1993 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1993 Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 fat-soluble vitamin (dpeaa)DE-He213 retinol palmitate (dpeaa)DE-He213 tocopherol acetate (dpeaa)DE-He213 Koike, Shinichi aut Handa, Mitsuichi aut Sagara, Kazuhiko aut Mizutani, Taku aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 9(1993), 1 vom: Feb., Seite 29-32 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:9 year:1993 number:1 month:02 pages:29-32 https://dx.doi.org/10.2116/analsci.9.29 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 9 1993 1 02 29-32 |
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10.2116/analsci.9.29 doi (DE-627)SPR047560738 (SPR)analsci.9.29-e DE-627 ger DE-627 rakwb eng Masuda, Mitsuhiro verfasserin aut Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment 1993 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1993 Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 fat-soluble vitamin (dpeaa)DE-He213 retinol palmitate (dpeaa)DE-He213 tocopherol acetate (dpeaa)DE-He213 Koike, Shinichi aut Handa, Mitsuichi aut Sagara, Kazuhiko aut Mizutani, Taku aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 9(1993), 1 vom: Feb., Seite 29-32 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:9 year:1993 number:1 month:02 pages:29-32 https://dx.doi.org/10.2116/analsci.9.29 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 9 1993 1 02 29-32 |
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10.2116/analsci.9.29 doi (DE-627)SPR047560738 (SPR)analsci.9.29-e DE-627 ger DE-627 rakwb eng Masuda, Mitsuhiro verfasserin aut Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment 1993 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1993 Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 fat-soluble vitamin (dpeaa)DE-He213 retinol palmitate (dpeaa)DE-He213 tocopherol acetate (dpeaa)DE-He213 Koike, Shinichi aut Handa, Mitsuichi aut Sagara, Kazuhiko aut Mizutani, Taku aut Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 9(1993), 1 vom: Feb., Seite 29-32 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:9 year:1993 number:1 month:02 pages:29-32 https://dx.doi.org/10.2116/analsci.9.29 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 9 1993 1 02 29-32 |
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Masuda, Mitsuhiro @@aut@@ Koike, Shinichi @@aut@@ Handa, Mitsuichi @@aut@@ Sagara, Kazuhiko @@aut@@ Mizutani, Taku @@aut@@ |
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Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 fat-soluble vitamin (dpeaa)DE-He213 retinol palmitate (dpeaa)DE-He213 tocopherol acetate (dpeaa)DE-He213 |
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Application of Supercritical Fluid Extraction and Chromatography to Assay Fat-Soluble Vitamins in Hydrophobic Ointment |
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Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. © The Japan Society for Analytical Chemistry 1993 |
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Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. © The Japan Society for Analytical Chemistry 1993 |
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Abstract The determination of retinol palmitate and tocopherol acetate in a hydrophobic ointment by a coupled supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) system is described. The ointment, triturated with diatomaceous earth powder, was subjected to SFE with carbon dioxide, and the extract containing fat-soluble vitamins was trapped on a trimethylsilyl silica-gel column by reducing the fluid pressure. The trapped components were analyzed on an octadecylsilyl silica-gel column by SFC using carbon dioxide containing ethanol as a mobile phase and UV absorption monitoring at 284 nm. In this method, retinol palmitate and tocopherol acetate in preparations could be determined within ten minutes without any manual products after placing the sample into the system. © The Japan Society for Analytical Chemistry 1993 |
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code="h">29-32</subfield></datafield></record></collection>
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| score |
7.397253 |