Thermal behavior and pyrolysis kinetics of olive stone residue

Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their or...
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Autor*in:	Asimakidou, T. [verfasserIn] Chrissafis, K.

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2022

Schlagwörter:	Pyrolysis Olive stone residues Thermogravimetric analysis Kinetic analysis

Anmerkung:	© Akadémiai Kiadó, Budapest, Hungary 2021

Übergeordnetes Werk:	Enthalten in: Journal of thermal analysis and calorimetry - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969, 147(2022), 16 vom: 22. Jan., Seite 9045-9054
Übergeordnetes Werk:	volume:147 ; year:2022 ; number:16 ; day:22 ; month:01 ; pages:9045-9054

Links:	Volltext

DOI / URN:	10.1007/s10973-021-11163-w

Katalog-ID:	SPR047572477

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245	1	0	\|a Thermal behavior and pyrolysis kinetics of olive stone residue
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520			\|a Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation.
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allfields	10.1007/s10973-021-11163-w doi (DE-627)SPR047572477 (SPR)s10973-021-11163-w-e DE-627 ger DE-627 rakwb eng Asimakidou, T. verfasserin aut Thermal behavior and pyrolysis kinetics of olive stone residue 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2021 Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. Pyrolysis (dpeaa)DE-He213 Olive stone residues (dpeaa)DE-He213 Thermogravimetric analysis (dpeaa)DE-He213 Kinetic analysis (dpeaa)DE-He213 Chrissafis, K. aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 16 vom: 22. Jan., Seite 9045-9054 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054 https://dx.doi.org/10.1007/s10973-021-11163-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 16 22 01 9045-9054
spelling	10.1007/s10973-021-11163-w doi (DE-627)SPR047572477 (SPR)s10973-021-11163-w-e DE-627 ger DE-627 rakwb eng Asimakidou, T. verfasserin aut Thermal behavior and pyrolysis kinetics of olive stone residue 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2021 Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. Pyrolysis (dpeaa)DE-He213 Olive stone residues (dpeaa)DE-He213 Thermogravimetric analysis (dpeaa)DE-He213 Kinetic analysis (dpeaa)DE-He213 Chrissafis, K. aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 16 vom: 22. Jan., Seite 9045-9054 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054 https://dx.doi.org/10.1007/s10973-021-11163-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 16 22 01 9045-9054
allfields_unstemmed	10.1007/s10973-021-11163-w doi (DE-627)SPR047572477 (SPR)s10973-021-11163-w-e DE-627 ger DE-627 rakwb eng Asimakidou, T. verfasserin aut Thermal behavior and pyrolysis kinetics of olive stone residue 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2021 Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. Pyrolysis (dpeaa)DE-He213 Olive stone residues (dpeaa)DE-He213 Thermogravimetric analysis (dpeaa)DE-He213 Kinetic analysis (dpeaa)DE-He213 Chrissafis, K. aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 16 vom: 22. Jan., Seite 9045-9054 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054 https://dx.doi.org/10.1007/s10973-021-11163-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 16 22 01 9045-9054
allfieldsGer	10.1007/s10973-021-11163-w doi (DE-627)SPR047572477 (SPR)s10973-021-11163-w-e DE-627 ger DE-627 rakwb eng Asimakidou, T. verfasserin aut Thermal behavior and pyrolysis kinetics of olive stone residue 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2021 Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. Pyrolysis (dpeaa)DE-He213 Olive stone residues (dpeaa)DE-He213 Thermogravimetric analysis (dpeaa)DE-He213 Kinetic analysis (dpeaa)DE-He213 Chrissafis, K. aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 16 vom: 22. Jan., Seite 9045-9054 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054 https://dx.doi.org/10.1007/s10973-021-11163-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 16 22 01 9045-9054
allfieldsSound	10.1007/s10973-021-11163-w doi (DE-627)SPR047572477 (SPR)s10973-021-11163-w-e DE-627 ger DE-627 rakwb eng Asimakidou, T. verfasserin aut Thermal behavior and pyrolysis kinetics of olive stone residue 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2021 Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. Pyrolysis (dpeaa)DE-He213 Olive stone residues (dpeaa)DE-He213 Thermogravimetric analysis (dpeaa)DE-He213 Kinetic analysis (dpeaa)DE-He213 Chrissafis, K. aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 16 vom: 22. Jan., Seite 9045-9054 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054 https://dx.doi.org/10.1007/s10973-021-11163-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 16 22 01 9045-9054
language	English
source	Enthalten in Journal of thermal analysis and calorimetry 147(2022), 16 vom: 22. Jan., Seite 9045-9054 volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054
sourceStr	Enthalten in Journal of thermal analysis and calorimetry 147(2022), 16 vom: 22. Jan., Seite 9045-9054 volume:147 year:2022 number:16 day:22 month:01 pages:9045-9054
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Pyrolysis Olive stone residues Thermogravimetric analysis Kinetic analysis
isfreeaccess_bool	false
container_title	Journal of thermal analysis and calorimetry
authorswithroles_txt_mv	Asimakidou, T. @@aut@@ Chrissafis, K. @@aut@@
publishDateDaySort_date	2022-01-22T00:00:00Z
hierarchy_top_id	315295422
id	SPR047572477
language_de	englisch
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author	Asimakidou, T.
spellingShingle	Asimakidou, T. misc Pyrolysis misc Olive stone residues misc Thermogravimetric analysis misc Kinetic analysis Thermal behavior and pyrolysis kinetics of olive stone residue
authorStr	Asimakidou, T.
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topic_title	Thermal behavior and pyrolysis kinetics of olive stone residue Pyrolysis (dpeaa)DE-He213 Olive stone residues (dpeaa)DE-He213 Thermogravimetric analysis (dpeaa)DE-He213 Kinetic analysis (dpeaa)DE-He213
topic	misc Pyrolysis misc Olive stone residues misc Thermogravimetric analysis misc Kinetic analysis
topic_unstemmed	misc Pyrolysis misc Olive stone residues misc Thermogravimetric analysis misc Kinetic analysis
topic_browse	misc Pyrolysis misc Olive stone residues misc Thermogravimetric analysis misc Kinetic analysis
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title	Thermal behavior and pyrolysis kinetics of olive stone residue
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title_full	Thermal behavior and pyrolysis kinetics of olive stone residue
author_sort	Asimakidou, T.
journal	Journal of thermal analysis and calorimetry
journalStr	Journal of thermal analysis and calorimetry
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author_browse	Asimakidou, T. Chrissafis, K.
container_volume	147
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author-letter	Asimakidou, T.
doi_str_mv	10.1007/s10973-021-11163-w
title_sort	thermal behavior and pyrolysis kinetics of olive stone residue
title_auth	Thermal behavior and pyrolysis kinetics of olive stone residue
abstract	Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. © Akadémiai Kiadó, Budapest, Hungary 2021
abstractGer	Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. © Akadémiai Kiadó, Budapest, Hungary 2021
abstract_unstemmed	Abstract In the last decades, one of the most ordinary challenges that countries of Southern Europe face is the management of wastes and by-products of olive oil production activities which are disposed into the environment and contribute to the enhancement of major ecological issues due to their organic loads. Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation. © Akadémiai Kiadó, Budapest, Hungary 2021
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container_issue	16
title_short	Thermal behavior and pyrolysis kinetics of olive stone residue
url	https://dx.doi.org/10.1007/s10973-021-11163-w
remote_bool	true
author2	Chrissafis, K.
author2Str	Chrissafis, K.
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doi_str	10.1007/s10973-021-11163-w
up_date	2024-07-03T13:36:47.058Z
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Exploitation of these olive residues wastes by thermochemical treatment has been proved a very popular way to generate a wide range of valuable products. In this concept, this work studies the thermal decomposition process of olive stone samples using thermogravimetric analysis (TGA) data obtained under inert atmosphere at various heating rates (5–20 °C) and their kinetic analysis conducted via model-free and model fitting methods. The changes in the crystal structure for various pyrolysis temperatures of the sample were examined by X-ray diffraction analysis (XRD), while the morphological characteristics were examined by scanning electron microscopy (SEM). Results indicated that the thermal behavior of olive stone sample was a typical one for a lignocellulosic material with the first mass loss being attributed to moisture removal while the following stages were assigned to lignocellulosic degradation substances. Vyazovkin (VYA) isoconversional method was performed to estimate effective activation energy (Ea) and the pre-exponential factor, while using a model fitting method the best fitting results were obtained by a three independent parallel reactions model, obeying the nth order with Fn code and described by the f(α) = (1 − α)n equation.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pyrolysis</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Olive stone residues</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Thermogravimetric analysis</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Kinetic analysis</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Chrissafis, K.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of thermal analysis and calorimetry</subfield><subfield code="d">Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969</subfield><subfield code="g">147(2022), 16 vom: 22. Jan., Seite 9045-9054</subfield><subfield code="w">(DE-627)315295422</subfield><subfield code="w">(DE-600)2017304-0</subfield><subfield code="x">1572-8943</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:147</subfield><subfield code="g">year:2022</subfield><subfield code="g">number:16</subfield><subfield code="g">day:22</subfield><subfield code="g">month:01</subfield><subfield code="g">pages:9045-9054</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://dx.doi.org/10.1007/s10973-021-11163-w</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_SPRINGER</subfield></datafield><datafield 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Thermal behavior and pyrolysis kinetics of olive stone residue

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