Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor
Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ramírez-Ortega, Jorge Alberto [verfasserIn] Rodríguez-Betancourtt, Verónica María |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990, 33(2022), 23 vom: 15. Juli, Seite 18268-18283 |
|---|---|
| Übergeordnetes Werk: |
volume:33 ; year:2022 ; number:23 ; day:15 ; month:07 ; pages:18268-18283 |
| Links: |
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| DOI / URN: |
10.1007/s10854-022-08683-y |
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| Katalog-ID: |
SPR047779411 |
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| 100 | 1 | |a Ramírez-Ortega, Jorge Alberto |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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| 520 | |a Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. | ||
| 700 | 1 | |a Guillén-Bonilla, Héctor |0 (orcid)0000-0003-2202-9819 |4 aut | |
| 700 | 1 | |a Guillén-Bonilla, Alex |4 aut | |
| 700 | 1 | |a Rodríguez-Betancourtt, Verónica María |4 aut | |
| 700 | 1 | |a Sánchez-Martínez, A. |4 aut | |
| 700 | 1 | |a Guillén-Bonilla, José Trinidad |4 aut | |
| 700 | 1 | |a Gildo-Ortiz, Lorenzo |4 aut | |
| 700 | 1 | |a Huízar-Padilla, Emilio |4 aut | |
| 700 | 1 | |a Reyes-Gómez, Juan |4 aut | |
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10.1007/s10854-022-08683-y doi (DE-627)SPR047779411 (SPR)s10854-022-08683-y-e DE-627 ger DE-627 rakwb eng Ramírez-Ortega, Jorge Alberto verfasserin aut Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. Guillén-Bonilla, Héctor (orcid)0000-0003-2202-9819 aut Guillén-Bonilla, Alex aut Rodríguez-Betancourtt, Verónica María aut Sánchez-Martínez, A. aut Guillén-Bonilla, José Trinidad aut Gildo-Ortiz, Lorenzo aut Huízar-Padilla, Emilio aut Reyes-Gómez, Juan aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990 33(2022), 23 vom: 15. Juli, Seite 18268-18283 (DE-627)317827154 (DE-600)2016994-2 1573-482X nnns volume:33 year:2022 number:23 day:15 month:07 pages:18268-18283 https://dx.doi.org/10.1007/s10854-022-08683-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 33 2022 23 15 07 18268-18283 |
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10.1007/s10854-022-08683-y doi (DE-627)SPR047779411 (SPR)s10854-022-08683-y-e DE-627 ger DE-627 rakwb eng Ramírez-Ortega, Jorge Alberto verfasserin aut Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. Guillén-Bonilla, Héctor (orcid)0000-0003-2202-9819 aut Guillén-Bonilla, Alex aut Rodríguez-Betancourtt, Verónica María aut Sánchez-Martínez, A. aut Guillén-Bonilla, José Trinidad aut Gildo-Ortiz, Lorenzo aut Huízar-Padilla, Emilio aut Reyes-Gómez, Juan aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990 33(2022), 23 vom: 15. Juli, Seite 18268-18283 (DE-627)317827154 (DE-600)2016994-2 1573-482X nnns volume:33 year:2022 number:23 day:15 month:07 pages:18268-18283 https://dx.doi.org/10.1007/s10854-022-08683-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 33 2022 23 15 07 18268-18283 |
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10.1007/s10854-022-08683-y doi (DE-627)SPR047779411 (SPR)s10854-022-08683-y-e DE-627 ger DE-627 rakwb eng Ramírez-Ortega, Jorge Alberto verfasserin aut Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. Guillén-Bonilla, Héctor (orcid)0000-0003-2202-9819 aut Guillén-Bonilla, Alex aut Rodríguez-Betancourtt, Verónica María aut Sánchez-Martínez, A. aut Guillén-Bonilla, José Trinidad aut Gildo-Ortiz, Lorenzo aut Huízar-Padilla, Emilio aut Reyes-Gómez, Juan aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990 33(2022), 23 vom: 15. Juli, Seite 18268-18283 (DE-627)317827154 (DE-600)2016994-2 1573-482X nnns volume:33 year:2022 number:23 day:15 month:07 pages:18268-18283 https://dx.doi.org/10.1007/s10854-022-08683-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 33 2022 23 15 07 18268-18283 |
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10.1007/s10854-022-08683-y doi (DE-627)SPR047779411 (SPR)s10854-022-08683-y-e DE-627 ger DE-627 rakwb eng Ramírez-Ortega, Jorge Alberto verfasserin aut Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. Guillén-Bonilla, Héctor (orcid)0000-0003-2202-9819 aut Guillén-Bonilla, Alex aut Rodríguez-Betancourtt, Verónica María aut Sánchez-Martínez, A. aut Guillén-Bonilla, José Trinidad aut Gildo-Ortiz, Lorenzo aut Huízar-Padilla, Emilio aut Reyes-Gómez, Juan aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990 33(2022), 23 vom: 15. Juli, Seite 18268-18283 (DE-627)317827154 (DE-600)2016994-2 1573-482X nnns volume:33 year:2022 number:23 day:15 month:07 pages:18268-18283 https://dx.doi.org/10.1007/s10854-022-08683-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 33 2022 23 15 07 18268-18283 |
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10.1007/s10854-022-08683-y doi (DE-627)SPR047779411 (SPR)s10854-022-08683-y-e DE-627 ger DE-627 rakwb eng Ramírez-Ortega, Jorge Alberto verfasserin aut Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. Guillén-Bonilla, Héctor (orcid)0000-0003-2202-9819 aut Guillén-Bonilla, Alex aut Rodríguez-Betancourtt, Verónica María aut Sánchez-Martínez, A. aut Guillén-Bonilla, José Trinidad aut Gildo-Ortiz, Lorenzo aut Huízar-Padilla, Emilio aut Reyes-Gómez, Juan aut Enthalten in Journal of materials science Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990 33(2022), 23 vom: 15. Juli, Seite 18268-18283 (DE-627)317827154 (DE-600)2016994-2 1573-482X nnns volume:33 year:2022 number:23 day:15 month:07 pages:18268-18283 https://dx.doi.org/10.1007/s10854-022-08683-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 33 2022 23 15 07 18268-18283 |
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Ramírez-Ortega, Jorge Alberto @@aut@@ Guillén-Bonilla, Héctor @@aut@@ Guillén-Bonilla, Alex @@aut@@ Rodríguez-Betancourtt, Verónica María @@aut@@ Sánchez-Martínez, A. @@aut@@ Guillén-Bonilla, José Trinidad @@aut@@ Gildo-Ortiz, Lorenzo @@aut@@ Huízar-Padilla, Emilio @@aut@@ Reyes-Gómez, Juan @@aut@@ |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR047779411</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230508011912.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">220807s2022 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10854-022-08683-y</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR047779411</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10854-022-08683-y-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Ramírez-Ortega, Jorge Alberto</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2022</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor.</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Guillén-Bonilla, Héctor</subfield><subfield code="0">(orcid)0000-0003-2202-9819</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Guillén-Bonilla, Alex</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Rodríguez-Betancourtt, Verónica María</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sánchez-Martínez, A.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Guillén-Bonilla, José Trinidad</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Gildo-Ortiz, Lorenzo</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Huízar-Padilla, Emilio</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Reyes-Gómez, Juan</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of materials science</subfield><subfield code="d">Dordrecht [u.a.] : Springer Science + Business Media B.V, 1990</subfield><subfield code="g">33(2022), 23 vom: 15. 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Ramírez-Ortega, Jorge Alberto |
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Ramírez-Ortega, Jorge Alberto Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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Ramírez-Ortega, Jorge Alberto Guillén-Bonilla, Héctor Guillén-Bonilla, Alex Rodríguez-Betancourtt, Verónica María Sánchez-Martínez, A. Guillén-Bonilla, José Trinidad Gildo-Ortiz, Lorenzo Huízar-Padilla, Emilio Reyes-Gómez, Juan |
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synthesis of the oxide $ nisb_{2} %$ o_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
| abstract |
Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
| abstractGer |
Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
| abstract_unstemmed |
Abstract In this work, nanoparticles of the trirutile-type oxide $ NiSb_{2} %$ O_{6} $ were synthesized for its application as a gas sensor using the colloidal method assisted by microwave radiation. The crystalline evolution of the powders was analyzed by X-ray diffraction, finding the phase $ NiSb_{2} %$ O_{6} $ at 600 °C. SEM micrographs revealed the growth of microspheres, microrods, and irregularly shaped particles. Using TEM, the average size of the nanoparticles was calculated at ~ 17.1 nm. For dynamic tests, pellets and thick films were made from the powders calcined at 600 °C. For the thick films, alternating current was used at frequencies of 0.1 and 1 kHz in $ C_{3} %$ H_{8} $ and $ CO_{2} $ atmospheres at 360 °C, where the material’s sensitivity magnitude in $ CO_{2} $ was ~ 2.61% (0.1 kHz) and ~ 2.97% (1 kHz). In contrast, for $ C_{3} %$ H_{8} $, the sensitivity was ~ 6.69% (0.1 kHz) and ~ 5.12% (1 kHz) on average. For the pellets, direct current signals and volumetric flow rates of 100, 150, and 200 $ cm^{3} $/min of CO at 200 °C were applied, where the sensitivities were ~ 24.37, ~ 35.33, and ~ 40.77%, respectively. In each test, the sensitivity visibly increased when the gases were injected. Likewise, the response and recovery times decreased when the frequency and gas concentration increased. The results obtained for the trirutile-type oxide $ NiSb_{2} %$ O_{6} $, which showed good stability, efficiency, and high sensitivity in $ CO_{2} $, $ C_{3} %$ H_{8} $, and CO atmospheres, make it ideal as a toxic gas sensor. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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| title_short |
Synthesis of the oxide $ NiSb_{2} %$ O_{6} $ and its electrical characterization in toxic atmospheres for its application as a gas sensor |
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https://dx.doi.org/10.1007/s10854-022-08683-y |
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Guillén-Bonilla, Héctor Guillén-Bonilla, Alex Rodríguez-Betancourtt, Verónica María Sánchez-Martínez, A. Guillén-Bonilla, José Trinidad Gildo-Ortiz, Lorenzo Huízar-Padilla, Emilio Reyes-Gómez, Juan |
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Guillén-Bonilla, Héctor Guillén-Bonilla, Alex Rodríguez-Betancourtt, Verónica María Sánchez-Martínez, A. Guillén-Bonilla, José Trinidad Gildo-Ortiz, Lorenzo Huízar-Padilla, Emilio Reyes-Gómez, Juan |
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10.1007/s10854-022-08683-y |
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2024-07-03T14:56:10.727Z |
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| score |
7.399727 |