A Novel Rapid Pyrolysis of Non-fluorine MOD-Derived YBCO Thin Films
Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than...
Ausführliche Beschreibung
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| Autor*in: |
Yang, Zhao [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
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| Anmerkung: |
© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of superconductivity - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988, 35(2022), 10 vom: 29. Juni, Seite 2699-2707 |
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| Übergeordnetes Werk: |
volume:35 ; year:2022 ; number:10 ; day:29 ; month:06 ; pages:2699-2707 |
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| DOI / URN: |
10.1007/s10948-022-06323-4 |
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| 520 | |a Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). | ||
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10.1007/s10948-022-06323-4 doi (DE-627)SPR048112194 (SPR)s10948-022-06323-4-e DE-627 ger DE-627 rakwb eng Yang, Zhao verfasserin (orcid)0000-0003-1627-7912 aut A Novel Rapid Pyrolysis of Non-fluorine MOD-Derived YBCO Thin Films 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). YBCO film (dpeaa)DE-He213 MOD (dpeaa)DE-He213 Low-vacuum (dpeaa)DE-He213 Rapid pyrolysis (dpeaa)DE-He213 Critical current density (dpeaa)DE-He213 Chu, Ningdong aut Tong, Shuyun aut Lu, Yuming aut Liu, Zhiyong aut Cai, Chuanbing aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 35(2022), 10 vom: 29. Juni, Seite 2699-2707 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:35 year:2022 number:10 day:29 month:06 pages:2699-2707 https://dx.doi.org/10.1007/s10948-022-06323-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 AR 35 2022 10 29 06 2699-2707 |
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10.1007/s10948-022-06323-4 doi (DE-627)SPR048112194 (SPR)s10948-022-06323-4-e DE-627 ger DE-627 rakwb eng Yang, Zhao verfasserin (orcid)0000-0003-1627-7912 aut A Novel Rapid Pyrolysis of Non-fluorine MOD-Derived YBCO Thin Films 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). YBCO film (dpeaa)DE-He213 MOD (dpeaa)DE-He213 Low-vacuum (dpeaa)DE-He213 Rapid pyrolysis (dpeaa)DE-He213 Critical current density (dpeaa)DE-He213 Chu, Ningdong aut Tong, Shuyun aut Lu, Yuming aut Liu, Zhiyong aut Cai, Chuanbing aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 35(2022), 10 vom: 29. Juni, Seite 2699-2707 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:35 year:2022 number:10 day:29 month:06 pages:2699-2707 https://dx.doi.org/10.1007/s10948-022-06323-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 AR 35 2022 10 29 06 2699-2707 |
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10.1007/s10948-022-06323-4 doi (DE-627)SPR048112194 (SPR)s10948-022-06323-4-e DE-627 ger DE-627 rakwb eng Yang, Zhao verfasserin (orcid)0000-0003-1627-7912 aut A Novel Rapid Pyrolysis of Non-fluorine MOD-Derived YBCO Thin Films 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). YBCO film (dpeaa)DE-He213 MOD (dpeaa)DE-He213 Low-vacuum (dpeaa)DE-He213 Rapid pyrolysis (dpeaa)DE-He213 Critical current density (dpeaa)DE-He213 Chu, Ningdong aut Tong, Shuyun aut Lu, Yuming aut Liu, Zhiyong aut Cai, Chuanbing aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 35(2022), 10 vom: 29. Juni, Seite 2699-2707 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:35 year:2022 number:10 day:29 month:06 pages:2699-2707 https://dx.doi.org/10.1007/s10948-022-06323-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 AR 35 2022 10 29 06 2699-2707 |
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10.1007/s10948-022-06323-4 doi (DE-627)SPR048112194 (SPR)s10948-022-06323-4-e DE-627 ger DE-627 rakwb eng Yang, Zhao verfasserin (orcid)0000-0003-1627-7912 aut A Novel Rapid Pyrolysis of Non-fluorine MOD-Derived YBCO Thin Films 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). YBCO film (dpeaa)DE-He213 MOD (dpeaa)DE-He213 Low-vacuum (dpeaa)DE-He213 Rapid pyrolysis (dpeaa)DE-He213 Critical current density (dpeaa)DE-He213 Chu, Ningdong aut Tong, Shuyun aut Lu, Yuming aut Liu, Zhiyong aut Cai, Chuanbing aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 35(2022), 10 vom: 29. Juni, Seite 2699-2707 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:35 year:2022 number:10 day:29 month:06 pages:2699-2707 https://dx.doi.org/10.1007/s10948-022-06323-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 AR 35 2022 10 29 06 2699-2707 |
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10.1007/s10948-022-06323-4 doi (DE-627)SPR048112194 (SPR)s10948-022-06323-4-e DE-627 ger DE-627 rakwb eng Yang, Zhao verfasserin (orcid)0000-0003-1627-7912 aut A Novel Rapid Pyrolysis of Non-fluorine MOD-Derived YBCO Thin Films 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). YBCO film (dpeaa)DE-He213 MOD (dpeaa)DE-He213 Low-vacuum (dpeaa)DE-He213 Rapid pyrolysis (dpeaa)DE-He213 Critical current density (dpeaa)DE-He213 Chu, Ningdong aut Tong, Shuyun aut Lu, Yuming aut Liu, Zhiyong aut Cai, Chuanbing aut Enthalten in Journal of superconductivity Dordrecht [u.a.] : Springer Science + Business Media B.V., 1988 35(2022), 10 vom: 29. Juni, Seite 2699-2707 (DE-627)313651175 (DE-600)2000540-4 1572-9605 nnns volume:35 year:2022 number:10 day:29 month:06 pages:2699-2707 https://dx.doi.org/10.1007/s10948-022-06323-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_152 GBV_ILN_161 GBV_ILN_171 GBV_ILN_187 GBV_ILN_224 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 AR 35 2022 10 29 06 2699-2707 |
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Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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Abstract A novel rapid pyrolysis method at 5 Pa with argon as background gas was proposed to prepare $ YBa_{2} %$ Cu_{3} %$ O_{7-δ} $ (YBCO) films by non-fluorine metal organic solution deposition (MOD). The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. The results of both Raman and X-ray spectra show that the c-axis growth is superior to the a-axis growth, leading to a better critical current density Jc of 1.3 MA/$ cm^{2} $ (77 K, self-field). © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022 |
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The YBCO sol–gel films were pyrolyzed about 29 min, warm up from 20 to 600 ℃, which is less than the one-twentieth of conventional pyrolysis time for non-fluorine MOD processing. The influence of the low-vacuum and the rapid decomposition on the microstructures of YBCO precursor films were investigated, while the high-temperature firing process was further optimized for epitaxially grown YBCO films. The results show that most of the defects generated in the low-vacuum processing can be eliminated nearly by increasing firing time up to 60 min, and finally the textured YBCO films with denser and smoother morphologies were obtained. 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