Thermal behavior of griseofulvin: fusion, sublimation and vaporization
The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Blokhina, Svetlana [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2022 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969, 147(2022), 20 vom: 15. Apr., Seite 11195-11204 |
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| Übergeordnetes Werk: |
volume:147 ; year:2022 ; number:20 ; day:15 ; month:04 ; pages:11195-11204 |
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| DOI / URN: |
10.1007/s10973-022-11329-0 |
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| Katalog-ID: |
SPR048144746 |
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| 100 | 1 | |a Blokhina, Svetlana |e verfasserin |0 (orcid)0000-0003-3492-6808 |4 aut | |
| 245 | 1 | 0 | |a Thermal behavior of griseofulvin: fusion, sublimation and vaporization |
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| 520 | |a The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract | ||
| 650 | 4 | |a Antifungal drug |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Fusion parameters |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Vapor pressure |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Sublimation enthalpy |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Vaporization enthalpy |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a Thermodynamics |7 (dpeaa)DE-He213 | |
| 700 | 1 | |a Sharapova, Angelica |0 (orcid)0000-0003-3883-3190 |4 aut | |
| 700 | 1 | |a Ol’khovich, Marina |0 (orcid)0000-0003-2680-240X |4 aut | |
| 700 | 1 | |a Perlovich, German |0 (orcid)0000-0002-6267-5244 |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Journal of thermal analysis and calorimetry |d Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 |g 147(2022), 20 vom: 15. Apr., Seite 11195-11204 |w (DE-627)315295422 |w (DE-600)2017304-0 |x 1572-8943 |7 nnns |
| 773 | 1 | 8 | |g volume:147 |g year:2022 |g number:20 |g day:15 |g month:04 |g pages:11195-11204 |
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10.1007/s10973-022-11329-0 doi (DE-627)SPR048144746 (SPR)s10973-022-11329-0-e DE-627 ger DE-627 rakwb eng Blokhina, Svetlana verfasserin (orcid)0000-0003-3492-6808 aut Thermal behavior of griseofulvin: fusion, sublimation and vaporization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022 The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract Antifungal drug (dpeaa)DE-He213 Fusion parameters (dpeaa)DE-He213 Vapor pressure (dpeaa)DE-He213 Sublimation enthalpy (dpeaa)DE-He213 Vaporization enthalpy (dpeaa)DE-He213 Thermodynamics (dpeaa)DE-He213 Sharapova, Angelica (orcid)0000-0003-3883-3190 aut Ol’khovich, Marina (orcid)0000-0003-2680-240X aut Perlovich, German (orcid)0000-0002-6267-5244 aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 20 vom: 15. Apr., Seite 11195-11204 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 https://dx.doi.org/10.1007/s10973-022-11329-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 20 15 04 11195-11204 |
| spelling |
10.1007/s10973-022-11329-0 doi (DE-627)SPR048144746 (SPR)s10973-022-11329-0-e DE-627 ger DE-627 rakwb eng Blokhina, Svetlana verfasserin (orcid)0000-0003-3492-6808 aut Thermal behavior of griseofulvin: fusion, sublimation and vaporization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022 The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract Antifungal drug (dpeaa)DE-He213 Fusion parameters (dpeaa)DE-He213 Vapor pressure (dpeaa)DE-He213 Sublimation enthalpy (dpeaa)DE-He213 Vaporization enthalpy (dpeaa)DE-He213 Thermodynamics (dpeaa)DE-He213 Sharapova, Angelica (orcid)0000-0003-3883-3190 aut Ol’khovich, Marina (orcid)0000-0003-2680-240X aut Perlovich, German (orcid)0000-0002-6267-5244 aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 20 vom: 15. Apr., Seite 11195-11204 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 https://dx.doi.org/10.1007/s10973-022-11329-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 20 15 04 11195-11204 |
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10.1007/s10973-022-11329-0 doi (DE-627)SPR048144746 (SPR)s10973-022-11329-0-e DE-627 ger DE-627 rakwb eng Blokhina, Svetlana verfasserin (orcid)0000-0003-3492-6808 aut Thermal behavior of griseofulvin: fusion, sublimation and vaporization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022 The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract Antifungal drug (dpeaa)DE-He213 Fusion parameters (dpeaa)DE-He213 Vapor pressure (dpeaa)DE-He213 Sublimation enthalpy (dpeaa)DE-He213 Vaporization enthalpy (dpeaa)DE-He213 Thermodynamics (dpeaa)DE-He213 Sharapova, Angelica (orcid)0000-0003-3883-3190 aut Ol’khovich, Marina (orcid)0000-0003-2680-240X aut Perlovich, German (orcid)0000-0002-6267-5244 aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 20 vom: 15. Apr., Seite 11195-11204 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 https://dx.doi.org/10.1007/s10973-022-11329-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 20 15 04 11195-11204 |
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10.1007/s10973-022-11329-0 doi (DE-627)SPR048144746 (SPR)s10973-022-11329-0-e DE-627 ger DE-627 rakwb eng Blokhina, Svetlana verfasserin (orcid)0000-0003-3492-6808 aut Thermal behavior of griseofulvin: fusion, sublimation and vaporization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022 The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract Antifungal drug (dpeaa)DE-He213 Fusion parameters (dpeaa)DE-He213 Vapor pressure (dpeaa)DE-He213 Sublimation enthalpy (dpeaa)DE-He213 Vaporization enthalpy (dpeaa)DE-He213 Thermodynamics (dpeaa)DE-He213 Sharapova, Angelica (orcid)0000-0003-3883-3190 aut Ol’khovich, Marina (orcid)0000-0003-2680-240X aut Perlovich, German (orcid)0000-0002-6267-5244 aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 20 vom: 15. Apr., Seite 11195-11204 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 https://dx.doi.org/10.1007/s10973-022-11329-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 20 15 04 11195-11204 |
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10.1007/s10973-022-11329-0 doi (DE-627)SPR048144746 (SPR)s10973-022-11329-0-e DE-627 ger DE-627 rakwb eng Blokhina, Svetlana verfasserin (orcid)0000-0003-3492-6808 aut Thermal behavior of griseofulvin: fusion, sublimation and vaporization 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022 The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract Antifungal drug (dpeaa)DE-He213 Fusion parameters (dpeaa)DE-He213 Vapor pressure (dpeaa)DE-He213 Sublimation enthalpy (dpeaa)DE-He213 Vaporization enthalpy (dpeaa)DE-He213 Thermodynamics (dpeaa)DE-He213 Sharapova, Angelica (orcid)0000-0003-3883-3190 aut Ol’khovich, Marina (orcid)0000-0003-2680-240X aut Perlovich, German (orcid)0000-0002-6267-5244 aut Enthalten in Journal of thermal analysis and calorimetry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1969 147(2022), 20 vom: 15. Apr., Seite 11195-11204 (DE-627)315295422 (DE-600)2017304-0 1572-8943 nnns volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 https://dx.doi.org/10.1007/s10973-022-11329-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 147 2022 20 15 04 11195-11204 |
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Enthalten in Journal of thermal analysis and calorimetry 147(2022), 20 vom: 15. Apr., Seite 11195-11204 volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 |
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Enthalten in Journal of thermal analysis and calorimetry 147(2022), 20 vom: 15. Apr., Seite 11195-11204 volume:147 year:2022 number:20 day:15 month:04 pages:11195-11204 |
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Antifungal drug Fusion parameters Vapor pressure Sublimation enthalpy Vaporization enthalpy Thermodynamics |
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Journal of thermal analysis and calorimetry |
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Blokhina, Svetlana @@aut@@ Sharapova, Angelica @@aut@@ Ol’khovich, Marina @@aut@@ Perlovich, German @@aut@@ |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">SPR048144746</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230519191317.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">220920s2022 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10973-022-11329-0</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR048144746</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s10973-022-11329-0-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Blokhina, Svetlana</subfield><subfield code="e">verfasserin</subfield><subfield code="0">(orcid)0000-0003-3492-6808</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Thermal behavior of griseofulvin: fusion, sublimation and vaporization</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2022</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Akadémiai Kiadó, Budapest, Hungary 2022</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. 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Blokhina, Svetlana |
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Thermal behavior of griseofulvin: fusion, sublimation and vaporization Antifungal drug (dpeaa)DE-He213 Fusion parameters (dpeaa)DE-He213 Vapor pressure (dpeaa)DE-He213 Sublimation enthalpy (dpeaa)DE-He213 Vaporization enthalpy (dpeaa)DE-He213 Thermodynamics (dpeaa)DE-He213 |
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Blokhina, Svetlana Sharapova, Angelica Ol’khovich, Marina Perlovich, German |
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thermal behavior of griseofulvin: fusion, sublimation and vaporization |
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Thermal behavior of griseofulvin: fusion, sublimation and vaporization |
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The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract © Akadémiai Kiadó, Budapest, Hungary 2022 |
| abstractGer |
The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract © Akadémiai Kiadó, Budapest, Hungary 2022 |
| abstract_unstemmed |
The saturated vapor pressure of the antifungal drug griseofulvin depending on temperature was measured by the transpiration method. The standard molar enthalpy of sublimation of the studied compound calculated from these data is (141.8 ± 1.2) kJ $ mol^{−1} $. Using thermogravimetric techniques, the vaporization enthalpy of drug was determined and the enthalpy of sublimation at reference temperature was calculated. It is shown that the values of this thermodynamic function derived by both these methods are equal within the experimental uncertainty. The space clusterization approach was applied for the estimation of thermodynamic sublimation functions of griseofulvin and structurally related compounds. In addition, the fusion temperature, enthalpy of fusion and heat capacity of the drug were measured by DSC. Graphical abstract © Akadémiai Kiadó, Budapest, Hungary 2022 |
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20 |
| title_short |
Thermal behavior of griseofulvin: fusion, sublimation and vaporization |
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https://dx.doi.org/10.1007/s10973-022-11329-0 |
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| author2 |
Sharapova, Angelica Ol’khovich, Marina Perlovich, German |
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Sharapova, Angelica Ol’khovich, Marina Perlovich, German |
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| doi_str |
10.1007/s10973-022-11329-0 |
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2024-07-03T17:18:06.238Z |
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| score |
7.399419 |