Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis
Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Nishikawa, Yasuhiko [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1991 |
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| Schlagwörter: |
Supercritical fluid extraction |
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| Anmerkung: |
© The Japan Society for Analytical Chemistry 1991 |
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| Übergeordnetes Werk: |
Enthalten in: Analytical sciences - [Cham] : Springer International Publishing, 1985, 7(1991), 4 vom: 01. Aug., Seite 567-572 |
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| Übergeordnetes Werk: |
volume:7 ; year:1991 ; number:4 ; day:01 ; month:08 ; pages:567-572 |
| Links: |
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| DOI / URN: |
10.2116/analsci.7.567 |
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SPR048348074 |
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| 520 | |a Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. | ||
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| 650 | 4 | |a residue analysis |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a filter paper |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a soil |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a crop |7 (dpeaa)DE-He213 | |
| 650 | 4 | |a electronic distribution |7 (dpeaa)DE-He213 | |
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10.2116/analsci.7.567 doi (DE-627)SPR048348074 (SPR)analsci.7.567-e DE-627 ger DE-627 rakwb eng Nishikawa, Yasuhiko verfasserin aut Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis 1991 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1991 Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 residue analysis (dpeaa)DE-He213 filter paper (dpeaa)DE-He213 soil (dpeaa)DE-He213 crop (dpeaa)DE-He213 electronic distribution (dpeaa)DE-He213 Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 7(1991), 4 vom: 01. Aug., Seite 567-572 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:7 year:1991 number:4 day:01 month:08 pages:567-572 https://dx.doi.org/10.2116/analsci.7.567 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 7 1991 4 01 08 567-572 |
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10.2116/analsci.7.567 doi (DE-627)SPR048348074 (SPR)analsci.7.567-e DE-627 ger DE-627 rakwb eng Nishikawa, Yasuhiko verfasserin aut Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis 1991 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1991 Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 residue analysis (dpeaa)DE-He213 filter paper (dpeaa)DE-He213 soil (dpeaa)DE-He213 crop (dpeaa)DE-He213 electronic distribution (dpeaa)DE-He213 Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 7(1991), 4 vom: 01. Aug., Seite 567-572 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:7 year:1991 number:4 day:01 month:08 pages:567-572 https://dx.doi.org/10.2116/analsci.7.567 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 7 1991 4 01 08 567-572 |
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10.2116/analsci.7.567 doi (DE-627)SPR048348074 (SPR)analsci.7.567-e DE-627 ger DE-627 rakwb eng Nishikawa, Yasuhiko verfasserin aut Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis 1991 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1991 Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 residue analysis (dpeaa)DE-He213 filter paper (dpeaa)DE-He213 soil (dpeaa)DE-He213 crop (dpeaa)DE-He213 electronic distribution (dpeaa)DE-He213 Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 7(1991), 4 vom: 01. Aug., Seite 567-572 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:7 year:1991 number:4 day:01 month:08 pages:567-572 https://dx.doi.org/10.2116/analsci.7.567 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 7 1991 4 01 08 567-572 |
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10.2116/analsci.7.567 doi (DE-627)SPR048348074 (SPR)analsci.7.567-e DE-627 ger DE-627 rakwb eng Nishikawa, Yasuhiko verfasserin aut Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis 1991 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1991 Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 residue analysis (dpeaa)DE-He213 filter paper (dpeaa)DE-He213 soil (dpeaa)DE-He213 crop (dpeaa)DE-He213 electronic distribution (dpeaa)DE-He213 Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 7(1991), 4 vom: 01. Aug., Seite 567-572 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:7 year:1991 number:4 day:01 month:08 pages:567-572 https://dx.doi.org/10.2116/analsci.7.567 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 7 1991 4 01 08 567-572 |
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10.2116/analsci.7.567 doi (DE-627)SPR048348074 (SPR)analsci.7.567-e DE-627 ger DE-627 rakwb eng Nishikawa, Yasuhiko verfasserin aut Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis 1991 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Japan Society for Analytical Chemistry 1991 Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 residue analysis (dpeaa)DE-He213 filter paper (dpeaa)DE-He213 soil (dpeaa)DE-He213 crop (dpeaa)DE-He213 electronic distribution (dpeaa)DE-He213 Enthalten in Analytical sciences [Cham] : Springer International Publishing, 1985 7(1991), 4 vom: 01. Aug., Seite 567-572 (DE-627)300895925 (DE-600)1483376-1 1348-2246 nnns volume:7 year:1991 number:4 day:01 month:08 pages:567-572 https://dx.doi.org/10.2116/analsci.7.567 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_95 GBV_ILN_105 GBV_ILN_110 GBV_ILN_151 GBV_ILN_161 GBV_ILN_170 GBV_ILN_213 GBV_ILN_230 GBV_ILN_250 GBV_ILN_285 GBV_ILN_293 GBV_ILN_602 GBV_ILN_2014 GBV_ILN_4012 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4249 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4700 AR 7 1991 4 01 08 567-572 |
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Enthalten in Analytical sciences 7(1991), 4 vom: 01. Aug., Seite 567-572 volume:7 year:1991 number:4 day:01 month:08 pages:567-572 |
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Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis Supercritical fluid extraction (dpeaa)DE-He213 supercritical fluid chromatography (dpeaa)DE-He213 residue analysis (dpeaa)DE-He213 filter paper (dpeaa)DE-He213 soil (dpeaa)DE-He213 crop (dpeaa)DE-He213 electronic distribution (dpeaa)DE-He213 |
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Application of Supercritical Fluid Extraction/ Supercritical Fluid Chromatography to Pesticide Residue Analysis |
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Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. © The Japan Society for Analytical Chemistry 1991 |
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Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. © The Japan Society for Analytical Chemistry 1991 |
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Abstract A new double-stage separation method was developed for residue analysis using direct coupling of supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC). While conventional residue analysis requires much time and labor, this new method makes it possible to extract analytes selectively with a small amount of organic solvent and to introduce them into the Chromatograph without injection. In this study, the extraction of pesticide residues from soil and various plant samples was investigated. In all cases, the pesticides were successfully extracted with supercritical carbon dioxide, especially with control of their separation from co-extracts in various ways, including adjustment of the modifier. For the soil samples, the extraction behavior of each pesticide from the matrix is discussed in terms of their electronic structures. © The Japan Society for Analytical Chemistry 1991 |
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