Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium

Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the ex...
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Autor*in:	Nair, Deepika [verfasserIn] Gireesan, Prema Banerjee, D. Mishra, R. K. Kumar, Sanjay Manohar, Smitha

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2022

Schlagwörter:	Actinide partitioning Minor actinide Lanthanide-actinide separation Bistriazinyl pyridines (BTPs) Camphor bistriazinyl pyridine (CA-BTP) Extraction chromatography

Anmerkung:	© Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Übergeordnetes Werk:	Enthalten in: Journal of radioanalytical and nuclear chemistry - Dordrecht [u.a.] : Springer Science + Business Media B.V., 1968, 331(2022), 12 vom: 22. Nov., Seite 5557-5567
Übergeordnetes Werk:	volume:331 ; year:2022 ; number:12 ; day:22 ; month:11 ; pages:5557-5567

Links:	Volltext

DOI / URN:	10.1007/s10967-022-08663-w

Katalog-ID:	SPR048950483

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520			\|a Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%.
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700	1		\|a Gireesan, Prema \|4 aut
700	1		\|a Banerjee, D. \|0 (orcid)0000-0002-3003-5453 \|4 aut
700	1		\|a Mishra, R. K. \|4 aut
700	1		\|a Kumar, Sanjay \|4 aut
700	1		\|a Manohar, Smitha \|4 aut
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912			\|a GBV_ILN_171
912			\|a GBV_ILN_187
912			\|a GBV_ILN_206
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_250
912			\|a GBV_ILN_281
912			\|a GBV_ILN_285
912			\|a GBV_ILN_293
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_636
912			\|a GBV_ILN_702
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912			\|a GBV_ILN_2006
912			\|a GBV_ILN_2007
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912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2031
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2037
912			\|a GBV_ILN_2038
912			\|a GBV_ILN_2039
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2056
912			\|a GBV_ILN_2057
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2065
912			\|a GBV_ILN_2068
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2093
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2107
912			\|a GBV_ILN_2108
912			\|a GBV_ILN_2110
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912			\|a GBV_ILN_4328
912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4335
912			\|a GBV_ILN_4336
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allfields	10.1007/s10967-022-08663-w doi (DE-627)SPR048950483 (SPR)s10967-022-08663-w-e DE-627 ger DE-627 rakwb eng Nair, Deepika verfasserin aut Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. Actinide partitioning (dpeaa)DE-He213 Minor actinide (dpeaa)DE-He213 Lanthanide-actinide separation (dpeaa)DE-He213 Bistriazinyl pyridines (BTPs) (dpeaa)DE-He213 Camphor bistriazinyl pyridine (CA-BTP) (dpeaa)DE-He213 Extraction chromatography (dpeaa)DE-He213 Gireesan, Prema aut Banerjee, D. (orcid)0000-0002-3003-5453 aut Mishra, R. K. aut Kumar, Sanjay aut Manohar, Smitha aut Enthalten in Journal of radioanalytical and nuclear chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1968 331(2022), 12 vom: 22. Nov., Seite 5557-5567 (DE-627)320578011 (DE-600)2017242-4 1588-2780 nnns volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567 https://dx.doi.org/10.1007/s10967-022-08663-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 331 2022 12 22 11 5557-5567
spelling	10.1007/s10967-022-08663-w doi (DE-627)SPR048950483 (SPR)s10967-022-08663-w-e DE-627 ger DE-627 rakwb eng Nair, Deepika verfasserin aut Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. Actinide partitioning (dpeaa)DE-He213 Minor actinide (dpeaa)DE-He213 Lanthanide-actinide separation (dpeaa)DE-He213 Bistriazinyl pyridines (BTPs) (dpeaa)DE-He213 Camphor bistriazinyl pyridine (CA-BTP) (dpeaa)DE-He213 Extraction chromatography (dpeaa)DE-He213 Gireesan, Prema aut Banerjee, D. (orcid)0000-0002-3003-5453 aut Mishra, R. K. aut Kumar, Sanjay aut Manohar, Smitha aut Enthalten in Journal of radioanalytical and nuclear chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1968 331(2022), 12 vom: 22. Nov., Seite 5557-5567 (DE-627)320578011 (DE-600)2017242-4 1588-2780 nnns volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567 https://dx.doi.org/10.1007/s10967-022-08663-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 331 2022 12 22 11 5557-5567
allfields_unstemmed	10.1007/s10967-022-08663-w doi (DE-627)SPR048950483 (SPR)s10967-022-08663-w-e DE-627 ger DE-627 rakwb eng Nair, Deepika verfasserin aut Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. Actinide partitioning (dpeaa)DE-He213 Minor actinide (dpeaa)DE-He213 Lanthanide-actinide separation (dpeaa)DE-He213 Bistriazinyl pyridines (BTPs) (dpeaa)DE-He213 Camphor bistriazinyl pyridine (CA-BTP) (dpeaa)DE-He213 Extraction chromatography (dpeaa)DE-He213 Gireesan, Prema aut Banerjee, D. (orcid)0000-0002-3003-5453 aut Mishra, R. K. aut Kumar, Sanjay aut Manohar, Smitha aut Enthalten in Journal of radioanalytical and nuclear chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1968 331(2022), 12 vom: 22. Nov., Seite 5557-5567 (DE-627)320578011 (DE-600)2017242-4 1588-2780 nnns volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567 https://dx.doi.org/10.1007/s10967-022-08663-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 331 2022 12 22 11 5557-5567
allfieldsGer	10.1007/s10967-022-08663-w doi (DE-627)SPR048950483 (SPR)s10967-022-08663-w-e DE-627 ger DE-627 rakwb eng Nair, Deepika verfasserin aut Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. Actinide partitioning (dpeaa)DE-He213 Minor actinide (dpeaa)DE-He213 Lanthanide-actinide separation (dpeaa)DE-He213 Bistriazinyl pyridines (BTPs) (dpeaa)DE-He213 Camphor bistriazinyl pyridine (CA-BTP) (dpeaa)DE-He213 Extraction chromatography (dpeaa)DE-He213 Gireesan, Prema aut Banerjee, D. (orcid)0000-0002-3003-5453 aut Mishra, R. K. aut Kumar, Sanjay aut Manohar, Smitha aut Enthalten in Journal of radioanalytical and nuclear chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1968 331(2022), 12 vom: 22. Nov., Seite 5557-5567 (DE-627)320578011 (DE-600)2017242-4 1588-2780 nnns volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567 https://dx.doi.org/10.1007/s10967-022-08663-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 331 2022 12 22 11 5557-5567
allfieldsSound	10.1007/s10967-022-08663-w doi (DE-627)SPR048950483 (SPR)s10967-022-08663-w-e DE-627 ger DE-627 rakwb eng Nair, Deepika verfasserin aut Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. Actinide partitioning (dpeaa)DE-He213 Minor actinide (dpeaa)DE-He213 Lanthanide-actinide separation (dpeaa)DE-He213 Bistriazinyl pyridines (BTPs) (dpeaa)DE-He213 Camphor bistriazinyl pyridine (CA-BTP) (dpeaa)DE-He213 Extraction chromatography (dpeaa)DE-He213 Gireesan, Prema aut Banerjee, D. (orcid)0000-0002-3003-5453 aut Mishra, R. K. aut Kumar, Sanjay aut Manohar, Smitha aut Enthalten in Journal of radioanalytical and nuclear chemistry Dordrecht [u.a.] : Springer Science + Business Media B.V., 1968 331(2022), 12 vom: 22. Nov., Seite 5557-5567 (DE-627)320578011 (DE-600)2017242-4 1588-2780 nnns volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567 https://dx.doi.org/10.1007/s10967-022-08663-w lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER SSG-OLC-PHA GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 331 2022 12 22 11 5557-5567
language	English
source	Enthalten in Journal of radioanalytical and nuclear chemistry 331(2022), 12 vom: 22. Nov., Seite 5557-5567 volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567
sourceStr	Enthalten in Journal of radioanalytical and nuclear chemistry 331(2022), 12 vom: 22. Nov., Seite 5557-5567 volume:331 year:2022 number:12 day:22 month:11 pages:5557-5567
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Actinide partitioning Minor actinide Lanthanide-actinide separation Bistriazinyl pyridines (BTPs) Camphor bistriazinyl pyridine (CA-BTP) Extraction chromatography
isfreeaccess_bool	false
container_title	Journal of radioanalytical and nuclear chemistry
authorswithroles_txt_mv	Nair, Deepika @@aut@@ Gireesan, Prema @@aut@@ Banerjee, D. @@aut@@ Mishra, R. K. @@aut@@ Kumar, Sanjay @@aut@@ Manohar, Smitha @@aut@@
publishDateDaySort_date	2022-11-22T00:00:00Z
hierarchy_top_id	320578011
id	SPR048950483
language_de	englisch
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The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. 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author	Nair, Deepika
spellingShingle	Nair, Deepika misc Actinide partitioning misc Minor actinide misc Lanthanide-actinide separation misc Bistriazinyl pyridines (BTPs) misc Camphor bistriazinyl pyridine (CA-BTP) misc Extraction chromatography Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium
authorStr	Nair, Deepika
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topic_title	Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium Actinide partitioning (dpeaa)DE-He213 Minor actinide (dpeaa)DE-He213 Lanthanide-actinide separation (dpeaa)DE-He213 Bistriazinyl pyridines (BTPs) (dpeaa)DE-He213 Camphor bistriazinyl pyridine (CA-BTP) (dpeaa)DE-He213 Extraction chromatography (dpeaa)DE-He213
topic	misc Actinide partitioning misc Minor actinide misc Lanthanide-actinide separation misc Bistriazinyl pyridines (BTPs) misc Camphor bistriazinyl pyridine (CA-BTP) misc Extraction chromatography
topic_unstemmed	misc Actinide partitioning misc Minor actinide misc Lanthanide-actinide separation misc Bistriazinyl pyridines (BTPs) misc Camphor bistriazinyl pyridine (CA-BTP) misc Extraction chromatography
topic_browse	misc Actinide partitioning misc Minor actinide misc Lanthanide-actinide separation misc Bistriazinyl pyridines (BTPs) misc Camphor bistriazinyl pyridine (CA-BTP) misc Extraction chromatography
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title	Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium
ctrlnum	(DE-627)SPR048950483 (SPR)s10967-022-08663-w-e
title_full	Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium
author_sort	Nair, Deepika
journal	Journal of radioanalytical and nuclear chemistry
journalStr	Journal of radioanalytical and nuclear chemistry
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author_browse	Nair, Deepika Gireesan, Prema Banerjee, D. Mishra, R. K. Kumar, Sanjay Manohar, Smitha
container_volume	331
format_se	Elektronische Aufsätze
author-letter	Nair, Deepika
doi_str_mv	10.1007/s10967-022-08663-w
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title_sort	extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium
title_auth	Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium
abstract	Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstractGer	Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstract_unstemmed	Abstract Camphor-bistriazinyl pyridine (bis-2,6-(5,6,7,8-tetrahydro-5,9,9-trimethyl-5,8-methano-1,2,4-benzotriazin-3-yl) pyridine (CA-BTP)) was synthesized and used to prepare two different resins for extraction chromatography studies. CA-BTP/XAD-7 resin was prepared by the direct sorption of the extractant CA-BTP onto the inert XAD-7 support. In contrast, CA-BTP-Oct/XAD-7 resin was prepared such that a polar diluent 1-octanol was incorporated along with the extractant CA-BTP into the resin beads. The extraction performance of both these resins was investigated in batch studies to separate Am(III) from Eu(III) in acidic nitrate solutions. Comparing the results obtained for both the resins indicated that CA-BTP-Oct/XAD-7 resin has better selectivity for Am(III) over Eu(III). In extraction chromatography, the separation of Am(III) from Eu(III) was demonstrated using CA-BTP-Oct/XAD-7 resin. Am(III) was quantitatively recovered from the column with a Eu(III) contamination of only 9%. © Akadémiai Kiadó, Budapest, Hungary 2022. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
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container_issue	12
title_short	Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium
url	https://dx.doi.org/10.1007/s10967-022-08663-w
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author2	Gireesan, Prema Banerjee, D. Mishra, R. K. Kumar, Sanjay Manohar, Smitha
author2Str	Gireesan, Prema Banerjee, D. Mishra, R. K. Kumar, Sanjay Manohar, Smitha
ppnlink	320578011
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doi_str	10.1007/s10967-022-08663-w
up_date	2024-07-03T22:25:46.871Z
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Extraction chromatography studies using camphor-bistriazinyl pyridine impregnated resins for americium separation from europium

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