Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil
Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization...
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| Autor*in: |
Hasan, M. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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© The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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| Übergeordnetes Werk: |
Enthalten in: Sensing and instrumentation for food quality and safety - New York, NY : Springer, 2007, 17(2022), 1 vom: 16. Sept., Seite 306-316 |
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| Übergeordnetes Werk: |
volume:17 ; year:2022 ; number:1 ; day:16 ; month:09 ; pages:306-316 |
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| DOI / URN: |
10.1007/s11694-022-01616-7 |
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SPR049154257 |
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| 520 | |a Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. | ||
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10.1007/s11694-022-01616-7 doi (DE-627)SPR049154257 (SPR)s11694-022-01616-7-e DE-627 ger DE-627 rakwb eng Hasan, M. verfasserin (orcid)0000-0001-5974-4053 aut Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. Facile fabrication (dpeaa)DE-He213 Active packaging (dpeaa)DE-He213 Clove oil (dpeaa)DE-He213 Corn starch (dpeaa)DE-He213 chitosan (dpeaa)DE-He213 Khaldun, Ibnu aut Zatya, Ismi aut Rusman, Rusman aut Nasir, M. aut Enthalten in Sensing and instrumentation for food quality and safety New York, NY : Springer, 2007 17(2022), 1 vom: 16. Sept., Seite 306-316 (DE-627)528359339 (DE-600)2279937-0 1932-9954 nnns volume:17 year:2022 number:1 day:16 month:09 pages:306-316 https://dx.doi.org/10.1007/s11694-022-01616-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_285 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2014 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2059 GBV_ILN_2106 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_2129 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2153 GBV_ILN_2190 AR 17 2022 1 16 09 306-316 |
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10.1007/s11694-022-01616-7 doi (DE-627)SPR049154257 (SPR)s11694-022-01616-7-e DE-627 ger DE-627 rakwb eng Hasan, M. verfasserin (orcid)0000-0001-5974-4053 aut Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. Facile fabrication (dpeaa)DE-He213 Active packaging (dpeaa)DE-He213 Clove oil (dpeaa)DE-He213 Corn starch (dpeaa)DE-He213 chitosan (dpeaa)DE-He213 Khaldun, Ibnu aut Zatya, Ismi aut Rusman, Rusman aut Nasir, M. aut Enthalten in Sensing and instrumentation for food quality and safety New York, NY : Springer, 2007 17(2022), 1 vom: 16. Sept., Seite 306-316 (DE-627)528359339 (DE-600)2279937-0 1932-9954 nnns volume:17 year:2022 number:1 day:16 month:09 pages:306-316 https://dx.doi.org/10.1007/s11694-022-01616-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_285 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2014 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2059 GBV_ILN_2106 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_2129 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2153 GBV_ILN_2190 AR 17 2022 1 16 09 306-316 |
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10.1007/s11694-022-01616-7 doi (DE-627)SPR049154257 (SPR)s11694-022-01616-7-e DE-627 ger DE-627 rakwb eng Hasan, M. verfasserin (orcid)0000-0001-5974-4053 aut Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. Facile fabrication (dpeaa)DE-He213 Active packaging (dpeaa)DE-He213 Clove oil (dpeaa)DE-He213 Corn starch (dpeaa)DE-He213 chitosan (dpeaa)DE-He213 Khaldun, Ibnu aut Zatya, Ismi aut Rusman, Rusman aut Nasir, M. aut Enthalten in Sensing and instrumentation for food quality and safety New York, NY : Springer, 2007 17(2022), 1 vom: 16. Sept., Seite 306-316 (DE-627)528359339 (DE-600)2279937-0 1932-9954 nnns volume:17 year:2022 number:1 day:16 month:09 pages:306-316 https://dx.doi.org/10.1007/s11694-022-01616-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_285 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2014 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2059 GBV_ILN_2106 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_2129 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2153 GBV_ILN_2190 AR 17 2022 1 16 09 306-316 |
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10.1007/s11694-022-01616-7 doi (DE-627)SPR049154257 (SPR)s11694-022-01616-7-e DE-627 ger DE-627 rakwb eng Hasan, M. verfasserin (orcid)0000-0001-5974-4053 aut Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. Facile fabrication (dpeaa)DE-He213 Active packaging (dpeaa)DE-He213 Clove oil (dpeaa)DE-He213 Corn starch (dpeaa)DE-He213 chitosan (dpeaa)DE-He213 Khaldun, Ibnu aut Zatya, Ismi aut Rusman, Rusman aut Nasir, M. aut Enthalten in Sensing and instrumentation for food quality and safety New York, NY : Springer, 2007 17(2022), 1 vom: 16. Sept., Seite 306-316 (DE-627)528359339 (DE-600)2279937-0 1932-9954 nnns volume:17 year:2022 number:1 day:16 month:09 pages:306-316 https://dx.doi.org/10.1007/s11694-022-01616-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_285 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2014 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2059 GBV_ILN_2106 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_2129 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2153 GBV_ILN_2190 AR 17 2022 1 16 09 306-316 |
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10.1007/s11694-022-01616-7 doi (DE-627)SPR049154257 (SPR)s11694-022-01616-7-e DE-627 ger DE-627 rakwb eng Hasan, M. verfasserin (orcid)0000-0001-5974-4053 aut Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil 2022 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. Facile fabrication (dpeaa)DE-He213 Active packaging (dpeaa)DE-He213 Clove oil (dpeaa)DE-He213 Corn starch (dpeaa)DE-He213 chitosan (dpeaa)DE-He213 Khaldun, Ibnu aut Zatya, Ismi aut Rusman, Rusman aut Nasir, M. aut Enthalten in Sensing and instrumentation for food quality and safety New York, NY : Springer, 2007 17(2022), 1 vom: 16. Sept., Seite 306-316 (DE-627)528359339 (DE-600)2279937-0 1932-9954 nnns volume:17 year:2022 number:1 day:16 month:09 pages:306-316 https://dx.doi.org/10.1007/s11694-022-01616-7 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_285 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2014 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2059 GBV_ILN_2106 GBV_ILN_2111 GBV_ILN_2119 GBV_ILN_2129 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2153 GBV_ILN_2190 AR 17 2022 1 16 09 306-316 |
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Hasan, M. |
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Hasan, M. misc Facile fabrication misc Active packaging misc Clove oil misc Corn starch misc chitosan Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil |
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Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil Facile fabrication (dpeaa)DE-He213 Active packaging (dpeaa)DE-He213 Clove oil (dpeaa)DE-He213 Corn starch (dpeaa)DE-He213 chitosan (dpeaa)DE-He213 |
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facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil |
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Facile fabrication and characterization of an economical active packaging film based on corn starch–chitosan biocomposites incorporated with clove oil |
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Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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Abstract Corn starch (CS)–chitosan (CH) films containing 9% w/w of clove oil (CO) were fabricated, and the structure, physicochemical, barrier, antioxidant activity, and biodegradability performance of the films were characterized. According to the results of atomic force microscopy characterization, the fabricated CH–CS films have a uniform shape and a smooth surface. Fourier transform infrared spectra show similar pattern absorption peaks, with the amplitude at some absorption peaks changing because of hydrogen bond formation of CH/CS-COs. The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. The fabricated film can be used for active packaging and can replace packaging films manufactured from native CH and CS, as well as reduce the use of packaging films derived from petrochemical raw materials. © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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The semicrystalline microstructure of the films was confirmed by X-ray diffraction (XRD) rheological studies. The XRD patterns for all combinations of the CH/CS matrix composition are identical. All CH/CS biocomposite films exhibit a very significant increase in tensile strength (TS) values, i.e., from 2.312 to 2.641 MPa, compared with the native CS (1.203 MPa) and CH (0.226 MPa) film, as well as their thermal stability. As the CH content in the matrix increases, the water vapor permeability (WVP) value of the films gradually decreases. The WVP value of pure CS is 10.13 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $, whereas the CH70CS30 sample has a WVP value of 2.17 × $ 10^{− 9} $ g.$ Pa^{− 1} %$ s^{− 1} $ $ m^{− 1} $. 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