Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives

Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side...
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Autor*in:	Shahzady, Tanzeela G. [verfasserIn] Rehman, Hajira Shuaib, Ahmad Ali, Zulfiqar Khurshid, Shazia Mushtaq, Amir

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2023

Schlagwörter:	Polyphosphazenes Biodegradable Hydrolytic degradation Biocompatible Hexachlorocyclotriphosphazene (HCCP) Thermal ring opening polymerization (T-ROP)

Anmerkung:	© The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Übergeordnetes Werk:	Enthalten in: Journal of polymer research - Dordrecht : Springer Science + Business Media B.V., 1994, 31(2023), 1 vom: 22. Dez.
Übergeordnetes Werk:	volume:31 ; year:2023 ; number:1 ; day:22 ; month:12

Links:	Volltext

DOI / URN:	10.1007/s10965-023-03841-0

Katalog-ID:	SPR054163072

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520			\|a Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field.
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912			\|a GBV_ILN_161
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allfields	10.1007/s10965-023-03841-0 doi (DE-627)SPR054163072 (SPR)s10965-023-03841-0-e DE-627 ger DE-627 rakwb eng Shahzady, Tanzeela G. verfasserin aut Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. Polyphosphazenes (dpeaa)DE-He213 Biodegradable (dpeaa)DE-He213 Hydrolytic degradation (dpeaa)DE-He213 Biocompatible (dpeaa)DE-He213 Hexachlorocyclotriphosphazene (HCCP) (dpeaa)DE-He213 Thermal ring opening polymerization (T-ROP) (dpeaa)DE-He213 Rehman, Hajira aut Shuaib, Ahmad aut Ali, Zulfiqar (orcid)0000-0003-2306-1159 aut Khurshid, Shazia aut Mushtaq, Amir aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 31(2023), 1 vom: 22. Dez. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:31 year:2023 number:1 day:22 month:12 https://dx.doi.org/10.1007/s10965-023-03841-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 31 2023 1 22 12
spelling	10.1007/s10965-023-03841-0 doi (DE-627)SPR054163072 (SPR)s10965-023-03841-0-e DE-627 ger DE-627 rakwb eng Shahzady, Tanzeela G. verfasserin aut Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. Polyphosphazenes (dpeaa)DE-He213 Biodegradable (dpeaa)DE-He213 Hydrolytic degradation (dpeaa)DE-He213 Biocompatible (dpeaa)DE-He213 Hexachlorocyclotriphosphazene (HCCP) (dpeaa)DE-He213 Thermal ring opening polymerization (T-ROP) (dpeaa)DE-He213 Rehman, Hajira aut Shuaib, Ahmad aut Ali, Zulfiqar (orcid)0000-0003-2306-1159 aut Khurshid, Shazia aut Mushtaq, Amir aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 31(2023), 1 vom: 22. Dez. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:31 year:2023 number:1 day:22 month:12 https://dx.doi.org/10.1007/s10965-023-03841-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 31 2023 1 22 12
allfields_unstemmed	10.1007/s10965-023-03841-0 doi (DE-627)SPR054163072 (SPR)s10965-023-03841-0-e DE-627 ger DE-627 rakwb eng Shahzady, Tanzeela G. verfasserin aut Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. Polyphosphazenes (dpeaa)DE-He213 Biodegradable (dpeaa)DE-He213 Hydrolytic degradation (dpeaa)DE-He213 Biocompatible (dpeaa)DE-He213 Hexachlorocyclotriphosphazene (HCCP) (dpeaa)DE-He213 Thermal ring opening polymerization (T-ROP) (dpeaa)DE-He213 Rehman, Hajira aut Shuaib, Ahmad aut Ali, Zulfiqar (orcid)0000-0003-2306-1159 aut Khurshid, Shazia aut Mushtaq, Amir aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 31(2023), 1 vom: 22. Dez. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:31 year:2023 number:1 day:22 month:12 https://dx.doi.org/10.1007/s10965-023-03841-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 31 2023 1 22 12
allfieldsGer	10.1007/s10965-023-03841-0 doi (DE-627)SPR054163072 (SPR)s10965-023-03841-0-e DE-627 ger DE-627 rakwb eng Shahzady, Tanzeela G. verfasserin aut Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. Polyphosphazenes (dpeaa)DE-He213 Biodegradable (dpeaa)DE-He213 Hydrolytic degradation (dpeaa)DE-He213 Biocompatible (dpeaa)DE-He213 Hexachlorocyclotriphosphazene (HCCP) (dpeaa)DE-He213 Thermal ring opening polymerization (T-ROP) (dpeaa)DE-He213 Rehman, Hajira aut Shuaib, Ahmad aut Ali, Zulfiqar (orcid)0000-0003-2306-1159 aut Khurshid, Shazia aut Mushtaq, Amir aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 31(2023), 1 vom: 22. Dez. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:31 year:2023 number:1 day:22 month:12 https://dx.doi.org/10.1007/s10965-023-03841-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 31 2023 1 22 12
allfieldsSound	10.1007/s10965-023-03841-0 doi (DE-627)SPR054163072 (SPR)s10965-023-03841-0-e DE-627 ger DE-627 rakwb eng Shahzady, Tanzeela G. verfasserin aut Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives 2023 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. Polyphosphazenes (dpeaa)DE-He213 Biodegradable (dpeaa)DE-He213 Hydrolytic degradation (dpeaa)DE-He213 Biocompatible (dpeaa)DE-He213 Hexachlorocyclotriphosphazene (HCCP) (dpeaa)DE-He213 Thermal ring opening polymerization (T-ROP) (dpeaa)DE-He213 Rehman, Hajira aut Shuaib, Ahmad aut Ali, Zulfiqar (orcid)0000-0003-2306-1159 aut Khurshid, Shazia aut Mushtaq, Amir aut Enthalten in Journal of polymer research Dordrecht : Springer Science + Business Media B.V., 1994 31(2023), 1 vom: 22. Dez. (DE-627)340872098 (DE-600)2065616-6 1572-8935 nnns volume:31 year:2023 number:1 day:22 month:12 https://dx.doi.org/10.1007/s10965-023-03841-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_206 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 31 2023 1 22 12
language	English
source	Enthalten in Journal of polymer research 31(2023), 1 vom: 22. Dez. volume:31 year:2023 number:1 day:22 month:12
sourceStr	Enthalten in Journal of polymer research 31(2023), 1 vom: 22. Dez. volume:31 year:2023 number:1 day:22 month:12
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Polyphosphazenes Biodegradable Hydrolytic degradation Biocompatible Hexachlorocyclotriphosphazene (HCCP) Thermal ring opening polymerization (T-ROP)
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container_title	Journal of polymer research
authorswithroles_txt_mv	Shahzady, Tanzeela G. @@aut@@ Rehman, Hajira @@aut@@ Shuaib, Ahmad @@aut@@ Ali, Zulfiqar @@aut@@ Khurshid, Shazia @@aut@@ Mushtaq, Amir @@aut@@
publishDateDaySort_date	2023-12-22T00:00:00Z
hierarchy_top_id	340872098
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author	Shahzady, Tanzeela G.
spellingShingle	Shahzady, Tanzeela G. misc Polyphosphazenes misc Biodegradable misc Hydrolytic degradation misc Biocompatible misc Hexachlorocyclotriphosphazene (HCCP) misc Thermal ring opening polymerization (T-ROP) Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives
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topic_title	Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives Polyphosphazenes (dpeaa)DE-He213 Biodegradable (dpeaa)DE-He213 Hydrolytic degradation (dpeaa)DE-He213 Biocompatible (dpeaa)DE-He213 Hexachlorocyclotriphosphazene (HCCP) (dpeaa)DE-He213 Thermal ring opening polymerization (T-ROP) (dpeaa)DE-He213
topic	misc Polyphosphazenes misc Biodegradable misc Hydrolytic degradation misc Biocompatible misc Hexachlorocyclotriphosphazene (HCCP) misc Thermal ring opening polymerization (T-ROP)
topic_unstemmed	misc Polyphosphazenes misc Biodegradable misc Hydrolytic degradation misc Biocompatible misc Hexachlorocyclotriphosphazene (HCCP) misc Thermal ring opening polymerization (T-ROP)
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title	Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives
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title_full	Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives
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author_browse	Shahzady, Tanzeela G. Rehman, Hajira Shuaib, Ahmad Ali, Zulfiqar Khurshid, Shazia Mushtaq, Amir
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title_sort	synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives
title_auth	Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives
abstract	Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstractGer	Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstract_unstemmed	Abstract In this study, the cyclic trimer of hexachlorocyclotriphosphazene (HCCP) was used as the starting material for the thermal ring opening polymerization (T-ROP) method, which was followed by a macromolecular substitution reaction to create three Polyphosphazene derivatives with aromatic side groups. FTIR, 1HNMR, 31PNMR, DSC, elemental analysis, and gel permeation chromatography were used to characterise the synthesised polymer (GPC). The hydrolytic breakdown using shaker bath was studied at various pH at 37 °C for 42 days. Significant degradation products were noticed at different pH values. Studies on degradation revealed that synthetic polymers offer a wide range of potential uses in the biological field. © The Polymer Society, Taipei 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
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Synthesis, characterization and hydrolytic degradation studies of aromatic polyphosphazenes derivatives

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