Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation

Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical prope...
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Autor*in:	Hebbaz, Abdennour [verfasserIn] Belhani, Mehdi Tahraoui, Tarek

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2024

Schlagwörter:	Cerium-doped magnesium spinel ferrite Co-precipitation Fenton-like Magnesium spinel ferrite Photocatalytic activity Sunlight

Anmerkung:	© The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Übergeordnetes Werk:	Enthalten in: Applied physics - Berlin : Springer, 1973, 130(2024), 2 vom: 13. Jan.
Übergeordnetes Werk:	volume:130 ; year:2024 ; number:2 ; day:13 ; month:01

Links:	Volltext

DOI / URN:	10.1007/s00339-023-07219-3

Katalog-ID:	SPR054378648

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520			\|a Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min.
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650		4	\|a Photocatalytic activity \|7 (dpeaa)DE-He213
650		4	\|a Sunlight \|7 (dpeaa)DE-He213
700	1		\|a Belhani, Mehdi \|4 aut
700	1		\|a Tahraoui, Tarek \|4 aut
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author_variant	a h ah m b mb t t tt
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allfields	10.1007/s00339-023-07219-3 doi (DE-627)SPR054378648 (SPR)s00339-023-07219-3-e DE-627 ger DE-627 rakwb eng Hebbaz, Abdennour verfasserin (orcid)0000-0001-6837-6678 aut Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. Cerium-doped magnesium spinel ferrite (dpeaa)DE-He213 Co-precipitation (dpeaa)DE-He213 Fenton-like (dpeaa)DE-He213 Magnesium spinel ferrite (dpeaa)DE-He213 Photocatalytic activity (dpeaa)DE-He213 Sunlight (dpeaa)DE-He213 Belhani, Mehdi aut Tahraoui, Tarek aut Enthalten in Applied physics Berlin : Springer, 1973 130(2024), 2 vom: 13. Jan. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:130 year:2024 number:2 day:13 month:01 https://dx.doi.org/10.1007/s00339-023-07219-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 130 2024 2 13 01
spelling	10.1007/s00339-023-07219-3 doi (DE-627)SPR054378648 (SPR)s00339-023-07219-3-e DE-627 ger DE-627 rakwb eng Hebbaz, Abdennour verfasserin (orcid)0000-0001-6837-6678 aut Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. Cerium-doped magnesium spinel ferrite (dpeaa)DE-He213 Co-precipitation (dpeaa)DE-He213 Fenton-like (dpeaa)DE-He213 Magnesium spinel ferrite (dpeaa)DE-He213 Photocatalytic activity (dpeaa)DE-He213 Sunlight (dpeaa)DE-He213 Belhani, Mehdi aut Tahraoui, Tarek aut Enthalten in Applied physics Berlin : Springer, 1973 130(2024), 2 vom: 13. Jan. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:130 year:2024 number:2 day:13 month:01 https://dx.doi.org/10.1007/s00339-023-07219-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 130 2024 2 13 01
allfields_unstemmed	10.1007/s00339-023-07219-3 doi (DE-627)SPR054378648 (SPR)s00339-023-07219-3-e DE-627 ger DE-627 rakwb eng Hebbaz, Abdennour verfasserin (orcid)0000-0001-6837-6678 aut Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. Cerium-doped magnesium spinel ferrite (dpeaa)DE-He213 Co-precipitation (dpeaa)DE-He213 Fenton-like (dpeaa)DE-He213 Magnesium spinel ferrite (dpeaa)DE-He213 Photocatalytic activity (dpeaa)DE-He213 Sunlight (dpeaa)DE-He213 Belhani, Mehdi aut Tahraoui, Tarek aut Enthalten in Applied physics Berlin : Springer, 1973 130(2024), 2 vom: 13. Jan. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:130 year:2024 number:2 day:13 month:01 https://dx.doi.org/10.1007/s00339-023-07219-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 130 2024 2 13 01
allfieldsGer	10.1007/s00339-023-07219-3 doi (DE-627)SPR054378648 (SPR)s00339-023-07219-3-e DE-627 ger DE-627 rakwb eng Hebbaz, Abdennour verfasserin (orcid)0000-0001-6837-6678 aut Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. Cerium-doped magnesium spinel ferrite (dpeaa)DE-He213 Co-precipitation (dpeaa)DE-He213 Fenton-like (dpeaa)DE-He213 Magnesium spinel ferrite (dpeaa)DE-He213 Photocatalytic activity (dpeaa)DE-He213 Sunlight (dpeaa)DE-He213 Belhani, Mehdi aut Tahraoui, Tarek aut Enthalten in Applied physics Berlin : Springer, 1973 130(2024), 2 vom: 13. Jan. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:130 year:2024 number:2 day:13 month:01 https://dx.doi.org/10.1007/s00339-023-07219-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 130 2024 2 13 01
allfieldsSound	10.1007/s00339-023-07219-3 doi (DE-627)SPR054378648 (SPR)s00339-023-07219-3-e DE-627 ger DE-627 rakwb eng Hebbaz, Abdennour verfasserin (orcid)0000-0001-6837-6678 aut Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. Cerium-doped magnesium spinel ferrite (dpeaa)DE-He213 Co-precipitation (dpeaa)DE-He213 Fenton-like (dpeaa)DE-He213 Magnesium spinel ferrite (dpeaa)DE-He213 Photocatalytic activity (dpeaa)DE-He213 Sunlight (dpeaa)DE-He213 Belhani, Mehdi aut Tahraoui, Tarek aut Enthalten in Applied physics Berlin : Springer, 1973 130(2024), 2 vom: 13. Jan. (DE-627)235503231 (DE-600)1398311-8 1432-0630 nnns volume:130 year:2024 number:2 day:13 month:01 https://dx.doi.org/10.1007/s00339-023-07219-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_267 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 AR 130 2024 2 13 01
language	English
source	Enthalten in Applied physics 130(2024), 2 vom: 13. Jan. volume:130 year:2024 number:2 day:13 month:01
sourceStr	Enthalten in Applied physics 130(2024), 2 vom: 13. Jan. volume:130 year:2024 number:2 day:13 month:01
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Cerium-doped magnesium spinel ferrite Co-precipitation Fenton-like Magnesium spinel ferrite Photocatalytic activity Sunlight
isfreeaccess_bool	false
container_title	Applied physics
authorswithroles_txt_mv	Hebbaz, Abdennour @@aut@@ Belhani, Mehdi @@aut@@ Tahraoui, Tarek @@aut@@
publishDateDaySort_date	2024-01-13T00:00:00Z
hierarchy_top_id	235503231
id	SPR054378648
language_de	englisch
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Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. 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author	Hebbaz, Abdennour
spellingShingle	Hebbaz, Abdennour misc Cerium-doped magnesium spinel ferrite misc Co-precipitation misc Fenton-like misc Magnesium spinel ferrite misc Photocatalytic activity misc Sunlight Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation
authorStr	Hebbaz, Abdennour
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topic_title	Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation Cerium-doped magnesium spinel ferrite (dpeaa)DE-He213 Co-precipitation (dpeaa)DE-He213 Fenton-like (dpeaa)DE-He213 Magnesium spinel ferrite (dpeaa)DE-He213 Photocatalytic activity (dpeaa)DE-He213 Sunlight (dpeaa)DE-He213
topic	misc Cerium-doped magnesium spinel ferrite misc Co-precipitation misc Fenton-like misc Magnesium spinel ferrite misc Photocatalytic activity misc Sunlight
topic_unstemmed	misc Cerium-doped magnesium spinel ferrite misc Co-precipitation misc Fenton-like misc Magnesium spinel ferrite misc Photocatalytic activity misc Sunlight
topic_browse	misc Cerium-doped magnesium spinel ferrite misc Co-precipitation misc Fenton-like misc Magnesium spinel ferrite misc Photocatalytic activity misc Sunlight
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title	Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation
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title_full	Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation
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title_sort	synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation
title_auth	Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation
abstract	Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstractGer	Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
abstract_unstemmed	Abstract Magnesium spinel ferrite ($ MgFe_{2} %$ O_{4} $) and cerium-doped magnesium spinel ferrite ($ MgFe_{2-x} %$ Ce_{x} %$ O_{4} $) (x = 0.0, 0.05, 0.1) were synthesized using an inexpensive coprecipitation method. The investigation focused on the influence of cerium on the physicochemical properties and the photocatalytic activity of this material under sunlight irradiation. The various characterization techniques, including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), environmental scanning electron microscopy (ESEM-EDX), the Brunauer–Emmett–Teller (BET) method, and vibrating sample magnetometer (VSM), were used to determine the structural, morphological, and magnetic properties of the prepared samples. The increase in cerium percentage was found to better agglomerate the sheet-like morphology formed in the pure spinel and increase the average crystallite size, with a decrease in the magnetic properties. The optical band gap measured by UV–visible spectroscopy decreased from 2.21 eV, 2.21 eV, and 2.36 eV, accompanied by a change in the specific surface area of 47.23 $ m^{2} $/g, 57.86 $ m^{2} $/g, and 47.25 $ m^{2} $/g for $ MgFe_{2} %$ O_{4} $, $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $, and $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $, respectively. The maximum photocatalytic degradation of methylene blue under sunlight irradiation was achieved for the $ MgFe_{1.95} %$ Ce_{0.05} %$ O_{4} $ (58.35%) in the absence of hydrogen peroxide, and the maximum degradation for Fenton-like processes was achieved in the presence of $ MgFe_{1.90} %$ Ce_{0.1} %$ O_{4} $ (91.05%) within 180 min. © The Author(s), under exclusive licence to Springer-Verlag GmbH, DE part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
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title_short	Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation
url	https://dx.doi.org/10.1007/s00339-023-07219-3
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author2	Belhani, Mehdi Tahraoui, Tarek
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doi_str	10.1007/s00339-023-07219-3
up_date	2024-07-04T01:19:32.971Z
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Synthesis of cerium-doped magnesium spinel ferrites and study of their physical properties for photocatalytic applications under sunlight irradiation

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