An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique
Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture usi...
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| Autor*in: |
Kiran, Tupuri Vishnu [verfasserIn] Patil, Pravinkumar D. [verfasserIn] Thati, Jyothi [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2024 |
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| Schlagwörter: |
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| Anmerkung: |
© Indian Academy of Sciences 2024 |
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| Übergeordnetes Werk: |
Enthalten in: Resonance - Springer India, 1996, 29(2024), 5 vom: Mai, Seite 709-727 |
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| Übergeordnetes Werk: |
volume:29 ; year:2024 ; number:5 ; month:05 ; pages:709-727 |
| Links: |
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| DOI / URN: |
10.1007/s12045-024-0709-x |
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| Katalog-ID: |
SPR056870078 |
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| 245 | 1 | 0 | |a An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique |
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| 520 | |a Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. | ||
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10.1007/s12045-024-0709-x doi (DE-627)SPR056870078 (SPR)s12045-024-0709-x-e DE-627 ger DE-627 rakwb eng 500 VZ 30.00 bkl Kiran, Tupuri Vishnu verfasserin aut An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Indian Academy of Sciences 2024 Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. Seeding (dpeaa)DE-He213 nucleation (dpeaa)DE-He213 oxalic acid dihydrate (C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 2H (dpeaa)DE-He213 O) (dpeaa)DE-He213 cooling crystallization and crystal size distribution (dpeaa)DE-He213 Patil, Pravinkumar D. verfasserin aut Thati, Jyothi verfasserin aut Enthalten in Resonance Springer India, 1996 29(2024), 5 vom: Mai, Seite 709-727 (DE-627)352260963 (DE-600)2085223-X 0973-712X nnns volume:29 year:2024 number:5 month:05 pages:709-727 https://dx.doi.org/10.1007/s12045-024-0709-x X:SPRINGER Resolving-System lizenzpflichtig Volltext SYSFLAG_0 GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 30.00 VZ AR 29 2024 5 05 709-727 |
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10.1007/s12045-024-0709-x doi (DE-627)SPR056870078 (SPR)s12045-024-0709-x-e DE-627 ger DE-627 rakwb eng 500 VZ 30.00 bkl Kiran, Tupuri Vishnu verfasserin aut An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Indian Academy of Sciences 2024 Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. Seeding (dpeaa)DE-He213 nucleation (dpeaa)DE-He213 oxalic acid dihydrate (C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 2H (dpeaa)DE-He213 O) (dpeaa)DE-He213 cooling crystallization and crystal size distribution (dpeaa)DE-He213 Patil, Pravinkumar D. verfasserin aut Thati, Jyothi verfasserin aut Enthalten in Resonance Springer India, 1996 29(2024), 5 vom: Mai, Seite 709-727 (DE-627)352260963 (DE-600)2085223-X 0973-712X nnns volume:29 year:2024 number:5 month:05 pages:709-727 https://dx.doi.org/10.1007/s12045-024-0709-x X:SPRINGER Resolving-System lizenzpflichtig Volltext SYSFLAG_0 GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 30.00 VZ AR 29 2024 5 05 709-727 |
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10.1007/s12045-024-0709-x doi (DE-627)SPR056870078 (SPR)s12045-024-0709-x-e DE-627 ger DE-627 rakwb eng 500 VZ 30.00 bkl Kiran, Tupuri Vishnu verfasserin aut An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Indian Academy of Sciences 2024 Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. Seeding (dpeaa)DE-He213 nucleation (dpeaa)DE-He213 oxalic acid dihydrate (C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 2H (dpeaa)DE-He213 O) (dpeaa)DE-He213 cooling crystallization and crystal size distribution (dpeaa)DE-He213 Patil, Pravinkumar D. verfasserin aut Thati, Jyothi verfasserin aut Enthalten in Resonance Springer India, 1996 29(2024), 5 vom: Mai, Seite 709-727 (DE-627)352260963 (DE-600)2085223-X 0973-712X nnns volume:29 year:2024 number:5 month:05 pages:709-727 https://dx.doi.org/10.1007/s12045-024-0709-x X:SPRINGER Resolving-System lizenzpflichtig Volltext SYSFLAG_0 GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 30.00 VZ AR 29 2024 5 05 709-727 |
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10.1007/s12045-024-0709-x doi (DE-627)SPR056870078 (SPR)s12045-024-0709-x-e DE-627 ger DE-627 rakwb eng 500 VZ 30.00 bkl Kiran, Tupuri Vishnu verfasserin aut An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Indian Academy of Sciences 2024 Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. Seeding (dpeaa)DE-He213 nucleation (dpeaa)DE-He213 oxalic acid dihydrate (C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 2H (dpeaa)DE-He213 O) (dpeaa)DE-He213 cooling crystallization and crystal size distribution (dpeaa)DE-He213 Patil, Pravinkumar D. verfasserin aut Thati, Jyothi verfasserin aut Enthalten in Resonance Springer India, 1996 29(2024), 5 vom: Mai, Seite 709-727 (DE-627)352260963 (DE-600)2085223-X 0973-712X nnns volume:29 year:2024 number:5 month:05 pages:709-727 https://dx.doi.org/10.1007/s12045-024-0709-x X:SPRINGER Resolving-System lizenzpflichtig Volltext SYSFLAG_0 GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 30.00 VZ AR 29 2024 5 05 709-727 |
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10.1007/s12045-024-0709-x doi (DE-627)SPR056870078 (SPR)s12045-024-0709-x-e DE-627 ger DE-627 rakwb eng 500 VZ 30.00 bkl Kiran, Tupuri Vishnu verfasserin aut An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique 2024 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier © Indian Academy of Sciences 2024 Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. Seeding (dpeaa)DE-He213 nucleation (dpeaa)DE-He213 oxalic acid dihydrate (C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 2H (dpeaa)DE-He213 O) (dpeaa)DE-He213 cooling crystallization and crystal size distribution (dpeaa)DE-He213 Patil, Pravinkumar D. verfasserin aut Thati, Jyothi verfasserin aut Enthalten in Resonance Springer India, 1996 29(2024), 5 vom: Mai, Seite 709-727 (DE-627)352260963 (DE-600)2085223-X 0973-712X nnns volume:29 year:2024 number:5 month:05 pages:709-727 https://dx.doi.org/10.1007/s12045-024-0709-x X:SPRINGER Resolving-System lizenzpflichtig Volltext SYSFLAG_0 GBV_SPRINGER GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_39 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_120 GBV_ILN_138 GBV_ILN_150 GBV_ILN_151 GBV_ILN_152 GBV_ILN_161 GBV_ILN_170 GBV_ILN_171 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_250 GBV_ILN_281 GBV_ILN_285 GBV_ILN_293 GBV_ILN_370 GBV_ILN_602 GBV_ILN_636 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2037 GBV_ILN_2038 GBV_ILN_2039 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2057 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2093 GBV_ILN_2106 GBV_ILN_2107 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2144 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2188 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2446 GBV_ILN_2470 GBV_ILN_2472 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4012 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4246 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4328 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4367 GBV_ILN_4393 GBV_ILN_4700 30.00 VZ AR 29 2024 5 05 709-727 |
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Enthalten in Resonance 29(2024), 5 vom: Mai, Seite 709-727 volume:29 year:2024 number:5 month:05 pages:709-727 |
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Enthalten in Resonance 29(2024), 5 vom: Mai, Seite 709-727 volume:29 year:2024 number:5 month:05 pages:709-727 |
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Seeding nucleation oxalic acid dihydrate (C H O 2H O) cooling crystallization and crystal size distribution |
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Kiran, Tupuri Vishnu @@aut@@ Patil, Pravinkumar D. @@aut@@ Thati, Jyothi @@aut@@ |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000naa a22002652 4500</leader><controlfield tag="001">SPR056870078</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20240807064715.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">240807s2024 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s12045-024-0709-x</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)SPR056870078</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(SPR)s12045-024-0709-x-e</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">500</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">30.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Kiran, Tupuri Vishnu</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2024</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">Computermedien</subfield><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Indian Academy of Sciences 2024</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Seeding</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">nucleation</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">oxalic acid dihydrate (C</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">H</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">O</subfield><subfield code="7">(dpeaa)DE-He213</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield 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Kiran, Tupuri Vishnu |
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Kiran, Tupuri Vishnu ddc 500 bkl 30.00 misc Seeding misc nucleation misc oxalic acid dihydrate (C misc H misc O misc 2H misc O) misc cooling crystallization and crystal size distribution An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique |
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500 VZ 30.00 bkl An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique Seeding (dpeaa)DE-He213 nucleation (dpeaa)DE-He213 oxalic acid dihydrate (C (dpeaa)DE-He213 H (dpeaa)DE-He213 O (dpeaa)DE-He213 2H (dpeaa)DE-He213 O) (dpeaa)DE-He213 cooling crystallization and crystal size distribution (dpeaa)DE-He213 |
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ddc 500 bkl 30.00 misc Seeding misc nucleation misc oxalic acid dihydrate (C misc H misc O misc 2H misc O) misc cooling crystallization and crystal size distribution |
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An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique |
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Kiran, Tupuri Vishnu |
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10.1007/s12045-024-0709-x |
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an experimental study of crystallization of oxalic acid dihydrate ($ c_{2} $$ h_{2} $$ o_{4} $$ 2h_{2} $o) using the seeding technique |
| title_auth |
An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique |
| abstract |
Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. © Indian Academy of Sciences 2024 |
| abstractGer |
Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. © Indian Academy of Sciences 2024 |
| abstract_unstemmed |
Abstract Crystallization is one of the prominent unit operation processes in major chemical industries, such as pharmaceuticals, food, fine chemicals, etc. It is the last stage in the entire chemical process, and it is the purification step to separate one component from a multicomponent mixture using different crystallization methods. The objective of the crystallization process is to achieve good crystal attributes, such as good crystal purity, good crystal size distribution, mean crystal size, morphology, size, etc. The crystal quality can be achieved through various techniques that include the seeding technique and the non-seeding technique. The former is considered important when the objective of the product quality is not met with the usual crystallization process. It can direct towards process optimization. Although, it is a meaningful approach, it is a challenging task to achieve the desired quality of the crystal, process efficiency and optimization of the overall crystallization process. Seeding can also be done at a low level of supersaturation to trigger secondary nucleation, which is an important part of the crystallization process in crystal development. The solute concentration is increased in the existing solution with seeding of similar crystals. Reproducible crystal quality can be achieved by defining the reproducible crystal growth rate at the point of the process where seed crystals are added. The essential surface area of the seeds and the quality of the surface area are also important to define the size of the crystal. However, temperature and concentration play an important role in achieving the desired crystal attributes. The type of the temperature profile applied has a significant role in achieving the final crystalline product in the batch crystallization process. This experimental study aims to understand the particle size distribution of oxalic acid dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) crystals by evaluating solubility of oxalic acid at three different temperatures using seed crystals of size 250 µm. © Indian Academy of Sciences 2024 |
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An Experimental Study of Crystallization of Oxalic Acid Dihydrate ($ C_{2} $$ H_{2} $$ O_{4} $$ 2H_{2} $O) Using the Seeding Technique |
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| score |
7.3972845 |